EP2382064B1 - Press tooling - Google Patents
Press tooling Download PDFInfo
- Publication number
- EP2382064B1 EP2382064B1 EP10701002A EP10701002A EP2382064B1 EP 2382064 B1 EP2382064 B1 EP 2382064B1 EP 10701002 A EP10701002 A EP 10701002A EP 10701002 A EP10701002 A EP 10701002A EP 2382064 B1 EP2382064 B1 EP 2382064B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- armature
- tube
- insert
- housing
- recess
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Not-in-force
Links
- 238000003825 pressing Methods 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 description 12
- 239000011159 matrix material Substances 0.000 description 11
- 230000006835 compression Effects 0.000 description 7
- 238000007906 compression Methods 0.000 description 7
- 239000000843 powder Substances 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 4
- 230000007704 transition Effects 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 230000002238 attenuated effect Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 239000003879 lubricant additive Substances 0.000 description 1
- 239000003758 nuclear fuel Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B30—PRESSES
- B30B—PRESSES IN GENERAL
- B30B15/00—Details of, or accessories for, presses; Auxiliary measures in connection with pressing
- B30B15/02—Dies; Inserts therefor; Mounting thereof; Moulds
- B30B15/022—Moulds for compacting material in powder, granular of pasta form
- B30B15/024—Moulds for compacting material in powder, granular of pasta form using elastic mould parts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/02—Compacting only
- B22F3/03—Press-moulding apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B30—PRESSES
- B30B—PRESSES IN GENERAL
- B30B11/00—Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B30—PRESSES
- B30B—PRESSES IN GENERAL
- B30B11/00—Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses
- B30B11/02—Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses, tabletting presses using a ram exerting pressure on the material in a moulding space
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B30—PRESSES
- B30B—PRESSES IN GENERAL
- B30B15/00—Details of, or accessories for, presses; Auxiliary measures in connection with pressing
- B30B15/02—Dies; Inserts therefor; Mounting thereof; Moulds
Definitions
- the subject of the invention is a press tool according to the preamble of claim 1.
- the manufacture of mechanical parts by powder pressing to give a compact blank, followed by sintering may involve the use of uniaxial compression machines comprising a die consisting of a housing into which the powder is poured and a punch s engaging in the housing to effect compression of the powder or, alternatively, a pair of punches engaging two opposite ends of the housing in two opposite directions. These presses operate at relatively high rates.
- the applications are numerous: they may concern mechanical metal or ceramic parts such as gears, magnets, nuclear fuel pellets, etc.
- Still other methods include adding rubber or other flexible materials to the matrix that facilitate demolding and are then sacrificed, but this is also expensive.
- a variation of this design is to clamp the die by springs, external pressure, or any other means to reduce its diameter during pressing; it is exposed in the documents EP - A - 1,602,473 , US - A - 5,694,640 and in the article of Holownia "Balanced die method for metal powder compaction", published in Powder Metallurgy, vol.39, No. 3, Money Publishing .
- the clamping is stopped after pressing, which allows the die to expand to reduce the extraction friction of the formed part and thus facilitate demolding.
- the technical problem is somewhat different, and these methods do not contribute to improving the transition of the constraints at the exit of the matrix between the unmolded portion and the portion still retained in the matrix. It should also be noted that, in these examples, the centripetal pressure is applied only to the center of the matrix, while the edges are held rigidly in the apparatus and therefore have no flexibility.
- the invention has been designed to obviate these disadvantages and allow automatic compression and reliable parts at high rates while reducing the risk of damage to the mold and subsequent defects in shape and size.
- the invention thus relates to a press tool comprising a die, an armature external to the die, a flexible tube delimiting a central recess in which coin pressings are made, and an insert disposed between the flexible tube. and the frame and mobile under the action of a mechanism, characterized in that the insert slides on the tube and extends to an end of the tube through which the pressed pieces are extracted from the housing, and in that that the insert releases said end, which remains separated from the armature by a game, in another position.
- This arrangement has the effect of allowing the tube to flex by expanding near the release orifice, and thus partially yield to the internal compressive stresses of the part. These internal stresses partially relax before demolding, with a progression towards the demolding orifice, so that the transition between the demolded parts and the parts still present in the housing is greatly attenuated when the part is demolded, and the concentrations traditionally observed strain at the junction between these two states of the room are extremely reduced or even disappeared.
