EP4085994A1 - Mischgerät - Google Patents

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Publication number
EP4085994A1
EP4085994A1 EP22171403.3A EP22171403A EP4085994A1 EP 4085994 A1 EP4085994 A1 EP 4085994A1 EP 22171403 A EP22171403 A EP 22171403A EP 4085994 A1 EP4085994 A1 EP 4085994A1
Authority
EP
European Patent Office
Prior art keywords
substance
screw
mixing
chamber
fluid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP22171403.3A
Other languages
English (en)
French (fr)
Inventor
Claudio LOMMI
Paolo Ferrari
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ar Ecologia Srl
Original Assignee
Ar Ecologia Srl
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ar Ecologia Srl filed Critical Ar Ecologia Srl
Publication of EP4085994A1 publication Critical patent/EP4085994A1/de
Pending legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/192—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements
    • B01F27/1921—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements comprising helical elements and paddles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/115—Stirrers characterised by the configuration of the stirrers comprising discs or disc-like elements essentially perpendicular to the stirrer shaft axis
    • B01F27/1151—Stirrers characterised by the configuration of the stirrers comprising discs or disc-like elements essentially perpendicular to the stirrer shaft axis with holes on the surface
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/70—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/72—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with helices or sections of helices
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/73—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with rotary discs

