EP3601624B1 - Abschnitt und verfahren zum kühlen einer kontinuierlichen leitung mit trockenkühlung und nasskühlung - Google Patents

Abschnitt und verfahren zum kühlen einer kontinuierlichen leitung mit trockenkühlung und nasskühlung Download PDF

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Publication number
EP3601624B1
EP3601624B1 EP18715225.1A EP18715225A EP3601624B1 EP 3601624 B1 EP3601624 B1 EP 3601624B1 EP 18715225 A EP18715225 A EP 18715225A EP 3601624 B1 EP3601624 B1 EP 3601624B1
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European Patent Office
Prior art keywords
zone
cooling zone
cooling
strip
wet
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EP18715225.1A
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English (en)
French (fr)
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EP3601624A1 (de
Inventor
Michel Clin
Florent CODE
Loïc PHILIPPE
Eric MAGADOUX
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Fives Stein SA
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Fives Stein SA
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/52—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for wires; for strips ; for rods of unlimited length
    • C21D9/54—Furnaces for treating strips or wire
    • C21D9/56—Continuous furnaces for strip or wire
    • C21D9/573—Continuous furnaces for strip or wire with cooling
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/56—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering characterised by the quenching agents
    • C21D1/60—Aqueous agents
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/56—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering characterised by the quenching agents
    • C21D1/613—Gases; Liquefied or solidified normally gaseous material
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D11/00—Process control or regulation for heat treatments
    • C21D11/005—Process control or regulation for heat treatments for cooling
    • C—CHEMISTRY; METALLURGY
    • C21—METALLURGY OF IRON
    • C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/52—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for wires; for strips ; for rods of unlimited length
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/003—Apparatus
    • C23C2/0035—Means for continuously moving substrate through, into or out of the bath
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/003—Apparatus
    • C23C2/0038—Apparatus characterised by the pre-treatment chambers located immediately upstream of the bath or occurring locally before the dipping process
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/02—Pretreatment of the material to be coated, e.g. for coating on selected surface areas
    • C23C2/022—Pretreatment of the material to be coated, e.g. for coating on selected surface areas by heating
    • C23C2/0224—Two or more thermal pretreatments
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/50—Controlling or regulating the coating processes
    • C23C2/52—Controlling or regulating the coating processes with means for measuring or sensing
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor
    • C23C2/34—Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor characterised by the shape of the material to be treated
    • C23C2/36—Elongated material
    • C23C2/40—Plates; Strips