- the flexible tube is superior to the traditional chamfer or rounding at the top of the housing as it flexes according to the distribution of the internal stresses in the demolding direction and thus that it takes of itself a profile to greatly reduce the stress concentrations. And it gives a simpler design matrix than the segmented dies, and without the risk of a bad closure of the housing.
- the tube is joined to the frame by a flange at one end of the armature opposite to the extraction location, the frame includes a recess partially delimited by the collar, and the insert comprises a movable protrusion in the recess between stop states on opposite walls of the recess.
- the figure 1 represents a press comprising a control system 1, an upper punch 2, a lower punch 3 and a tool 4 specific to the invention which comprises a die 5.
- the upper punch 2 and the lower punch 3 comprise rods 6 and 7 directed towards each other.
- the matrix 5 comprises a housing 8 in the alignment of the rods 6 and 7, which can penetrate between the orifices 9 and 10 opposite.
- the lower piston 3 and its rod 7 comprise a needle 37 which slides therein, and the rod 6 of the upper piston 2 comprises a housing 11 in front of the needle 37, which can enter therein. This arrangement makes it possible to compress hollow pieces of annular shape.
- the invention is not limited to this situation and also relates to presses without a needle, possibly with a single punch; the dwelling would then be provided with a single orifice and would include a bottom on the other side.
- the control system 1 governs the movement of the punches 2 and 3 and the needle 37.
- the matrix 5 is composed of an armature 15 which is a main portion thereof, a flexible tube 16 surrounded by the frame 15 with a clearance and which delimits the housing 8, and an insert 17 of cylindrical shape and introduced between the two previous under a slippery fit.
- the tube 16 is joined to the armature 15 by a lower flange 18 (on the side of the lower punch 3), and which delimits a recess 19 with the armature 15.
- the insert 17 comprises a radial protrusion 20 present in the recess 19, in which it can move in the vertical direction to abut on opposite surfaces of the recess 19.
- a control mechanism 21 acts on the insert 17 allowing it to move vertically between the two stop positions mentioned above. It may be a rod penetrating into a passage 22 of the armature 15 and attached to the protrusion 20. The rod is controlled by a means such as a jack connected to the armature 15.
- the tube 16 An essential property of the tube 16 is that it must be flexible enough to be able to expand, this flexibility is dictated by its thickness. It must be thin, for example of thickness between 0.5 and 1 mm if it is constructed of tungsten carbide, which has good wear resistance.
- the insert 17 is normally thicker, but its dimensions are not critical, and it can consist of a steel tube 2 to 10 mm thick.
- the armature 15 may be in the form of a cylindrical sleeve 10 to 15 mm thick, still made of steel.
- the insert completely withdraws from contact with the tube so as to eliminate the friction forces during demolding. It is then necessary to develop a sliding zone large enough to disengage these two elements from one another.
Description
Le sujet de l'invention est un outillage de presse selon le préambule de la revendication 1.The subject of the invention is a press tool according to the preamble of
La fabrication des pièces mécaniques par un pressage de poudres pour donner une ébauche compacte, suivi d'un frittage, peut impliquer l'emploi de machines de compression uniaxiale comprenant une matrice constituée d'un logement dans lequel la poudre est versée et un poinçon s'engageant dans le logement pour réaliser la compression de la poudre ou, en variante, une paire de poinçons s'engageant par deux extrémités opposées du logement dans deux sens opposés. Ces presses fonctionnent à des cadences relativement élevées. Les applications sont nombreuses: elles peuvent concerner des pièces mécaniques en métal ou en céramique comme les engrenages, les aimants, les pastilles des combustibles nucléaires, etc.The manufacture of mechanical parts by powder pressing to give a compact blank, followed by sintering, may involve the use of uniaxial compression machines comprising a die consisting of a housing into which the powder is poured and a punch s engaging in the housing to effect compression of the powder or, alternatively, a pair of punches engaging two opposite ends of the housing in two opposite directions. These presses operate at relatively high rates. The applications are numerous: they may concern mechanical metal or ceramic parts such as gears, magnets, nuclear fuel pellets, etc.
