EP1681365A1 - Acier de cementation pour des composants fortement chargés - Google Patents
Acier de cementation pour des composants fortement chargés Download PDFInfo
- Publication number
- EP1681365A1 EP1681365A1 EP06450006A EP06450006A EP1681365A1 EP 1681365 A1 EP1681365 A1 EP 1681365A1 EP 06450006 A EP06450006 A EP 06450006A EP 06450006 A EP06450006 A EP 06450006A EP 1681365 A1 EP1681365 A1 EP 1681365A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- weight
- ppm
- steel
- content
- gew
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910000831 Steel Inorganic materials 0.000 title claims abstract description 52
- 239000010959 steel Substances 0.000 title claims abstract description 52
- 239000000203 mixture Substances 0.000 claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 claims abstract description 13
- 239000000126 substance Substances 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 11
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 7
- 239000012535 impurity Substances 0.000 claims abstract description 7
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 5
- 238000002844 melting Methods 0.000 claims abstract description 4
- 230000008018 melting Effects 0.000 claims abstract description 4
- 229910052804 chromium Inorganic materials 0.000 claims abstract description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 40
- 238000010791 quenching Methods 0.000 claims description 25
- 230000000171 quenching effect Effects 0.000 claims description 23
- 229910052757 nitrogen Inorganic materials 0.000 claims description 20
- 239000007789 gas Substances 0.000 claims description 13
- 238000005255 carburizing Methods 0.000 claims description 9
- 239000002344 surface layer Substances 0.000 claims description 6
- 238000009792 diffusion process Methods 0.000 claims description 5
- 238000005496 tempering Methods 0.000 claims description 5
- 238000000641 cold extrusion Methods 0.000 claims description 4
- 238000005242 forging Methods 0.000 claims description 4
- 238000003754 machining Methods 0.000 claims description 3
- 238000001125 extrusion Methods 0.000 claims description 2
- 238000004898 kneading Methods 0.000 claims description 2
- 230000005540 biological transmission Effects 0.000 abstract description 14
- 229910052759 nickel Inorganic materials 0.000 abstract description 4
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052796 boron Inorganic materials 0.000 abstract description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 2
- -1 0.27-.035 Chemical compound 0.000 abstract 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 abstract 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 abstract 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- 239000011651 chromium Substances 0.000 abstract 1
- 230000001143 conditioned effect Effects 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 239000011572 manganese Substances 0.000 abstract 1
- 229910052698 phosphorus Inorganic materials 0.000 abstract 1
- 239000011574 phosphorus Substances 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 239000010936 titanium Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
- 235000019589 hardness Nutrition 0.000 description 18
- 239000000463 material Substances 0.000 description 11
- 238000005275 alloying Methods 0.000 description 8
- 238000012360 testing method Methods 0.000 description 7
- 229910045601 alloy Inorganic materials 0.000 description 5
- 239000000956 alloy Substances 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 230000003068 static effect Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 3
- 229910052750 molybdenum Inorganic materials 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000010687 lubricating oil Substances 0.000 description 2
- 229910000734 martensite Inorganic materials 0.000 description 2
- 238000001000 micrograph Methods 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- 229910052720 vanadium Inorganic materials 0.000 description 2
- 241001295925 Gegenes Species 0.000 description 1
- 229910000760 Hardened steel Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 229910001566 austenite Inorganic materials 0.000 description 1
- 229910001563 bainite Inorganic materials 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000009749 continuous casting Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 210000001061 forehead Anatomy 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 239000004848 polyfunctional curative Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D7/00—Modifying the physical properties of iron or steel by deformation
- C21D7/02—Modifying the physical properties of iron or steel by deformation by cold working
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/28—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for plain shafts
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/56—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering characterised by the quenching agents
- C21D1/613—Gases; Liquefied or solidified normally gaseous material
Definitions
- the invention relates to a steel for case-hardened heavy-duty machine parts and to a method for producing a heavy-duty machine part and a heavy-duty machine part.
- a transmission shaft of this kind is a central main component of a transmission, which is also exposed to extreme requirements. Such a shaft must absorb high shock-like moments, with a relatively small outer diameter. In addition, most are strong weakenings due to a notch effect, caused by oil longitudinal and transverse holes, grooves, etc., given.
- Such insert steels have a C content of between 0.10 and 0.20% by weight, in addition to other alloying elements provided for hardenability, such as Cr, Mn, Ni, Mo and V, in some cases in high alloy contents.