Definitions

  • the cooling phase of the steel strips is particularly critical. Indeed, it is the cooling phase which mainly conditions the final mechanical and metallurgical properties of the steel strip. Depending on the cooling rate of the steel strip and its chemical composition, different metallurgical phases can be created and thus lead to different mechanical properties of the steel strip.
  • a cooling section of a continuous line for annealing or galvanizing steel strips arranged to receive a metal strip, said section comprising at least one cooling zone dry arranged to project a gas onto said steel strip and at least one wet cooling zone arranged to project a liquid or a mixture of gas and liquid onto said steel strip.
  • the dry cooling zone can comprise blowing boxes arranged to project the gas onto the steel strip.
  • the gas can be a mixture of nitrogen and hydrogen.
  • the wet cooling zone can comprise nozzles arranged to project the liquid or the mixture of gas and liquid onto the steel strip.
  • the liquid can be water, an acid solution, or any other solution.
  • the cooling section according to the invention can make it possible to produce steels with high mechanical properties which can directly undergo a galvanizing step at the outlet of said section, without requiring intermediate chemical treatment.
  • the wet cooling zone makes it possible to reach cooling speeds of the order of 1000°C/s for a steel strip 1 mm thick.
  • the cooling section according to the invention also makes it possible to successively perform dry cooling and wet cooling without having to cut the strip to bypass one of the cooling zones.
  • the gain in productivity is therefore substantial.
  • the wet cooling zone and the dry cooling zone are arranged, respectively, along a first vertical direction and a second vertical direction parallel to the first direction.
  • the wet cooling zone can be arranged upstream, according to the direction of travel of the steel strip in the cooling section, or downstream of the dry cooling zone.
  • the wet cooling zone and the dry cooling zone are arranged in the same vertical direction.
  • a person skilled in the art usually designates this variant by qualifying it as a one-pass embodiment.
  • the dry cooling zone can be arranged below the wet cooling zone.
  • a system for drying the steel strip can be interposed between the wet cooling zone and the dry cooling zone.
  • the atmosphere separation airlock comprises three pairs of rollers or flaps, each of the pairs being arranged transversely to a running direction of the metal strip, said three pairs of rollers or flaps delimiting between them two zones of said airlock, respectively a first zone delimited by the first two pairs of rollers or flaps in the running direction of the strip and located on the side of the dry cooling zone comprising withdrawal means, and respectively a second zone, delimited by the last two pairs of rollers or shutters in the running direction of the strip and located on the side of the wet cooling zone and comprising means arranged to inject an inert gas.
  • a buffer zone is thus created between the first two pairs of rollers and an atmosphere extraction system between the last two pairs of rollers.
  • this airlock advantageously creates a "clean" zone in which it is possible to measure the temperature of the strip over its width, for example by means of a scanner, or occasionally, by means of for example a pyrometer. This temperature measurement can help to better regulate the strip cooling process.
  • a method for cooling a continuous line for annealing or galvanizing steel strips arranged to receive a metal strip comprising at least one dry cooling zone arranged to spraying a gas onto said steel strip, said method comprising at least one dry cooling step comprising spraying a gas onto the steel strip and at least one wet cooling step comprising spraying a liquid or a mixture of gas and liquid on the steel strip.
  • a cooling section according to the first embodiment, of a continuous line for annealing or galvanizing metal strips arranged to receive a metal strip 1 in a running direction S, successively combining, in the direction of scrolling, at least one zone 2 of dry cooling and one zone 5 of wet cooling.
  • the cooling section further comprises an airlock 4 for separating atmospheres separating the zone 2 of dry cooling and the zone 5 of wet cooling.
  • the wet cooling zone 5 comprises means for withdrawal 7 of vapors which, in the example shown in the figure, are arranged in the upper part of this zone 5 of wet cooling.
  • the airlock 4 for separating atmospheres disposed between the dry zone 2 and the wet zone 5 comprises three successive pairs 8, 9 and 10 of rollers, according to the running direction S of the metal strip 1. Each of the pairs is placed transversely to the running direction of the metal strip.
  • Nitrogen is injected into zone 12 by means of a supply 14 constituting a means arranged to inject an inert gas.
  • a draw-off is carried out in zone 11 by a draw-off means 15.
  • the pressure and the inert gas injection rate in zone 12 and the draw-off flow rate in zone 11 are fixed so that the flow of gas between the zones 11 and 12 or only from zone 12 to zone 11. This prevents the entry of humid atmosphere coming from the humid zone 5 into zone 11 of the airlock and any mixing of the latter with the dry atmosphere of the airlock. area 2.
  • the return tank 18 includes a second set 19 of gas knives intended to remove the liquid which could still be present on the metal strip 1.
  • the system of drying and purging of the cooling zone of the second embodiment comprises points 28 for injecting an inert gas, for example nitrogen, and vents 29 allow rapid purging of the wet cooling zone 5 .
  • the inert gas supplying the knives 27 and the injection points 28 is heated beforehand, for example to a temperature of about 50°C.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heat Treatment Of Strip Materials And Filament Materials (AREA)
  • Blast Furnaces (AREA)
  • Coating With Molten Metal (AREA)

Claims (13)

