EP1948838A1 - Poudre polymetallique et piece frittee fabriquee a partir de cette poudre - Google Patents
Poudre polymetallique et piece frittee fabriquee a partir de cette poudreInfo
- Publication number
- EP1948838A1 EP1948838A1 EP06831061A EP06831061A EP1948838A1 EP 1948838 A1 EP1948838 A1 EP 1948838A1 EP 06831061 A EP06831061 A EP 06831061A EP 06831061 A EP06831061 A EP 06831061A EP 1948838 A1 EP1948838 A1 EP 1948838A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- powder
- polymetallic
- powders
- diamond
- metal powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 81
- 229910052751 metal Inorganic materials 0.000 title abstract description 12
- 239000002184 metal Substances 0.000 title abstract description 12
- 239000010432 diamond Substances 0.000 claims abstract description 38
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 35
- 239000010949 copper Substances 0.000 claims abstract description 31
- 229910003460 diamond Inorganic materials 0.000 claims abstract description 25
- 238000005520 cutting process Methods 0.000 claims abstract description 21
- 229910017052 cobalt Inorganic materials 0.000 claims abstract description 15
- 239000010941 cobalt Substances 0.000 claims abstract description 15
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 claims abstract description 15
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000001301 oxygen Substances 0.000 claims abstract description 11
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 11
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 9
- 239000012535 impurity Substances 0.000 claims abstract description 6
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000011733 molybdenum Substances 0.000 claims abstract description 5
- 229910052802 copper Inorganic materials 0.000 claims description 14
- 239000000654 additive Substances 0.000 claims description 13
- 230000000996 additive effect Effects 0.000 claims description 11
- 229910052742 iron Inorganic materials 0.000 claims description 9
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 7
- 230000006835 compression Effects 0.000 claims description 6
- 238000007906 compression Methods 0.000 claims description 6
- 229910000906 Bronze Inorganic materials 0.000 claims description 4
- 239000010974 bronze Substances 0.000 claims description 4
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 claims description 4
- 150000001247 metal acetylides Chemical class 0.000 claims description 3
- 238000005056 compaction Methods 0.000 abstract 1
- IYRDVAUFQZOLSB-UHFFFAOYSA-N copper iron Chemical compound [Fe].[Cu] IYRDVAUFQZOLSB-UHFFFAOYSA-N 0.000 abstract 1
- 239000011230 binding agent Substances 0.000 description 17
- 239000000203 mixture Substances 0.000 description 15
- 229910017061 Fe Co Inorganic materials 0.000 description 9
- 238000005245 sintering Methods 0.000 description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- 239000010426 asphalt Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 150000002739 metals Chemical class 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000004567 concrete Substances 0.000 description 3
- 238000005087 graphitization Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000523 sample Substances 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000007731 hot pressing Methods 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011150 reinforced concrete Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 230000035945 sensitivity Effects 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 239000011135 tin Substances 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 230000003313 weakening effect Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 description 1
- 239000011609 ammonium molybdate Substances 0.000 description 1
- 229940010552 ammonium molybdate Drugs 0.000 description 1
- 235000018660 ammonium molybdate Nutrition 0.000 description 1
- 230000002051 biphasic effect Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000005496 eutectics Effects 0.000 description 1
- 239000010438 granite Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 150000002751 molybdenum Chemical class 0.000 description 1
- 239000006259 organic additive Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000010587 phase diagram Methods 0.000 description 1
- 238000013001 point bending Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000013074 reference sample Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- -1 sandstone Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000005476 soldering Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000007847 structural defect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C33/00—Making ferrous alloys
- C22C33/02—Making ferrous alloys by powder metallurgy
- C22C33/0257—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements
- C22C33/0278—Making ferrous alloys by powder metallurgy characterised by the range of the alloying elements with at least one alloying element having a minimum content above 5%
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/0425—Copper-based alloys
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C26/00—Alloys containing diamond or cubic or wurtzitic boron nitride, fullerenes or carbon nanotubes
Definitions
- micron powders of cobalt, iron, nickel, copper, and atomized powders typically 5 to 100 ⁇ m
- These base binders can be additive micronic WC tungsten carbide, fused carbide (typically 50 to 500 microns), or micron tungsten to increase the wear resistance.
- Cold compression at 150 to 500 MPa.
- the pressure is adjusted to obtain a tablet whose holding raw is sufficient to allow its handling.
- the binder + diamond mixture is most often granulated using an organic additive.
- the size of the granules is typically 50 to 700 ⁇ m.
- Hot compression The purpose of this step is to crimp the diamond in a binder matrix whose relative density is greater than 95% of its theoretical density. For this, pressures of the order of 25 to 50 MPa, and temperatures of the order of 700 to 1100 0 C are used.
- the sintering stage at maximum temperature lasts 2 to 10 minutes.
- the temperature is chosen according to the nature of the binder, to optimize its properties of hardness, impact resistance, wear resistance, diamond retention. It must be minimized to avoid degrading diamonds by graphitization.
- the use of diamonds coated with titanium, chromium, silicon or nickel improves the resistance of diamonds to graphitization, and improves the chemical bond between diamond and metal binder.
- the softening additive may be selected from copper and bronze.
