EP2547975A1 - Heisswindsteuerungsventil für eine metallurgische installation - Google Patents
Heisswindsteuerungsventil für eine metallurgische installationInfo
- Publication number
- EP2547975A1 EP2547975A1 EP11710152A EP11710152A EP2547975A1 EP 2547975 A1 EP2547975 A1 EP 2547975A1 EP 11710152 A EP11710152 A EP 11710152A EP 11710152 A EP11710152 A EP 11710152A EP 2547975 A1 EP2547975 A1 EP 2547975A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- hot blast
- valve member
- control valve
- blast control
- shaft
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000009434 installation Methods 0.000 title claims abstract description 7
- 230000008878 coupling Effects 0.000 claims description 19
- 238000010168 coupling process Methods 0.000 claims description 19
- 238000005859 coupling reaction Methods 0.000 claims description 19
- 239000002184 metal Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 5
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 229910010293 ceramic material Inorganic materials 0.000 claims description 3
- 230000002093 peripheral effect Effects 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 239000012809 cooling fluid Substances 0.000 claims description 2
- 239000011810 insulating material Substances 0.000 claims description 2
- 238000007789 sealing Methods 0.000 description 8
- 238000012423 maintenance Methods 0.000 description 4
- 239000000498 cooling water Substances 0.000 description 2
- 239000012774 insulation material Substances 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- 230000001010 compromised effect Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B7/00—Blast furnaces
- C21B7/16—Tuyéres
- C21B7/163—Blowpipe assembly
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21B—MANUFACTURE OF IRON OR STEEL
- C21B9/00—Stoves for heating the blast in blast furnaces
- C21B9/10—Other details, e.g. blast mains
- C21B9/12—Hot-blast valves or slides for blast furnaces
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27B—FURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
- F27B1/00—Shaft or like vertical or substantially vertical furnaces
- F27B1/10—Details, accessories, or equipment peculiar to furnaces of these types
- F27B1/16—Arrangements of tuyeres
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D3/00—Charging; Discharging; Manipulation of charge
- F27D3/16—Introducing a fluid jet or current into the charge
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D19/00—Arrangements of controlling devices
- F27D2019/0028—Regulation
- F27D2019/0034—Regulation through control of a heating quantity such as fuel, oxidant or intensity of current
Definitions
- the present invention generally relates to a hot blast control valve for a metallurgical installation, in particular for controlling the flow of hot blast of a blast furnace.
- hot air In blast furnaces, hot air, generally referred to as hot blast, is injected into the furnace for aiding the reduction of ore in the furnace.
- Air is heated to a temperature of up to 1250°C before it is fed as hot blast to the furnace.
- Reducing gas or hot air may be mixed into the hot blast to further aid the reduction of ore in the furnace.
- Any valve used to control the flow of hot blast is exposed to extreme conditions in that the temperature of the gas is very high and the gas may also be very aggressive.
- butterfly valves in the feeding conduits of the hot blast to control the flow of hot blast to the furnace.
- One such butterfly valve is known from JP 09095720 and comprises a disc-shaped control member mounted on a rotation axis centrally arranged in the path of the hot blast. In the closed position, the disc-shaped control member is perpendicular to the flow of hot blast and essentially blocks the path of the hot blast. The control member may then be rotated by 90° into its open position, wherein the control member is essentially parallel to the flow of hot blast, thereby allowing the hot blast to flow through the valve. In fact, the hot blast flows past the control member, on two sides thereof.
- a disadvantage of such a butterfly valve is that because the rotation axis is centrally arranged in the conduit, the control member is still in the path of the hot blast, even when the control member is in the fully open position. Indeed, even if the flow restriction of the control member is, in the open position, reduced to a minimum, the control member represents an obstruction to the free flow of hot blast through the valve.
- cooling channels are provided for cooling the disc-shaped control member. Such cooling is however often not sufficient to prevent damage to the control member. Consequently, the control member needs replacement after some time. Replacement of the control member is however particularly difficult because access to the control member is only possible once the control valve has been uninstalled and taken out of the conduit. Maintenance time and cost is therefore considerable.
- the present invention proposes a hot blast control valve for a metallurgical installation, in particular for controlling the flow of hot blast of a blast furnace.
- the hot blast control valve comprises a metallic valve housing with a refractory lining in which a gas channel is defined; and a valve member rotatably arranged in the gas channel so as to be able of varying a free passage in the gas channel by rotation of the valve member about a rotation axis between an open position and a closed position.
- the valve member has an envelope with rotational symmetry about the rotation axis and has a through passage arranged in the valve member in a direction transversely to the rotation axis of the valve member.