Ce genre de procédé présente toutefois des inconvénients. L'un des plus importants apparaît au démoulage de la pièce comprimée en la sortant progressivement du logement par un mouvement axial de poussée du poinçon. La compression a produit des contraintes radiales dans la pièce, qui se libèrent à mesure qu'elle sort du logement en produisant une dilatation radiale. Les risques d'endommagement de la pièce par fissuration ou rupture sont fréquents à l'orifice du logement, entre les portions encore contraintes et les portions subitement relâchées, où des concentrations de contrainte apparaissent. Divers procédés ont été employés pour améliorer la qualité des pièces. On peut citer l'utilisation d'additifs lubrifiants ou liants dans les poudres ou le choix de séquences particulières de compression par les poinçons; mais les additifs nuisent au frittage puisqu'ils sont volatils et peuvent être polluants, et les seconds procédés ralentissent beaucoup les cadences de production. Ces deux groupes de procédés remédient d'ailleurs plutôt à d'autres défauts, comme une cohésion insuffisante de la matière après la compression.This kind of process, however, has disadvantages. One of the most important appears in the release of the compressed part gradually out of the housing by an axial movement of pushing the punch. The compression has produced radial stresses in the workpiece, which are released as it exits the housing producing radial expansion. The risks of damage to the part by cracking or rupture are frequent at the orifice of the housing, between the portions still constrained and the portions suddenly released, where stress concentrations appear. Various processes have been employed to improve the quality of the parts. Mention may be made of the use of lubricant additives or binders in powders or the choice of particular compression sequences by the punches; but the additives interfere with sintering since they are volatile and can be pollutants, and the second processes slow down the production rates considerably. These two groups of processes moreover remedy other defects, such as insufficient cohesion of the material after compression.
D'autres procédés consistent à pourvoir l'orifice du logement de la matrice d'un chanfrein ou d'un rayon de raccordement pour éviter à la pièce en cours de démoulage une transition brusque entre l'état contraint et l'état relâché, mais ce procédé est efficace seulement avec des profils d'orifice bien déterminés et particuliers à chaque variétés de pièces, de sorte qu'il est difficile à mettre en oeuvre.Other methods consist in providing the orifice of the housing of the matrix of a chamfer or a connecting radius to avoid the part being demolded an abrupt transition between the constrained state and the relaxed state, but this method is effective only with well defined orifice profiles and particular to each variety of parts, so that it is difficult to implement.
D'autres procédés encore consistent à ajouter dans la matrice des tubes de caoutchouc ou d'autres matières souples qui facilitent le démoulage et sont ensuite sacrifiés, mais cela est aussi coûteux.Still other methods include adding rubber or other flexible materials to the matrix that facilitate demolding and are then sacrificed, but this is also expensive.
Enfin, un autre genre de procédés, décrit par exemple dans le document
Une variante de cette conception consiste à serrer la matrice par des ressorts, une pression externe ou tout autre moyen pour réduire son diamètre pendant le pressage ; elle est exposée dans les documents
L'invention a été conçue pour obvier à ces inconvénients et permettre une compression automatique et fiable de pièces à cadence élevée tout en réduisant les risques de dommages au démoulage et les défauts ultérieurs de forme et de dimension.The invention has been designed to obviate these disadvantages and allow automatic compression and reliable parts at high rates while reducing the risk of damage to the mold and subsequent defects in shape and size.
Sous une forme générale, l'invention concerne ainsi un outillage de presse comprenant une matrice, une armature extérieure à la matrice, un tube flexible délimitant un logement central dans lequel des pressages de pièces sont effectués, et un insert, disposé entre le tube flexible et l'armature et mobile sous l'action d'un mécanisme, caractérisé en ce que l'insert glisse sur le tube et s'étend jusqu'à une extrémité du tube par laquelle les pièces pressées sont extraites du logement, et en ce que l'insert dégage ladite extrémité, qui reste separée de l'armature par un jeu, dans une autre position.In a general form, the invention thus relates to a press tool comprising a die, an armature external to the die, a flexible tube delimiting a central recess in which coin pressings are made, and an insert disposed between the flexible tube. and the frame and mobile under the action of a mechanism, characterized in that the insert slides on the tube and extends to an end of the tube through which the pressed pieces are extracted from the housing, and in that that the insert releases said end, which remains separated from the armature by a game, in another position.
Cette disposition a pour effet de permettre au tube de fléchir en se dilatant à proximité de l'orifice de démoulage, et de céder ainsi partiellement aux contraintes internes de compression de la pièce. Ces contraintes internes se relâchent partiellement avant le démoulage, avec une progression vers l'orifice de démoulage, de sorte que la transition entre les parties démoulées et les parties encore présentes dans le logement est beaucoup atténuée au démoulage de la pièce, et que les concentrations de contrainte traditionnellement observées à la jonction entre ces deux états de la pièce sont extrêmement réduites ou même ont disparu.This arrangement has the effect of allowing the tube to flex by expanding near the release orifice, and thus partially yield to the internal compressive stresses of the part. These internal stresses partially relax before demolding, with a progression towards the demolding orifice, so that the transition between the demolded parts and the parts still present in the housing is greatly attenuated when the part is demolded, and the concentrations traditionally observed strain at the junction between these two states of the room are extremely reduced or even disappeared.
