EP1673495A1 - Method and installation for producing a flat multifilament elastomer thread - Google Patents
Method and installation for producing a flat multifilament elastomer threadInfo
- Publication number
- EP1673495A1 EP1673495A1 EP04790409A EP04790409A EP1673495A1 EP 1673495 A1 EP1673495 A1 EP 1673495A1 EP 04790409 A EP04790409 A EP 04790409A EP 04790409 A EP04790409 A EP 04790409A EP 1673495 A1 EP1673495 A1 EP 1673495A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- wire
- shaping
- filaments
- multifilament
- flat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products
- D01F6/70—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyurethanes
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/06—Wet spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/253—Formation of filaments, threads, or the like with a non-circular cross section; Spinnerette packs therefor
Definitions
- the present invention relates to a new process for manufacturing a multifilament elastomeric wire with a flat cross section, as well as an installation for the manufacture of this wire.
- the elastomeric yarn of the invention is advantageously used, for example but not exclusively, in the field of manufacturing hygienic articles, and in particular diapers.
- PRIOR ART In the field of hygienic articles, and more particularly diapers, it is customary to incorporate elastic threads into the structure of the article.
- elastic bands are inserted on the one hand at the level of the belt and on the other hand at the level of each leg passage, in order to ensure a better sealing of the faecal barriers of the diaper.
- the expression “flat” wire or “flat” cross-section wire means a wire whose cross section has two main axes: a large axis subsequently designated width (L) (largest dimension of the section) and a small axis subsequently designated thickness (e) (smallest dimension of the section) which are substantially perpendicular.
- a wire has a flat section within the meaning of the invention, when the width (L) is at least five times greater than the thickness (e), and preferably at minus ten times greater than the thickness (e).
- the wires with a flat cross section there are in particular the wires having a cross section substantially in the shape of a rectangle, trapezium, ellipse, oval, etc.
- the intermediate multifilament yarn, before shaping, which is obtained at the end of the aforementioned first manufacturing step is produced according to a process usual known as dry spinning process.
- International patent application WO00 / 00681 describes a multifilament spandex yarn which is obtained by a wet spinning process.
- the filaments which are extruded in the coagulation bath are withdrawn from said bath by means of a first roller which is placed just above the coagulation bath (see in particular example 1), and are then washed in a single washing bath equipped with two drive rollers, being wound several times around these two drive rollers.
- the present invention aims to propose a new method for manufacturing an elastomeric wire with a flat section, which can be implemented on an industrial scale.
- the method of manufacturing a flat multifilament elastomeric thread, by wet spinning which is the subject of claim 1.
- the filaments are passed at the outlet of the extrusion dies, when they are still immersed in the coagulation bath, on a rotary shaping cylinder which has a channel on its periphery shaping, the filaments being positioned relative to each other in said shaping channel so as to form the required flat cross section.
- the shaping channel is essential because it makes it possible to guide and maintain the filaments laterally during the shaping of the flat multifilament thread in the coagulation bath.
- a multifilament yarn is obtained which has a more uniform thickness over its entire section, and the width of which is controlled and reproducible.
- the implementation of several shaping channels on the cylinder makes it possible to envisage the parallel production of a plurality of wires (one wire per shaping channel).
- the flattening of the multifilament yarn is carried out from the spinning stage, and while the filaments do not have not been dimensionally stabilized by the traditional heating operations (drying and cooking) of the spinning process.
- the method of the invention advantageously comprises the additional technical characteristics of claims 2 to 11 taken individually or in combination with each other.
- the subject of the invention is also a wet spinning installation for implementing the method of the invention, and according to any one of claims 12 to 20, as well as a multifilament elastomeric wire having a flat cross section. , obtained by wet spinning according to the method of the invention (claim 21).
- the yarn of the invention advantageously comprises the additional technical characteristics of claims 22 to 25 taken individually or in combination with each other.
- FIG. 1 schematically shows a first alternative embodiment of an installation for the production of multifilament yarns of the invention
- - - the Figure 2 is a sectional view of the shaping cylinder and the accompanying roller associated with it
- - Figure 3 is a top view of the comb of the installation of Figure 1 positioned upstream of the shaping cylinder in shape
- - Figure 4 is a photograph (taken using an optical microscope) of the section of a wire (referenced A) of the invention having a titration of 1350 dtex
- FIG. 1 schematically shows a first alternative embodiment of an installation for the production of multifilament yarns of the invention
- - Figure 2 is a sectional view of the shaping cylinder and the accompanying roller associated with it
- - Figure 3 is a top view of the comb of the installation of Figure 1 positioned upstream of the shaping cylinder in shape
- - Figure 4 is a photograph (taken using an optical microscope) of the section of a wire (referenced A) of the invention
- FIG. 5 is a photograph (taken by means of an optical microscope) of the section of a wire (referenced B) of the invention having a titration of 1450 dtex.