- the through passage has a cross-section substantially identical to that of the gas passage.
- the through passage is arranged in the valve member so as to be aligned with the gas channel when the valve member is in its open position.
- the valve member comprises a cylindrical body portion with a first base and an opposite second base; the first base being provided with connection means for connecting the valve member to a shaft; the cylindrical body portion having a diameter larger than the diameter of the gas channel.
- the valve member further comprises a hemispherical body portion with a base arranged on the second base of the cylindrical body portion.
- Such a hot blast control valve has the advantage that, when the control member is in its open position, the hot blast can freely flow through the through passage of the control member. Indeed, the control member does not constitute an obstacle to the flow of hot blast. Contrary to the butterfly-type control valve, which causes a pressure drop of up to 20% when it is in the open position, the pressure drop across an open control valve according to the present invention is negligent. Furthermore, in their closed position, butterfly-type control valves generally present considerable leakage (up to 40%). Due to the particular shape (cylindrical and hemispherical body portions) of the hot blast control valve according to the present invention, such leakage may be considerably reduced. An improved control of the flow of hot blast is therefore possible.
- the gas channel and the through passage have circular cross- section and the through passage has a diameter substantially corresponding to the diameter of the gas channel.
- the through passage has an axis perpendicular to the rotation axis of the valve member.
- the base of the hemispherical body portion has a diameter corresponding to the diameter of the second base of the cylindrical body portion.
- the base of the hemispherical body portion is advantageously arranged so as to lie on the axis of the gas channel.
- connection means preferably comprises a connection shoe on the first base of the cylindrical body portion, the connection shoe forming a circumferential groove with a coupling flange inside the groove, the coupling flange facing the first base of the cylindrical body portion.
- the coupling flange may be parallel to the first base of the cylindrical body portion.
- the coupling flange is at an angle tapering away from the first base towards the outer periphery of the first base.
- the shaft comprises a clamping means engaging the circumferential groove in the connection shoe, the clamping means being such that a contact surface of the clamping means is in tight contact with the coupling flange of the connection shoe in such a way that rotational movement of the clamping means of the shaft is transmitted to the valve member.
- a refractory insulation paper is arranged between the contact surface of the clamping means and the coupling flange of the connection shoe.
- the clamping means advantageously comprises at least two clamping elements engaging the circumferential groove, the clamping elements being connected to an enlarged head portion of the shaft.
- a fixation ring is preferably further provided for engaging the at least two clamping elements, thereby avoiding a movement of the clamping elements in a direction radially away from the connection shoe.
- the at least two clamping elements can be connected to the enlarged head portion by means of screws; the screws being preferably provided with spring means for pulling the clamping elements towards the enlarged head portion, the screws being preferably provided with a sleeve for limiting the travel of the screw.
- the shaft is advantageously provided with cooling channels for feeding cooling fluid to the enlarged head portion of the shaft.
- An intermediate plate may be arranged between the at least two clamping elements and the enlarged head portion of the shaft.
- Such an intermediate plate may be provided with an auxiliary shaft engaging in a matching recess arranged in the connection shoe of the valve member so as to create a form-fit connection.
- Such an arrangement may be useful for ensuring that the valve member is entrained by the form-fit connection provided by the auxiliary shaft in the unlikely event that the frictional connection between the contact surface and the coupling flange fails.
- the clamping elements and/or the fixation ring and/or the intermediate plate and/or the auxiliary shaft is preferably made from heat-resistant steel. Heat- insulating material may be arranged in gaps between various elements of the clamping means.
- the valve member is advantageously formed in one piece from refractory or ceramic material.
- the metal valve housing preferably comprises a lateral opening for operating the valve member via the shaft; the lateral opening having a diameter at least slightly bigger that the diameter of the cylindrical body portion of the valve member.
- a lateral opening allows for the valve member to be easily retracted from the valve housing for maintenance purposes. There is no need to remove the valve housing in order to access the valve member to be serviced.
- Any bearings for the shaft are preferably located outside the metal valve housing, thereby not subjecting the bearings to the extremely harsh conditions reigning in the metal valve housing.
- the bearings hence have prolonged lifetime.
- An annular groove may be arranged in a peripheral area of the first base of the valve member, an annular sheet engaging the annular groove to form a labyrinth seal.
- a labyrinth seal allows preventing large quantities of hot blast from entering the connection arrangement and travelling towards the main sealing arrangement. The lifetime of the main sealing arrangement may thereby be prolonged.
- Fig. 1 is a cut through a hot blast control valve according to the present invention
- Fig.2 is an enlarged view of the connection between valve member and shaft of Fig.1 ;
- Fig.3 is a perspective view of a valve member according to a preferred embodiment of Fig .1 .