Definitions

  • the flotation and dewatering treatments to which this sludge is subjected require that it be first added to and intimately mixed with specific chemical agents that change its chemical and physical characteristics, making it suitable for subsequent treatment.
  • chemical agents are usually polyelectrolytes, initially in the form of powders and/or emulsions.
  • aqueous solution of these polyelectrolytes in advance, with a concentration varying between 3 and 8 per thousand depending on the characteristics of the sludge to be treated, and then adding this solution to the sludge and mixing the mixture obtained, is known.
  • the solution is usually prepared in special mixing tanks into which the appropriate quantities of water and polyelectrolytes are placed, where the mixing action is carried out by means of motor-driven propellers.
  • the solution thus prepared is stored in the mixing tank until it is added to the sludge to be treated.
  • the water used to make this solution can be mains water or reclaimed water, depending on availability.
  • a first disadvantage relates to the use of mains water to prepare the aqueous solution: the occurrence of sudden pressure changes in the water supply system can compromise correct proportioning of the water and polyelectrolytes needed for the subsequent flotation or dewatering treatment.
  • mains water is particularly expensive and represents a significant cost item in plants using the process described above: an average-sized plant may use up to 250 cubic metres of water per day. If, on the other hand, waste water is used to make the aqueous solution, a different problem arises: waste water is usually very rich in chloride ions, which interfere with the added polyelectrolytes and significantly reduce their effectiveness in sludge treatment.
  • stirring by means of motor-driven propellers subjects the polyelectrolytes to considerable mechanical stresses caused by the high rotation speed of the blades, and these stresses can eventually cause the molecules of the polyelectrolytes and the lattices they form to break down when added to the water, consequently reducing the effectiveness of the solution in sludge treatment.
  • a number of devices have been developed which allow the sludge to be treated to be mixed directly with the polyelectrolytes, thus avoiding preparation of the aqueous solution in advance.
  • These devices are intended to effect particularly thorough mixing of the polyelectrolytes with the sludge, achieving a level of mixing between the two substances in just one step that would otherwise be achieved in two steps, that is by first making the aqueous polyelectrolyte solution and then adding this solution to the sludge.
  • These devices comprise powerful motor-driven propellers to mix the two substances, and special compulsory paths along which the sludge is run to force it to pass through the propellers several times.
  • the present invention relates to a mixing device.
  • the present invention relates to a device for mixing a first fluid substance and a second fluid substance in order to obtain a mixture.
  • the present invention relates to a device for mixing a first fluid substance and a second fluid substance through the use of selectively rotatable mixing elements.
  • a device for mixing a first fluid substance and a second fluid substance in order to obtain a mixture comprising a hollow vessel extending along a first axis and having a first extremity and a second extremity opposite to said first extremity along said first axis, said vessel having a loading opening located at said first extremity to allow entry of said first substance and/or said second substance into said vessel, and a discharge opening located at said second extremity to allow said mixture to exit from said vessel; said device further comprising mixing means located within said container and able to rotate selectively about said first axis to mix said first substance and said second substance and to move said first substance and/or said second substance and/or said mixture along said first axis towards said second extremity, said mixing means further comprising a first screw extending along said first axis.
  • said mixing means comprise a second separating device located between said first screw and said second extremity to separate off a first portion, in which said first screw is located, and a second portion in said vessel; said second separating device having second fluid-dynamic communication elements arranged to allow fluid to pass between said first portion and said second portion.
  • said mixing means comprise a first separating device located between said first extremity and said first screw conveyor to divide said first portion into a loading chamber, in which said loading opening is provided, and a first mixing chamber, in which said first screw conveyor is located; said first separating device having first fluid-dynamic communication elements arranged to allow fluid to pass between said loading chamber and said first chamber.
  • said mixing means comprise a second screw extending along said first axis, said second screw being located in said second portion.
  • said mixing means comprise a third separating device located between said second screw and said second extremity to divide said second portion into a second mixing chamber, in which said second screw is located, and a third portion; said third separating device having third fluid-dynamic communication elements arranged to allow fluid to pass between said second chamber and said third portion.
  • said mixing means comprise a third screw extending along said first axis, said third screw being located in said third portion.
  • said mixing means include a fourth separating device located between said third screw and said second extremity to divide said third portion into a third mixing chamber in which said third screw is located and a fourth portion; said fourth separating device having fourth fluid-dynamic communication elements arranged to allow fluid to pass between said third chamber and said fourth portion.
  • said mixing means comprise a fourth screw extending along said first axis, said fourth screw being located in said fourth portion.
  • said discharge opening is made in said fourth portion.
  • said mixing means comprise a regulating device arranged to regulate the amount of fluid capable of passing between said first portion and said second portion via said second fluid-dynamic communication elements.
  • said regulating device is selectively coupled to said second separating device.
  • said mixing means comprise a mixing device located in said loading chamber, said mixing device being arranged to impart a rotational movement to said first substance and/or said second substance present in said loading chamber.