- the invention aims to avoid the above-mentioned disadvantages and difficulties and has set itself the task of creating a steel for case-hardened heavy-duty machine parts and a method for producing such heavy duty machine parts, which in addition to a high core strength even with larger wall thickness by case hardening to very high hardnesses in Surface area can be brought, and this at a negligible even for complicated machine parts delay.
- a good mechanical machinability by machining should be given.
- the steel itself should be inexpensive, by using inexpensive alloying elements and avoiding the very expensive alloying elements such as Mo, and also the contents of alloying elements should be as low as possible.
- the steel according to the invention thus has a significantly higher C content compared to classic case-hardening steels, namely more than 0.20% by weight, whereas it is between 0.10 and 0.20% by weight for classic case-hardened steels.
- This higher C content is usually realized only for tempered steels.
- this higher C content achieves higher core strengths during case hardening, and on the other hand, the transition to the case-hardened layer-a carburized surface layer has a C content of 0.8% by weight-is not so abrupt, but rather there is a rather smooth continuous strength transition between the rim and the core.
- the boron content is between 30 and 120 ppm, ideally between 35 and 60 ppm. Boron brings an extremely strong increase in hardenability and is available as an alloying element virtually "free of charge”.
- the steel expediently has a C content before case hardening of between 0.26 and 0.30% by weight, and an Mn content of between 1.5 and 2% by weight.
- the Si content is appropriate to limit to 0.15 to 0.25 wt.% (Also advantageous because of the lower edge oxidation for increased fatigue strength) ,
- the Si content may be up to 0.4 wt.%.
- the Cr content is preferably between 0.05 and 1.0 wt%, more preferably between 0.4 and 0.8 wt%, ideally at about 0.6 wt%. Cr increases hardenability, but is more expensive than Mn.
- the sulfur content is advantageously limited to between 0.02 and 0.4% by weight, resulting in better machinability by machining.
- This optimally balanced composition of the alloying elements has the surprising effect that the hardenability of the material is extremely high even under the mildest quenching conditions. Due to the novelty of this alloy, the hardenability is of course also in the latest regulations (SEP1664, June 2004, "Determination of formulas by multiple regression to calculate the hardenability in the stimulus quenching test from the chemical composition of steels" + supplementary sheet to the SEP1664) not calculable, but only to characterize by practical experiments.
- the case hardening is expediently carried out in a temperature range between 880 and 1050 ° C., preferably between 900 and 950 ° C. during carburization with subsequent diffusion between 840 and 880 ° C., preferably at about 860 ° C., where a C is suitably used during case hardening Level of 0.7 to 1.2 wt.%, Preferably from 1.0 to 1.1 wt.% When carburizing and from 0.7 to 0.8 wt.% Is set when diffusing.
- the curing is advantageously carried out starting from a temperature of about 850 to 910 ° C, preferably starting from about 860 ° C.
- Subsequent tempering takes place over a temperature range of max. 200 ° C, preferably to a temperature of about 160 ° C, wherein advantageously the quenching extremely mild, preferably with a gas pressure of about 2-3 bar nitrogen or air, is performed.
- Fig. 1 shows a transmission shaft in section, which was made of a steel according to the invention and case hardened.
- Fig. 2 gives the hardness values HRC of a case-hardened steel according to the invention in comparison with various other case-hardened steels according to the prior art, wherein the illustrated spreading widths of the hardness bands should be given special attention.
- Figures 3, 4 and 5 show further comparisons of the achievable hardness HRC between a steel according to the invention and various conventional steel grades.
- Figs. 6 to 8 illustrate micrographs of the surface area of a machine part.
- the transmission shaft 1 shown in Fig. 1 represents a machine part, which can be difficult to use hardened, especially since it has a very large length and highly divergent cross-sectional values. Such a part is prone to distortion and is difficult to straighten after case hardening.
- an internal toothing 2 and an external toothing 3 various snap grooves 4, and grooves and holes 6 for oil supply, resulting notch effects that result in the use of conventional steels only a low dynamic load capacity.
- a second gear shaft (shaft II) of the same chemical composition was made with a case hardening depth Eht620HV1 of about 0.7 mm, by carburizing at 900 ° C (due to the observance of the exact gear data), with carburization over 4.7 hours with a C level of 1.05%.
- the subsequent diffusion was carried out at 860 ° C over a period of one hour with a C level of 0.75%.