- Fig .1 schematically shows a hot blast control valve for installation in a hot blast conduit.
- the hot blast control valve 10 comprises a metal valve housing 12 with an entry end 14 and an exit end 16, each of which comprises a connection flange 18 for connection to the conduit (not shown).
- the valve housing 12 comprises a refractory lining 20 in which a gas channel 22 is defined for feeding hot blast from the entry end 14 to the exit end 16.
- a valve member 24 is rotatably arranged in the gas channel 22 for varying the free passage therein by rotation of the valve member 24 about a rotation axis 26 between an open position and a closed position.
- the valve member 24 has an envelope with rotational symmetry about the rotation axis 26. The envelope of the valve member 24 will be more closely described later.
- the valve member 24 comprises a through passage 28 with a cross- section substantially identical to that of the gas passage 22.
- the through passage 28 is arranged such that, when the valve member 24 is in its open position as shown in Fig.1 , the through passage 28 is in alignment with the gas channel 22 and forms a continuation of the gas channel 22 such that the hot blast can freely flow from the entry end 14 to the exit end 16 of the hot blast control valve 10.
- the valve member 24 comprises a cylindrical body portion 30 with a first base 32 with a connection shoe 34 for connecting the valve member 24 to a shaft 36.
- the connection between shaft 36 and valve member 24 will be more closely described later when referring to Fig.2.
- the valve housing 12 is provided with a lateral opening 38 for allowing the shaft 36 from penetrating from outside the valve housing into the valve housing and connect to the valve member 24.
- the lateral opening 38 is dimensioned so as to allow for the valve member 24 to be retracted from the valve housing 12 through this lateral opening 38. The maintenance or replacement of the valve member 24 can thereby be performed easily and quickly. There is no need to disconnect the hot blast control valve 10 from the conduit at connection flanges 18 to access the valve member 24.
- the assembly comprising the valve member 24 and the shaft 36 is maintained in position by connecting a shaft support assembly 40 to a connection flange 42.
- the shaft support assembly 40 comprises, amongst others, the shaft bearings 44 and the main sealing arrangement 46 (preferably in the form of a packing box). It should be noted that these elements are all arranged outside the valve housing 12, i.e. away from the aggressive conditions reigning inside the valve housing 12.
- the valve member 24 comprises a connection shoe 34 forming a circumferential groove 50 with a slanted coupling flange 52 inside the groove 50.
- the shaft 36 comprises clamping means engaging the circumferential groove 50.
- the clamping means are formed by at least two clamping elements 54 with a nose 56 for engaging the circumferential groove 50.
- the nose 56 of the clamping elements 54 has a cross-section essentially corresponding to the cross-section of the groove 50 of the connection shoe 34.
- a contact surface 58 of the nose 56 is in tight contact with the coupling flange 52 of the connection shoe 34, such that rotational movement of the clamping elements 54, which are rotationally fixed to the shaft 36, is transferred via the contact surface 58 and coupling flange 52 to the valve member 24.
- a refractory insulation paper 60 may be sandwiched between the contact surface 58 and the coupling flange 52 to further improve the force transfer from the shaft 36 to the valve member 24.
- the at least two clamping elements 54 are prevented from moving radially outwards by means of a fixation ring 62 engaging a circumferential recess 64 arranged in the clamping elements 54.
- the clamping elements 54 are connected to an enlarged head portion 66 of the shaft 36 by means screws 68.
- the screws 68 pull the clamping elements 54 towards the enlarged head portion 66.
- the screws 68 also pull the contact surface 58 tightly against the coupling flange 52 so as to ensure good contact between the clamping elements 54 and the connection shoe 34 of the valve member 24.
- the enlarged head portion 66 may be formed in one piece with the shaft 36. Preferably, however, the enlarged head portion 66 is formed separately and fixed to the shaft 36 by welding.
- An intermediate plate 70 is furthermore arranged between the clamping elements 54 and the enlarged head portion 66.
- a form-fit connection between the intermediate plate 70 and the valve member 24 is provided by an auxiliary shaft, e.g. a polygon shaft 72 provided on the intermediate plate 70, in alignment with the rotation axis 26 of the shaft 36, and a corresponding polygon recess 74 in the connection shoe 34 of the valve member 24.
- auxiliary shaft e.g. a polygon shaft 72 provided on the intermediate plate 70, in alignment with the rotation axis 26 of the shaft 36, and a corresponding polygon recess 74 in the connection shoe 34 of the valve member 24.