Le tube flexible est supérieur au chanfrein ou à l'arrondi traditionnel au sommet du logement en tant qu'il fléchit en fonction de la répartition des contraintes internes dans la direction de démoulage et donc qu'il prend de lui-même un profil permettant de réduire fortement les concentrations de contrainte. Et il donne une matrice de conception plus simple que les matrices segmentées, et dépourvue du risque d'une mauvaise fermeture du logement.The flexible tube is superior to the traditional chamfer or rounding at the top of the housing as it flexes according to the distribution of the internal stresses in the demolding direction and thus that it takes of itself a profile to greatly reduce the stress concentrations. And it gives a simpler design matrix than the segmented dies, and without the risk of a bad closure of the housing.
Dans un mode préféré de réalisation de l'invention, le tube est uni à l'armature par une collerette à une extrémité de l'armature opposée à l'emplacement d'extraction, l'armature englobe un évidement délimité partiellement par la collerette, et l'insert comprend une excroissance mobile dans l'évidement entre des états de butée sur des parois opposées de l'évidement.In a preferred embodiment of the invention, the tube is joined to the frame by a flange at one end of the armature opposite to the extraction location, the frame includes a recess partially delimited by the collar, and the insert comprises a movable protrusion in the recess between stop states on opposite walls of the recess.
L'invention sera maintenant décrite en liaison aux figures suivantes:
- la
figure 1 illustre une presse munie d'un outillage, - la
figure 2 illustre le phénomène qu'on rencontre, - la
figure 3 illustre la matrice, - la
figure 4 illustre un autre état de la matrice, - et la
figure 5 illustre le démoulage.
- the
figure 1 illustrates a press equipped with tools, - the
figure 2 illustrates the phenomenon we encounter, - the
figure 3 illustrates the matrix, - the
figure 4 illustrates another state of the matrix, - and the
figure 5 illustrates the demolding.
La
Le problème affronté au cours du démoulage est illustré à la
On se reporte à la
Pendant la plus grande partie du processus de fabrication, l'état est celui de la
Une propriété essentielle du tube 16 est qu'il doit être suffisamment souple pour pouvoir se dilater, cette souplesse est dictée par son épaisseur. Il doit donc être fin, par exemple d'épaisseur comprise entre 0,5 et 1 mm s'il est construit en carbure de tungstène, qui présente une bonne résistance à l'usure. L'insert 17 est normalement plus épais, mais ses dimensions ne sont pas critiques, et il peut consister en un tube en acier de 2 à 10 mm d'épaisseur. Enfin, l'armature 15 peut être en forme de manchon cylindrique de 10 à 15 mm d'épaisseur, encore en acier.An essential property of the
Selon un développement de l'invention, dans le cadre de son fonctionnement, on peut prévoir que l'insert se retire totalement du contact avec le tube de manière à éliminer les forces de friction lors du démoulage. Il convient alors d'aménager une zone de glissement suffisamment importante pour dégager ces deux éléments l'un de l'autre.According to a development of the invention, in the context of its operation, it can be provided that the insert completely withdraws from contact with the tube so as to eliminate the friction forces during demolding. It is then necessary to develop a sliding zone large enough to disengage these two elements from one another.
Claims (2)
- A press tool including a die (5), an armature (15) external to the die, a flexible tube (16) forming a central housing (8) in which part pressings (12) are accomplished, and an insert (17), positioned between the flexible tube and the armature, and which is mobile when moved by a mechanism (21), characterised in that the insert slides over the tube and extends as far as one end of the tube, by which the pressed parts are extracted from the housing, and in that the insert releases the said end, which remains separated from the armature by a gap, in another position.