  1. Kühlstrecke einer durchgehenden Ausglüh- oder Verzinkungslinie für Stahlbänder, die zum Aufnehmen eines Metallbands (1) angeordnet ist, die Strecke umfassend mindestens einen Trockenkühlbereich (2), der zum Ausstoßen eines Gases auf das Stahlband angeordnet ist, mindestens einen Nasskühlbereich (5), der zum Ausstoßen einer Flüssigkeit oder eines Gemisches aus Gas und Flüssigkeit auf das Stahlband angeordnet ist, und eine Atmosphärentrennungsschleuse (4), die zwischen dem Trockenkühlbereich und dem Nasskühlbereich eingesetzt ist,
    wobei die Atmosphärentrennungsschleuse drei Walzen- oder Klappenpaare (8, 9, 10) aufweist, wobei jedes der Paare quer zu einer Laufrichtung des Metallbandes eingerichtet ist, wobei die drei Walzen- oder Klappenpaare zwischen sich zwei Bereiche der Schleuse begrenzen, jeweils einen ersten Bereich (11), der durch die ersten zwei Walzen- oder Klappenpaare (8, 9) in der Laufrichtung des Bandes begrenzt ist und auf der Seite des Trockenkühlbereichs (2) gelegen ist und umfassend Entnahmemittel (15), und jeweils einen zweiten Bereich (12), der durch die letzten zwei Walzen- oder Klappenpaare (9, 10) in der Laufrichtung des Bandes begrenzt ist und auf der Seite des Nasskühlbereichs (5) gelegen ist und umfassend Mittel (14), die zum Eindrücken eines Inertgases angeordnet sind.
  2. Kühlstrecke nach dem vorstehenden Anspruch, wobei der Trockenkühlbereich und der Nasskühlbereich in einem vertikalen Durchgang eingerichtet sind, wobei der Nasskühlbereich unterhalb des Trockenkühlbereichs eingerichtet ist.
  3. Kühlstrecke nach einem der vorstehenden Ansprüche, ferner umfassend ein Trocknungs-und Abblassystem (24, 25, 26, 27, 28, 29) des Nasskühlbereichs.
  4. Kühlstrecke nach dem vorstehenden Anspruch, wobei das Trocknungs- und Abblassystem des Nasskühlbereichs eine Einrichtung (27, 28) umfasst, die zum Eindrücken von Stickstoff angeordnet ist.
  5. Kühlstrecke nach Anspruch 4, wobei das Trocknungs- und Abblassystem des Nasskühlbereich eine Einrichtung (25) umfasst, die zum Erwärmen von Wänden des Nasskühlbereichs angeordnet ist.
  6. Kühlstrecke nach Anspruch 4, wobei das Trocknungs- und Abblassystem des Nasskühlbereichs ein Stickstoffmessersystem umfasst, das in Richtung des unteren Teils des Nasskühlbereichs gerichtet ist und zum Blasen von Stickstoff auf Innenwände des Nasskühlbereichs angeordnet ist.
  7. Kühlstrecke einer durchgehenden Ausglüh- oder Verzinkungslinie für Stahlbänder, die zum Aufnehmen eines Metallbands (1) angeordnet ist, die Strecke umfassend mindestens einen Trockenkühlbereich (2), der zum Ausstoßen eines Gases auf das Stahlband angeordnet ist, wobei das Verfahrens mindestens einen Trockenkühlschritt, der ein Ausstoßen eines Gases auf das Stahlband aufweist, mindestens einen Nasskühlschritt, der ein Ausstoßen einer Flüssigkeit oder eines Gemisches aus Gas und Flüssigkeit auf das Stahlband aufweist, und eine Atmosphärentrennung mittels einer Atmosphärentrennungsschleuse (4) aufweist, die zwischen dem Trockenkühlbereich und dem Nasskühlbereich eingesetzt ist, die Kühlstrecke, wobei die Atmosphärentrennungsschleuse drei Walzen- oder Klappenpaare (8, 9, 10) aufweist, wobei jedes der Paare quer zu einer Laufrichtung des Metallbandes eingerichtet ist, wobei die drei Walzen- oder Klappenpaare zwischen sich zwei Bereiche der Schleuse begrenzen, einen Entnahmeschritt in einem ersten Bereich (11), der durch die ersten zwei Walzen- oder Klappenpaare (8, 9) in der Laufrichtung des Bandes begrenzt ist und auf der Seite des Trockenkühlbereichs (2) gelegen ist, und einen Eindrückschritt eines Inertgases in einem zweiten Bereich (12), der durch die letzten zwei Walzen- oder Klappenpaare (9, 10) in der Laufrichtung des Bandes begrenzt ist und auf der Seite des Nasskühlbereichs (5) gelegen ist.
  8. Verfahren nach dem vorstehenden Anspruch, dadurch gekennzeichnet, dass die Flüssigkeit für das Band nicht oxidierend ist.
  9. Verfahren nach dem vorstehenden Anspruch, dadurch gekennzeichnet, dass die Flüssigkeit eine Ameisensäurelösung ist, deren Säurekonzentration zwischen 0,1 Masse-% und 6 Masse-% der Lösung liegt.
  10. Verfahren nach Anspruch 9, dadurch gekennzeichnet, dass die Flüssigkeit eine Ameisensäurelösung ist, deren Säurekonzentration zwischen 0,5 Masse-% und 2 Masse-% der Lösung liegt.
  11. Verfahren nach einem der Ansprüche 7 bis 10, ferner umfassend einen Atmosphärentrennungsschritt mittels einer Atmosphärentrennungsschleuse, die zwischen dem Trockenkühlbereich und dem Nasskühlbereich eingesetzt ist, wobei der Atmosphärentrennungsschritt einen Eindrückschritt eines Inertgases in einem ersten Bereich der Schleuse und einen Entnahmeschritt in einem zweiten Bereich der Schleuse umfasst.
  12. Verfahren nach einem der Ansprüche 7 bis 11, ferner umfassend einen Trocknungs- und Abblasschritt des Nasskühlbereichs, insbesondere mittels Kalorien, die von einem Erwärmungsbereich der durchgehenden Linie stammen.
  13. Computerprogrammprodukt, das von einem Kommunikationsnetzwerk herunterladbar und/oder auf einem computerlesbaren Medium gespeichert und/oder durch einen Mikroprozessor ausführbar und in einen internen Speicher einer Recheneinheit ladbar ist, dadurch gekennzeichnet, dass es Programmcodeanweisungen aufweist, die, wenn sie durch die Recheneinheit ausgeführt werden, die Schritte des Verfahrens nach einem der Ansprüche 7 bis 12 umsetzen.
EP18715225.1A 2017-03-22 2018-03-22 Abschnitt und verfahren zum kühlen einer kontinuierlichen leitung mit trockenkühlung und nasskühlung Active EP3601624B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1752353A FR3064278B1 (fr) 2017-03-22 2017-03-22 Section et procede de refroidissement d'une ligne continue combinant un refroidissement sec et un refroidissement humide
PCT/FR2018/050706 WO2018172714A1 (fr) 2017-03-22 2018-03-22 Section et procédé de refroidissement d'une ligne continue combinant un refroidissement sec et un refroidissement humide.