- the screw 68 is preferably guided through a sleeve 76 contacting the clamping element 54 and thereby limiting the travel of the screw 68.
- the sleeve 76 prevents the screw 68 from being over-tightened and thereby potentially damaging the clamping element 54 or the connection shoe 34.
- the spring is preferably further provided with pretensioned spring means 78 between the intermediate plate 70 and the screw head 80.
- the spring means 78 which may be in the form of disc springs, ensures that the load on the contact zone (coupling flange 52 and contact surface) is limited to a predetermined tension. Indeed, due to temperature variations, the load on the contact zone may vary. Due to the spring means 78 and the sleeve 76, this load cannot exceed a predetermined threshold.
- Cooling water may be supplied to the enlarged head portion 66 of the shaft 36 through the shaft 36 itself. At the head of the shaft, the cooling water is radially spread and collected by any known means.
- a further important aspect of the present invention is the slow heat transfer from the valve member 24 to the shaft 36.
- the valve member 24 which is arranged in direct contact with the hot blast may easily reach temperatures in the region of 1200°C.
- the valve member 24 is preferably made from refractory or ceramic material.
- the various elements between the valve member 24 and the shaft 36, i.e. clamping elements 54, fixation ring 62, intermediate plate 70 and the polygon shaft 72 are made from heat-resistant steel, thereby reducing heat transfer to the shaft 36.
- gaps 82 are provided between the various elements and insulation material, such as e.g. insulation felt, is arranged in these gaps 82.
- the sealing of the hot blast control valve 10 is mainly performed by the main sealing arrangement 46 arranged outside the valve housing 12.
- An additional sealing may however be provided by an annular sheet 84 arranged parallel and coaxial to the rotation axis 26.
- the annular sheet 84 comprises a protrusion 86 engaging an annular groove 88 arranged in a peripheral part of the first base 32 of the valve member 24.
- the protrusion 86 engaging the annular groove 88 forms a labyrinth seal preventing large quantities of hot blast from entering the connection arrangement and travelling towards the main sealing arrangement 46.
- valve member 24 has an outer envelope formed by a cylindrical body portion 30, with a first base 32 and an opposite second base 90, and a hemispherical body portion 92 connected with its base to the second base 90 of the cylindrical body portion 30.
- the base of the hemispherical body portion 92 and the second base 90 have identical diameter.
- the first base 32 comprises the connection shoe 34 for connection with the shaft.
- the hemispherical body portion 92, the cylindrical body portion 30 and the connection shoe 34 are formed in one piece.
- the through passage 28 is arranged such that its central axis 94 lies in the plane comprising the second base 90.
- valve member 50 circumferential groove
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Lift Valve (AREA)
- Blast Furnaces (AREA)
- Sliding Valves (AREA)
- Taps Or Cocks (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
LU91665A LU91665B1 (en) | 2010-03-15 | 2010-03-15 | Hot blast control valve for a metallurgical installation |
PCT/EP2011/053698 WO2011113761A1 (en) | 2010-03-15 | 2011-03-11 | Hot blast control valve for a metallurgical installation |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2547975A1 true EP2547975A1 (de) | 2013-01-23 |
EP2547975B1 EP2547975B1 (de) | 2015-07-15 |
Family
ID=42830756
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP11710152.7A Active EP2547975B1 (de) | 2010-03-15 | 2011-03-11 | Heisswindsteuerungsventil für eine metallurgische installation |
Country Status (9)
Country | Link |
---|---|
EP (1) | EP2547975B1 (de) |