  • said vessel is substantially cylindrical in shape and has an axis of symmetry coinciding with said first axis.
  • said device comprises drive means configured to drive said mixing means in rotation about said first axis.
  • said device comprises a loading conduit located outside said vessel and connected to said loading opening, said loading conduit being arranged to feed said first substance and/or said second substance to said loading opening.
  • said device comprises regulating means connected to said loading conduit, said regulating means being arranged to regulate the amount of said first substance and/or said second substance being fed to said loading opening.
  • fluid substance means any non-solid substance, that is one not having an intrinsic shape: this therefore includes liquids, gases, vapours, powders and emulsions, as well as any combination of one or more substances which, by their nature, take on the shape of the vessel containing them.
  • device 1 is particularly suitable for mixing liquids and/or emulsions: more particularly, the first substance may consist of an industrial sludge requiring purification treatment, while the second substance may consist of an emulsion of polyelectrolytes.
  • Device 1 comprises a hollow vessel 2, extending along a first axis A and having a substantially cylindrical shape: vessel 2 comprises a hollow cylindrical body 3 having an axis of symmetry coinciding with first axis A and is bounded along axis A by a first extremity 21 and a second opposite extremity 22, which are closed off by a first flange 4 and a second flange 5 respectively.
  • Body 3 has a loading opening 6 made in first extremity 21, that is close to first flange 4, and arranged to allow the first substance and the second substance to enter vessel 2; body 3 also has a discharge opening 7, made in second extremity 22, that is close to second flange 5, and arranged to allow the mixture to leave vessel 2, the mixture being obtained by mixing the first substance and the second substance within vessel 2.
  • Device 1 further comprises a loading conduit 8 located outside vessel 2 and connected to loading opening 6 to feed the first substance and the second substance to loading opening 6, and consequently to vessel 2; device 1 further comprises a discharge conduit 9 located outside vessel 2 and connected to discharge opening 7 to allow the mixture to be extracted from vessel 2 through discharge opening 7.
  • Device 1 further comprises a regulating device, which is known and not illustrated, connected to loading conduit 8 to regulate the quantities of the first substance and the second substance which travel through loading conduit 8 to be fed towards loading opening 6, thereby entering vessel 2.
  • Said regulating device comprises a volumetric flow meter for the first substance, which is connected to a special pump arranged to feed the first substance along loading conduit 8 towards the container 2 at a constant flow rate, and a dosing device arranged to introduce a quantity of the second substance determined according to the flow rate of the first substance detected by the flow meter into loading conduit 8, via an inlet opening 80.
  • Loading conduit 8 may further comprise a further connection to a source of a scrubbing fluid, which is known and not illustrated, arranged to selectively feed a specified amount of the scrubbing fluid into loading conduit 8 to clean loading conduit 8, vessel 2 and discharge conduit 9.
  • Vessel 2 is supported, with first axis A horizontal, by means of supporting means 10, which comprise a substantially rectangular base 11 provided with a plurality of supporting feet 110, 111, 112, 113, and a vertically positioned first bracket 12 and second bracket 13 connected to base 11 through their respective lower extremities, and connected to first flange 4 and second flange 5 respectively through their respective upper extremities.
  • supporting means 10 comprise a substantially rectangular base 11 provided with a plurality of supporting feet 110, 111, 112, 113, and a vertically positioned first bracket 12 and second bracket 13 connected to base 11 through their respective lower extremities, and connected to first flange 4 and second flange 5 respectively through their respective upper extremities.
  • device 1 comprises a cylindrical shaft 14 having a smaller diameter than the diameter of body 3 and a length greater than the length of vessel 2: said shaft 14 is located along first axis A, partly inside vessel 2, in such a way that its front end 140 projects from vessel 2 through a first support hole 40 provided centrally in first flange 4, and its rear end 141 projects from vessel 2 through a second support hole 50 provided centrally in second flange 5.
  • first support hole 40 and second support hole 50 respectively, there are first sealing elements 41 and second sealing elements 51 arranged to immobilise shaft 14 axially and radially, but to allow it to rotate about first axis A and at the same time prevent any leakage of the fluid substances present within vessel 2 through first support hole 40 and second support hole 50.
  • Rear end 141 of shaft 14 is connected to drive members 15, configured to selectively drive shaft 14 in rotation about first axis A: such drive members 15 may, for example, comprise a motor and gearbox, or any electromechanical, pneumatic, hydraulic, thermal, chemical or similar drive device.
  • Shaft 14 carries a first disc 31, a second disc 32, a third disc 33 and a fourth disc 34 coaxially keyed and spaced between first extremity 21 and second extremity 22 within vessel 2.
  • These discs 31, 32, 33, 34 have a diameter which is approximately smaller than the internal diameter of body 3 and, as described above, are able to rotate rigidly with shaft 14; furthermore, within vessel 2, disks 31, 32, 33, 34 demarcate a loading chamber 61 between first flange 4 and first disk 31, a first mixing chamber 62 between first disk 31 and second disk 32, a second mixing chamber 63 between second disk 32 and third disk 33, a third mixing chamber 64 between third disk 33 and fourth disk 34, and a discharge chamber 65 between fourth disk 34 and second flange 5.
  • Chambers 61, 62, 63, 64, 65 are demarcated by discs 31, 32, 33, 34 in such a way that fluid-tight access is gained to loading chamber 61 through loading opening 6, and in such a way that fluid-tight access to discharge chamber 65 is gained through discharge opening 7.
  • chambers 61, 62, 63, 64, 65 can be abstractly grouped into a plurality of portions of vessel 2.
  • loading chamber 61 and first chamber 62 form a first portion
  • second chamber 63, third chamber 64 and discharge chamber 65 form a second portion.