Publications (2)

Publication Number Publication Date
EP3601624A1 EP3601624A1 (de) 2020-02-05
EP3601624B1 true EP3601624B1 (de) 2022-12-14

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Country Status (10)

Country Link
US (1) US11339455B2 (de)
EP (1) EP3601624B1 (de)
JP (1) JP7065870B2 (de)
KR (1) KR102497882B1 (de)
CN (1) CN110582586B (de)
ES (1) ES2939365T3 (de)
FI (1) FI3601624T3 (de)
FR (1) FR3064278B1 (de)
PL (1) PL3601624T3 (de)
WO (1) WO2018172714A1 (de)

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FR3064279B1 (fr) * 2017-03-22 2020-06-26 Fives Stein Procede et dispositif de refroidissement d'une bande d'acier en defilement dans une section de refroidissement d'une ligne continue
MX2023012230A (es) * 2021-05-06 2023-10-30 Jfe Steel Corp Metodo de control del punto de rocio para horno de recocido continuo, metodo de recocido continuo para laminas de acero, metodo de fabricacion de laminas de acero, horno de recocido continuo, linea de galvanizado continuo por inmersion en caliente y linea de galvanizado y recocido.

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Publication number Publication date
ES2939365T3 (es) 2023-04-21
FI3601624T3 (fi) 2023-02-28
FR3064278B1 (fr) 2021-04-23
FR3064278A1 (fr) 2018-09-28
CN110582586B (zh) 2023-01-17
KR102497882B1 (ko) 2023-02-10
JP2020520408A (ja) 2020-07-09
JP7065870B2 (ja) 2022-05-12
CN110582586A (zh) 2019-12-17
PL3601624T3 (pl) 2023-03-13
US11339455B2 (en) 2022-05-24
WO2018172714A1 (fr) 2018-09-27
EP3601624A1 (de) 2020-02-05
US20200095652A1 (en) 2020-03-26
KR20190130611A (ko) 2019-11-22

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