- - Figure 6 is a sectional view of a shaping cylinder to illustrate another shaping groove profile
- - Figure 7 shows schematically a second alternative embodiment of an installation for the production of multifilament yarns of the invention.
- FIG. 1 shows an installation which conforms to a first variant embodiment of the invention, and which allows the spinning in the wet of multifilament yarns of synthetic elastomer and comprising a flat cross section.
- This installation comprises the usual technical means which are found in the known installations and methods for wet spinning of multifilamentary round section yarns, namely: - a reservoir 1, containing an appropriate quantity, in the form of a viscous solution, of an extrudable elastomeric polymer (P) and capable of being spun in the wet; this reservoir is replenished (supply conduit 2) with said polymer P, by a production unit (not shown) of this polymer P; - a main pump 3 having the function of feeding a set 4 of metering pump 4a with the polymer P contained in the reservoir 1.
- an extrusion / coagulation unit T1 allowing the continuous manufacture of a multifilament yarn (F ) - a plurality of successive washing units T2, ... Tn having the function of washing the multifilament yarn (F)
- a finishing unit 8 commonly designated “WEF” (“Wet End Finish”) having the function of '' apply to the wire F a liquid solution S allowing to lubricate the wire and make it anti-static
- a drying unit 9 for example of the type comprising an oven equipped with drums 9a with heating by steam and electricity on both last drums, - at least one drawing unit 10 followed by a cooking unit 11 (generally several successive drawing / cooking units are used), - a unit 12 for winding the multifilament yarn, for example on spools.
- the polymers preferred for the manufacture of a multifilament yarn of the invention are polyurethanes. More particularly, but not exclusively, among the known polyurethanes, use is preferably made of those which are prepared from aromatic diisocyanate, for example 4,4'-diphenylmethanediisocyanate (MDl), from a linear polyether, for example polytetramethylene ether glycol (PTG), and an alcohol type 1,4 butadienol (1,4 butylene glycol) commonly designated "40H".
- aromatic diisocyanate for example 4,4'-diphenylmethanediisocyanate (MDl)
- MDl 4,4'-diphenylmethanediisocyanate
- PEG polytetramethylene ether glycol
- 40H alcohol type 1,4 butadienol
- the extrusion / coagulation unit T1 comprises: a set 5 of extrusion dies 5a (“spinnerets”) which are immersed in a coagulation bath 6, and which are fed continuously and in parallel with the required quantity of solution of polymer P by the metering pumps 4a, - a cylinder 7 for shaping the wire, having the function, on the one hand, of bringing together and shaping, in the form of at least one flat multifilament wire (F), the filaments (f) which are extruded in parallel in the coagulation bath 6 at the outlet of the dies 5a, and on the other hand to bring out the multifilament yarn (F) from the coagulation bath 6.
- spinnerets extrusion dies 5a
- the coagulation bath 6 comprises so usual distilled water for example at a temperature of 60 ° C to 80 ° C mixed with a solvent such as DMF in an appropriate amount (for example with a concentration of 20%) in order to allow a complete extraction of the solvent ( DMF).
- Each washing unit T2 to Tn has an open tank containing a washing bath formed by distilled water, for example at a temperature of 40 ° C to 80 ° C, and are equipped with two motorized rollers R1 and R2 which are partially immersed in the washing bath and which make it possible to run the multifilament yarn (F) at a predetermined speed in the washing bath.
- the wire shaping cylinder 7 is a motorized cylinder, for example made of stainless steel, comprising at least one peripheral groove 7a (one groove per wire) in which the filaments (f) from the extrusion dies 5a are joined.
- This groove 7a forms a channel of shaping which extends over the entire periphery of the cylinder 7.
- this shaping channel has two opposite side walls 7b which are preferably divergent, so as to form a funnel facilitating the placement of the filaments in the shaping channel and the exit of the flat wire (F) from this shaping channel.