- the invention also relates to a sintered part by hot pressing of a polymetallic powder, characterized in that said polymetallic powder is a polymetallic powder of the above type.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Polishing Bodies And Polishing Tools (AREA)
- Processing Of Stones Or Stones Resemblance Materials (AREA)
- Powder Metallurgy (AREA)
Abstract
Description
Claims
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PL06831061T PL1948838T3 (pl) | 2005-11-09 | 2006-11-03 | Proszek wielometaliczny i element spiekany wykonany z zastosowaniem tego proszku |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0511420A FR2892957B1 (fr) | 2005-11-09 | 2005-11-09 | Poudre polymetallique et piece frittee fabriquee a partir de cette poudre |
PCT/FR2006/002458 WO2007057533A1 (fr) | 2005-11-09 | 2006-11-03 | Poudre polymetallique et piece frittee fabriquee a partir de cette poudre |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1948838A1 true EP1948838A1 (fr) | 2008-07-30 |
EP1948838B1 EP1948838B1 (fr) | 2018-12-05 |
Family
ID=36694252
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP06831061.4A Active EP1948838B1 (fr) | 2005-11-09 | 2006-11-03 | Poudre polymetallique et piece frittee fabriquee a partir de cette poudre |
Country Status (7)
Country | Link |
---|---|
US (1) | US7998230B2 (fr) |
EP (1) | EP1948838B1 (fr) |
JP (1) | JP2009515051A (fr) |
KR (1) | KR101363968B1 (fr) |
FR (1) | FR2892957B1 (fr) |
PL (1) | PL1948838T3 (fr) |
WO (1) | WO2007057533A1 (fr) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20110079901A (ko) | 2008-10-20 | 2011-07-11 | 하.체. 스타르크 게엠베하 | 텅스텐 카바이드를 주성분으로 하는 초경합금 제작용의 몰리브덴 함유 금속 분말 |
DE102008052559A1 (de) | 2008-10-21 | 2010-06-02 | H.C. Starck Gmbh | Metallpulver |
CN103038025B (zh) * | 2010-03-01 | 2014-10-15 | 俄罗斯联邦政府预算机构《联邦军事、特殊及双用途智力活动成果权利保护机构》 | 用于金刚石工具制造的铜基粘结剂 |
FR2979845B1 (fr) * | 2011-09-09 | 2015-02-13 | Saint Gobain | Meule de faconnage pour verre plat |
CN107598156A (zh) * | 2017-09-18 | 2018-01-19 | 江苏锋泰工具有限公司 | 金刚石烧结工具用胎体粉末 |
US20200216935A1 (en) * | 2019-01-04 | 2020-07-09 | Tenneco Inc. | Hard powder particles with improved compressibility and green strength |
CN111037754B (zh) * | 2019-12-31 | 2021-11-23 | 浙江省永康市金都工贸有限公司 | 一种用于切割石材的梯形刀头及其制备方法 |
CN112676562A (zh) * | 2020-12-17 | 2021-04-20 | 安徽奥微新材料有限公司 | 一种添加稀土的高性能金属预制粉制备方法 |
CN114274061A (zh) * | 2022-01-01 | 2022-04-05 | 苏州赛尔科技有限公司 | 一种铁基开槽金属切割刀及制备方法 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1998049361A1 (fr) * | 1997-04-29 | 1998-11-05 | N.V. Union Miniere S.A. | Poudre pre-alliee a base de cuivre, et utilisation de cette poudre dans la fabrication d'outils en diamant |
DE19822663A1 (de) * | 1998-05-20 | 1999-12-02 | Starck H C Gmbh Co Kg | Sinteraktive Metall- und Legierungspulver für pulvermetallurgische Anwendungen und Verfahren zu deren Herstellung und deren Verwendung |
FR2784690B1 (fr) * | 1998-10-16 | 2001-10-12 | Eurotungstene Poudres | Poudres metalliques microniques a base de tungstene et/ou de molybdene et de materiaux de transition 3d |
FR2784691B1 (fr) * | 1998-10-16 | 2000-12-29 | Eurotungstene Poudres | Poudre metallique prealliee micronique a base de metaux de transition 3d |
AU2003227056A1 (en) * | 2002-03-29 | 2003-10-13 | Umicore | Pre-alloyed bond powders |
-
2005
- 2005-11-09 FR FR0511420A patent/FR2892957B1/fr active Active
-
2006
- 2006-11-03 JP JP2008539467A patent/JP2009515051A/ja active Pending
- 2006-11-03 EP EP06831061.4A patent/EP1948838B1/fr active Active
- 2006-11-03 PL PL06831061T patent/PL1948838T3/pl unknown
- 2006-11-03 WO PCT/FR2006/002458 patent/WO2007057533A1/fr active Application Filing
- 2006-11-03 US US12/093,060 patent/US7998230B2/en active Active
- 2006-11-03 KR KR1020087013525A patent/KR101363968B1/ko active IP Right Grant
Non-Patent Citations (1)
Title |
---|
See references of WO2007057533A1 * |
Also Published As
Publication number | Publication date |
---|---|
FR2892957B1 (fr) | 2009-06-05 |
PL1948838T3 (pl) | 2019-06-28 |
EP1948838B1 (fr) | 2018-12-05 |
WO2007057533A1 (fr) | 2007-05-24 |
KR101363968B1 (ko) | 2014-02-18 |
JP2009515051A (ja) | 2009-04-09 |
US7998230B2 (en) | 2011-08-16 |
US20090188171A1 (en) | 2009-07-30 |
FR2892957A1 (fr) | 2007-05-11 |
KR20080077148A (ko) | 2008-08-21 |
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