  • third chamber 64 and discharge chamber 65 in turn form a third portion, which thus consists of a subset of the second portion; finally, discharge chamber 65 alone coincides with a fourth portion, which thus consists of a subset of the third portion.
  • each disc 31, 32, 33, 34 respectively has fluid-dynamic communication elements 310, 320, 330, 340 arranged to allow fluid to pass between the two chambers that the relative discs 31, 32, 33, 34 separate: for example, first fluid-dynamic communication elements 310 are provided in first disc 31 and comprise a first service hole 311 and a second service hole 312 arranged symmetrically with respect to first axis A to allow fluid to pass between loading chamber 61 and first mixing chamber 62.
  • second fluid-dynamic communication elements 320 on second disc 32 comprise a third service hole 321 and a fourth service hole 322
  • third fluid-dynamic communication elements 330 on third disc 33 comprise a fifth service hole 331 and a sixth service hole 33
  • fourth fluid-dynamic communication elements 340 on fourth disc 34 comprise a seventh service hole 341 and an eighth service hole 342.
  • One or more adjustment rings 350 may be coupled to each disc 31, 32, 33, 34, arranged to adjust the amount of fluid capable of passing through the relevant fluid dynamic communication elements 310, 320, 330, 340, and thus the amount of fluid capable of passing from one chamber to the adjacent chamber: said adjustment rings 350 are selectively coupled to relative discs 31, 32, 33, 34 at service holes 311, 312, 321, 322, 331, 332, 341, 342 in such a way as to decrease the useful bore through which fluid is allowed to pass from one chamber to the adjacent one. Accordingly, by varying the inner diameter of said adjustment rings 350, it is possible to vary the pressure that the fluid can reach inside the respective chamber.
  • first disc 31 supports a mixing device 35 located in loading chamber 61 and able to rotate together with first disc 31 to impart a rotational movement to the fluid substances present in loading chamber 61: in particular, mixing device 35 comprises a first blade 351 and a second blade 352 integral with first disc 31, extending parallel to the direction of first axis A and symmetrical with respect to first axis A.
  • first disc 31 and second disc 32 support a first screw conveyor 36 extending along first axis A within first chamber 61, said first screw conveyor 36 being integral with first disc 31 and second disc 32; first screw conveyor 36 has an external diameter substantially equal to the diameter of discs 31, 32, 33, 34, and an internal diameter substantially equal to the diameter of shaft 14, to which first screw conveyor 36 can also be directly connected.
  • second disc 32 and third disc 33 support a second screw 37 in second chamber 63, while third disc 33 and fourth disc 34 support a third screw 38 in third chamber 64.
  • fourth disc 34 supports a fourth screw 39 in discharge chamber 65.
  • first substance and the second substance are fed into load chamber 61 by means of loading conduit 8 connected to loading opening 6.
  • shaft 14 starts to rotate about first axis A, causing all the elements integral with it, which as a whole are referred to as mixing means 30 and include discs 31, 32, 33, 34, mixing device 35, and screws 36, 37, 38, 39, to rotate about first axis A.
  • mixing means 30 include discs 31, 32, 33, 34, mixing device 35, and screws 36, 37, 38, 39, to rotate about first axis A.
  • the two substances introduced into loading chamber 61 are caused to rotate by first blade 351 and second blade 352: this first step has the sole purpose of imparting rotary motion to the substances, and therefore can be performed at low speed, avoiding the risk of breaking up the molecules of the polyelectrolytes with high intensity mechanical stress.
  • first screw 36 begins to mix the first substance and the second substance, and moves them towards second disc 32, against which they are pressed by the rotation of same first screw 36, thus favouring mixing.
  • second screw 37 further mixes the two substances in second chamber 63 and presses them against third disc 33, causing a portion of them to pass into third chamber 64 where third screw 38 further mixes the two substances and presses them against fourth disc 34, causing a portion of them to pass into discharge chamber 65.
  • fourth screw 39 completes mixing of the two substances, obtaining the desired mixture and moving it towards discharge opening 7 to leave vessel 2.
  • Mixing device 1 described above makes it possible to obtain homogeneous mixing of the first substance and the second substance by means of pressure applied to the two substances within chambers 61, 62, 63, 64, 65 through the rotation of screws 36, 37, 38, 39, and not through mechanical mixing: consequently shaft 14, and consequently also screws 36, 37, 38, 39, can rotate at a moderate speed which safeguards the full effectiveness of the polyelectrolytes.
  • the pressure within chambers 61, 62, 63, 64, 65 can be adjusted in advance, depending on the characteristics of the substances that are to be mixed, by means of regulating rings 350, which limit the ability of the substances to pass into the next chamber via fluid-dynamic communication elements 310, 320, 330, 340.
  • the number of chambers into which vessel 2 is divided may differ depending on the characteristics of the substances to be mixed.
  • the fourth portion of the vessel is in turn subdivided by a fifth disc into a fourth mixing chamber (in which a fifth screw is present) and a fifth portion (in which the discharge opening is located), which may in turn be subdivided into a fifth mixing chamber and a sixth portion by a sixth disc. It is evident that there is no limit to the number of mixing chambers that can be provided between the loading chamber and the discharge chamber, starting from a minimum of one mixing chamber.
  • the shaft supports a single disc integral with the shaft itself: this disc demarcates a loading and mixing chamber, between the first flange and the disc, and a discharge chamber, between the disc and the second flange, within the vessel.
  • a first screw is located in the loading and mixing chamber, which has the loading opening, while a second screw can be located in the discharge chamber, which has the discharge opening.
  • the first portion of the vessel coincides with the loading and mixing chamber, while the second portion coincides with the discharge chamber.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Electrical Discharge Machining, Electrochemical Machining, And Combined Machining (AREA)
EP22171403.3A 2021-05-04 2022-05-03 Mischgerät Pending EP4085994A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT102021000011336A IT202100011336A1 (it) 2021-05-04 2021-05-04 Dispositivo di mescolamento