- A tool according to claim 1, characterised in that the tube is joined to the armature by a skirt (18) at one end of the armature opposite the extraction position, the armature encompasses a recess (19) partially formed by the skirt, and the insert (17) includes a moving protruberance (20) in the recess between stop states on facing walls of the recess.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0950407A FR2941636B1 (en) | 2009-01-23 | 2009-01-23 | PRESS TOOLS |
PCT/EP2010/050555 WO2010084110A1 (en) | 2009-01-23 | 2010-01-19 | Press tooling |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2382064A1 EP2382064A1 (en) | 2011-11-02 |
EP2382064B1 true EP2382064B1 (en) | 2012-11-07 |
Family
ID=40823500
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP10701002A Not-in-force EP2382064B1 (en) | 2009-01-23 | 2010-01-19 | Press tooling |
Country Status (7)
Country | Link |
---|---|
US (1) | US8647563B2 (en) |
EP (1) | EP2382064B1 (en) |
JP (1) | JP5627605B2 (en) |
KR (1) | KR101698077B1 (en) |
ES (1) | ES2399334T3 (en) |
FR (1) | FR2941636B1 (en) |
WO (1) | WO2010084110A1 (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102189706B (en) * | 2011-01-28 | 2014-10-08 | 南京理工大学 | High-pressure shearing deformation method and device for tubular materials |
KR101493974B1 (en) * | 2013-05-24 | 2015-02-17 | 한국전기연구원 | Production method of silicon-busbar |
CN106077634B (en) * | 2016-08-24 | 2018-06-12 | 广州晶体科技有限公司 | Beading cold stamping die and the beading production method using the cold stamping die |
CN106077633B (en) * | 2016-08-24 | 2018-06-12 | 广州晶体科技有限公司 | Beading cold stamping die and the beading production method using the cold stamping die |
CN111590069A (en) * | 2020-06-28 | 2020-08-28 | 南安市铭基金刚石工具有限公司 | Cold pressing equipment and cold pressing method of bead stringing machine |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2558823A (en) * | 1949-05-27 | 1951-07-03 | Henry L Crowley | Apparatus for molding articles |
US2942298A (en) * | 1954-12-28 | 1960-06-28 | Unexcelled Chemical Corp | Molding apparatus |
SU454133A1 (en) * | 1973-01-26 | 1974-12-25 | Предприятие П/Я В-8469 | Mold for isostatic pressing of products |
SU1303436A1 (en) * | 1985-03-04 | 1987-04-15 | Пермский политехнический институт | Press mould for compression moulding of powdery materials with friction coefficient |
SU1315135A1 (en) * | 1986-01-02 | 1987-06-07 | Всесоюзный научно-исследовательский и проектный институт тугоплавких металлов и твердых сплавов | Die-casting mould |
GB9318581D0 (en) * | 1993-09-08 | 1993-10-27 | Manganese Bronze Ltd | Method of and apparatus for producing a compression product |
US7128547B2 (en) | 2004-01-13 | 2006-10-31 | Chien-Min Sung | High pressure split die and associated methods |
DE102004026969A1 (en) * | 2004-06-02 | 2005-12-29 | Sms Meer Gmbh | Device for producing a molded part from powder |
ATE413256T1 (en) * | 2005-07-19 | 2008-11-15 | Abrasive Tech Inc | METHOD AND DEVICE FOR PRODUCING GRINDING TOOLS |
US7381046B2 (en) * | 2006-06-27 | 2008-06-03 | Fu Chin Kuo | Lipstick making device |
AT505947B1 (en) * | 2007-11-14 | 2016-04-15 | Miba Sinter Austria Gmbh | COMPRESSION TOOL |
-
2009
- 2009-01-23 FR FR0950407A patent/FR2941636B1/en not_active Expired - Fee Related
-
2010
- 2010-01-19 KR KR1020117015847A patent/KR101698077B1/en active IP Right Grant
- 2010-01-19 EP EP10701002A patent/EP2382064B1/en not_active Not-in-force
- 2010-01-19 JP JP2011546773A patent/JP5627605B2/en not_active Expired - Fee Related
- 2010-01-19 ES ES10701002T patent/ES2399334T3/en active Active
- 2010-01-19 WO PCT/EP2010/050555 patent/WO2010084110A1/en active Application Filing
- 2010-01-19 US US13/145,702 patent/US8647563B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
KR20110112814A (en) | 2011-10-13 |
JP5627605B2 (en) | 2014-11-19 |
FR2941636B1 (en) | 2012-12-07 |
KR101698077B1 (en) | 2017-01-19 |
US20110280982A1 (en) | 2011-11-17 |
US8647563B2 (en) | 2014-02-11 |
WO2010084110A1 (en) | 2010-07-29 |
FR2941636A1 (en) | 2010-08-06 |
JP2012515652A (en) | 2012-07-12 |
ES2399334T3 (en) | 2013-03-27 |
EP2382064A1 (en) | 2011-11-02 |
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