JP (1) | JP5669868B2 (de) |
KR (1) | KR101676680B1 (de) |
CN (1) | CN102803883B (de) |
BR (1) | BR112012023378B1 (de) |
LU (1) | LU91665B1 (de) |
RU (1) | RU2538848C2 (de) |
TW (1) | TWI493045B (de) |
WO (1) | WO2011113761A1 (de) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20220177783A1 (en) * | 2019-04-05 | 2022-06-09 | Unifrax I Llc | Exhaust gas control valve |
LU101340B1 (en) * | 2019-08-06 | 2021-02-09 | Wurth Paul Sa | Seal valve for a PCI system of a blast furnace |
CN111998089A (zh) * | 2020-08-20 | 2020-11-27 | 永嘉赛孚阀门有限公司 | 高温硬密封球阀 |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB311269A (en) * | 1928-05-08 | 1930-08-11 | Eduardo Hickman Y Emparan | Improvements in means for producing an intermittent supply of air to blast, smelting and like furnaces |
SU175067A1 (ru) * | 1963-10-19 | 1965-12-03 | Электростальский завод желого машиностроени | Клапан горячего дутья доменной печи |
JPS54125107A (en) * | 1978-03-24 | 1979-09-28 | Nippon Steel Corp | Tuyere branch pipe blast furnace |
LU85079A1 (fr) * | 1983-11-07 | 1985-07-17 | Wurth Paul Sa | Dispositif de reglage du debit de vent chaud dans un porte-vent de four a cuve et porte-vent equipe d'un tel dispositif |
JP2510172B2 (ja) * | 1986-12-09 | 1996-06-26 | アイシン・エィ・ダブリュ株式会社 | 自動変速機 |
JPH0688114A (ja) * | 1991-04-08 | 1994-03-29 | Nippon Steel Corp | 高炉送風量の制御弁 |
JPH0995720A (ja) | 1995-10-03 | 1997-04-08 | Azuma Tekko Kk | 熱風制御弁 |
JPH101705A (ja) * | 1996-06-11 | 1998-01-06 | Nippon Steel Corp | 高炉送風支管用風量制御弁 |
JP3233589B2 (ja) * | 1996-12-17 | 2001-11-26 | 東鉄工株式会社 | セラミックス弁装置 |
US5799928A (en) * | 1997-03-03 | 1998-09-01 | Conval Inc. | Ball valve with improved valve seat and bonnet assembly |
JP3116305B2 (ja) * | 1998-02-10 | 2000-12-11 | 日本鋼管株式会社 | 高温高圧流体の流量制御弁及びその弁軸の固着防止方法 |
EP1023982A1 (de) * | 1999-01-29 | 2000-08-02 | Novasfer S.r.l. | Verfahren zur Herstellung eines Ventilsteuerungselements und so hergestelltes Ventilsteuerungselement |
CN2525320Y (zh) * | 2002-02-04 | 2002-12-11 | 杜颐桂 | 小扭矩无泄漏可调式球阀 |
JP2006283913A (ja) * | 2005-04-01 | 2006-10-19 | Inter-Valve Technologies Corp | バルブ装置 |
CN2874152Y (zh) * | 2005-12-29 | 2007-02-28 | 邢佳静 | 新型焦炉煤气负压调节旋塞 |
RU2318023C1 (ru) * | 2006-04-26 | 2008-02-27 | Открытое акционерное общество "Электростальский завод тяжелого машиностроения" | Клапан горячего дутья доменных воздухонагревателей |
CN201198486Y (zh) * | 2007-11-29 | 2009-02-25 | 漯河市景恒冶金机械有限公司 | 新型节水热风阀 |
CN201334494Y (zh) * | 2008-12-09 | 2009-10-28 | 石家庄三环阀门股份有限公司 | 一种改进的热风阀密封结构 |
JP2012067814A (ja) * | 2010-09-22 | 2012-04-05 | Keihin Corp | 流路開閉弁 |
-
2010
- 2010-03-15 LU LU91665A patent/LU91665B1/en active
-
2011
- 2011-03-11 CN CN201180014375.8A patent/CN102803883B/zh active Active
- 2011-03-11 KR KR1020127025491A patent/KR101676680B1/ko active IP Right Grant
- 2011-03-11 JP JP2012557500A patent/JP5669868B2/ja active Active
- 2011-03-11 WO PCT/EP2011/053698 patent/WO2011113761A1/en active Application Filing
- 2011-03-11 BR BR112012023378-5A patent/BR112012023378B1/pt active IP Right Grant
- 2011-03-11 RU RU2012143688/02A patent/RU2538848C2/ru active
- 2011-03-11 EP EP11710152.7A patent/EP2547975B1/de active Active
- 2011-03-15 TW TW100108692A patent/TWI493045B/zh active
Non-Patent Citations (1)
Title |
---|
See references of WO2011113761A1 * |
Also Published As
Publication number | Publication date |
---|---|
LU91665B1 (en) | 2011-09-16 |
RU2538848C2 (ru) | 2015-01-10 |
WO2011113761A1 (en) | 2011-09-22 |
EP2547975B1 (de) | 2015-07-15 |
RU2012143688A (ru) | 2014-04-20 |
TW201144449A (en) | 2011-12-16 |
JP2013522467A (ja) | 2013-06-13 |
TWI493045B (zh) | 2015-07-21 |
CN102803883A (zh) | 2012-11-28 |
KR20130051436A (ko) | 2013-05-20 |
BR112012023378B1 (pt) | 2019-01-15 |
JP5669868B2 (ja) | 2015-02-18 |
CN102803883B (zh) | 2014-12-03 |
BR112012023378A2 (pt) | 2018-05-15 |
KR101676680B1 (ko) | 2016-11-16 |
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