Publications (1)

Publication Number Publication Date
EP4085994A1 true EP4085994A1 (de) 2022-11-09

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ID=77022007

Family Applications (1)

Application Number Title Priority Date Filing Date
EP22171403.3A Pending EP4085994A1 (de) 2021-05-04 2022-05-03 Mischgerät

Country Status (2)

Country Link
EP (1) EP4085994A1 (de)
IT (1) IT202100011336A1 (de)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0532903A1 (de) * 1991-08-16 1993-03-24 B.H. Kogyo Yugen Kaisha Kontinuierliches Knetapparat
EP0902057A2 (de) * 1997-09-11 1999-03-17 Dow Corning Toray Silicone Company, Ltd. Verfahren zur kontinuierlichen Herstellung einer Siliconkautschukzusammensetzung
WO2015074929A1 (de) * 2013-11-25 2015-05-28 Gneuss Gmbh Vorrichtung zur herstellung von polymeren
DE112016001990T5 (de) * 2015-04-28 2018-01-04 Toshiba Kikai Kabushiki Kaisha Extruderschnecke, Extruder und Extrusionsverfahren

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0532903A1 (de) * 1991-08-16 1993-03-24 B.H. Kogyo Yugen Kaisha Kontinuierliches Knetapparat
EP0902057A2 (de) * 1997-09-11 1999-03-17 Dow Corning Toray Silicone Company, Ltd. Verfahren zur kontinuierlichen Herstellung einer Siliconkautschukzusammensetzung
WO2015074929A1 (de) * 2013-11-25 2015-05-28 Gneuss Gmbh Vorrichtung zur herstellung von polymeren
DE112016001990T5 (de) * 2015-04-28 2018-01-04 Toshiba Kikai Kabushiki Kaisha Extruderschnecke, Extruder und Extrusionsverfahren

Also Published As

Publication number Publication date
IT202100011336A1 (it) 2022-11-04

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