- Case hardening produced a very hard surface layer> 58 HRC for both gear shafts. Values ranged from 61 to 62 HRC. At the same time, a very high core strength of over 42 HRC was found, ranging from 46 to 48 HRC, despite a very mild high pressure gas quench with nitrogen quench media.
- the following table shows the hardness values of the two shafts reached at different points, with the cuts 1, 2 and 3 from FIG. 1 as well as the surface hardness test points being able to be seen.
- the surface hardness measuring points are noted with OH1, OH2 and OH3 in Fig. 1.
- test bodies for the Jominy forehead quenching test according to ISO642 were also produced.
- the steel according to the invention has a superiority after case hardening in comparison to previously used types of steel, above all at a greater distance from the end face.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Heat Treatment Of Articles (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT0001105U AT8065U1 (de) | 2005-01-14 | 2005-01-14 | Stahl für einsatzgehärtete hochbeanspruchbare maschinenteile |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1681365A1 true EP1681365A1 (fr) | 2006-07-19 |
EP1681365B1 EP1681365B1 (fr) | 2010-09-29 |
Family
ID=35406108
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP06450006A Not-in-force EP1681365B1 (fr) | 2005-01-14 | 2006-01-12 | Procédé de fabrication des composants fortement chargés |
Country Status (3)
Country | Link |
---|---|
EP (1) | EP1681365B1 (fr) |
AT (1) | AT8065U1 (fr) |
DE (1) | DE502006007937D1 (fr) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2293837A1 (es) * | 2006-07-31 | 2008-03-16 | Sidenor Industrial, S.L. | Proceso de fabricacion de un acero, y acero obtenido en este proceso. |
CN113981316A (zh) * | 2021-10-27 | 2022-01-28 | 温州天和汽车部件有限公司 | 一种高精度链轮冷挤压工艺 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20210371947A1 (en) * | 2017-11-15 | 2021-12-02 | Sidenor Investigacion Y Desarrollo, S.A. | Alloyed steel and quenched and tempered steel |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5178688A (en) * | 1991-11-30 | 1993-01-12 | Samsung Heavy Industries Co., Ltd. | Carburized boron steels for gears |
JPH0892690A (ja) * | 1994-09-27 | 1996-04-09 | Sumitomo Metal Ind Ltd | 耐疲労特性に優れた浸炭部品およびその製造方法 |
JPH08311607A (ja) * | 1995-05-16 | 1996-11-26 | Sumitomo Metal Ind Ltd | 歯元曲げ強度に優れた低歪浸炭歯車およびその製造方法 |
-
2005
- 2005-01-14 AT AT0001105U patent/AT8065U1/de not_active IP Right Cessation
-
2006
- 2006-01-12 DE DE502006007937T patent/DE502006007937D1/de active Active
- 2006-01-12 EP EP06450006A patent/EP1681365B1/fr not_active Not-in-force
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5178688A (en) * | 1991-11-30 | 1993-01-12 | Samsung Heavy Industries Co., Ltd. | Carburized boron steels for gears |
JPH0892690A (ja) * | 1994-09-27 | 1996-04-09 | Sumitomo Metal Ind Ltd | 耐疲労特性に優れた浸炭部品およびその製造方法 |
JPH08311607A (ja) * | 1995-05-16 | 1996-11-26 | Sumitomo Metal Ind Ltd | 歯元曲げ強度に優れた低歪浸炭歯車およびその製造方法 |
Non-Patent Citations (2)
Title |
---|
PATENT ABSTRACTS OF JAPAN vol. 1996, no. 08 30 August 1996 (1996-08-30) * |
PATENT ABSTRACTS OF JAPAN vol. 1997, no. 03 31 March 1997 (1997-03-31) * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2293837A1 (es) * | 2006-07-31 | 2008-03-16 | Sidenor Industrial, S.L. | Proceso de fabricacion de un acero, y acero obtenido en este proceso. |
CN113981316A (zh) * | 2021-10-27 | 2022-01-28 | 温州天和汽车部件有限公司 | 一种高精度链轮冷挤压工艺 |
CN113981316B (zh) * | 2021-10-27 | 2022-07-19 | 温州天和汽车部件有限公司 | 一种高精度链轮冷挤压工艺 |
Also Published As
Publication number | Publication date |
---|---|
DE502006007937D1 (de) | 2010-11-11 |
EP1681365B1 (fr) | 2010-09-29 |
AT8065U1 (de) | 2006-01-15 |
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