- the shaping channel has in section a trapezoidal profile.
- the dimension (a) represents the largest dimension base of the trapezoid, and corresponds to the width of the open face of the groove at the level of the surface of the shaping cylinder 7; the dimensions (b) represent the base of smaller dimension of the trapezoid, and corresponds to the width of the bottom of the groove 7a; The dimension (c) corresponds to the depth of the groove 7a.
- FIG. 6 illustrates by way of example another variant profile for the shaping channel 7a.
- the lateral walls 7b of the shaping channel 7a make it possible to guide and laterally maintain the filaments constituting the thread F, and thus to obtain at the outlet of the shaping cylinder 7 a multifilament thread (F) whose width is calibrated by reproducibly, and which is more homogeneous in thickness, compared for example to the use of a smooth cylinder.
- a shaping cylinder has a plurality of parallel shaping channels 7a, allowing the manufacture in parallel and simultaneously of several flat multifilament son (F).
- each shaping channel 7a is produced in the form of a peripheral groove hollowed out by machining in the surface of the cylinder.
- the shaping cylinder 7 comprises at least two elements: a smooth base cylinder ( 1st element) covered with a cylindrical sheath ( 2nd element) which has been threaded and fixed on the base cylinder and which comprises the peripheral groove (s) 7a or equivalent.
- the filaments (f) in the form of a bundle of filaments
- the filaments (f) are brought from below into the groove 7a of the shaping cylinder 7 while still being immersed in the coagulation bath 6, and are positioned side by side in the groove 7a of the cylinder 7 and held laterally by the walls of the groove 7a so as to form the multifilament yarn (F).
- the flat multifilament yarn (F) thus formed in the groove 7a is then taken out of the coagulation bath 6 by the shaping cylinder 7.
- a rotary accompanying member in the form of a roller 7 'mounted free in rotation, of smaller diameter than the shaping cylinder 7, and which mainly fulfills the function following: the accompanying roller 7 'makes it possible to give, at the outlet of the shaping cylinder 7, a first tension to the multifilament thread (F) so that the multifilament thread (F) is applied against the surface of this cylinder which helps to maintain the flat shape in section of this wire.
- the filaments of the multifilament yarn (F) are not compressed between the shaping cylinder 7 and the accompanying roller 7 '.
- the accompanying roller 7 ′ has an elastomer type surface, and for example consists of a stainless steel cylinder coated on its periphery with a rubber surface coating.
- upstream of the shaping cylinder 7 are additionally and optionally provided: - a comb 12 comprising two offset rows (FIG.
- each bundle of filaments (f) intended to form a multifilamentary thread - between the extrusion dies 5a and the comb 12, two rods 13a and 13b which are preferably fixed.
- the filaments (f) from the extrusion dies 5a are, at the outlet of the dies, gathered in the form of a bundle of filaments (a bundle of filaments (f) being intended to subsequently form a multifilament yarn).
- Each bundle of filaments (f) passes between the two rods 13a and 13b along a substantially flat S-shaped path.
- each bundle of filaments (f) is guided by the comb 12 in the direction of a groove 7a of the shaping cylinder 7, passing between two teeth of each row 12a, 12b of the comb 12.
- the distance (d) between the two rows 12a, 12b of teeth of the comb 12 was 17mm
- the spacing (p) between two teeth 12c of each row was 14mm.
- this tensioning means 14 is composed of three rods 14a, 14b, and 14c of small diameter, which are preferably fixed. If necessary, in another variant, these rods could be rotatable.
- the three rods 14a, 14b, 14c are positioned and spaced from one another so that the multifilament yarn (F) is deflected along a segmented path between the shaping cylinder 7 and the first transfer roller RT1, which allows to apply on the wire (F), in its portion ascending, a tension allowing the wire to keep its flattened shape in cross section.
- the rods 14a to 14b could be replaced by any equivalent means allowing a tensioning of the wire.
- the rods 14a to 14c could for example be replaced by a fixed guide profile in the form of a C, L or equivalent.
- a rotary tensioning means 14 similar to the means 14 previously described is also mounted on the ascending portion of the multifilament yarn (F) between the cylinder R2 of the first washing unit T2 and the transfer roller RT2 between said unit T2 and the following washing unit T3.
- a rotary pressing member 15 On the periphery of the first transfer roller RT1 between the extrusion / coagulation unit and the first washing unit T2 is also mounted a rotary pressing member 15, in the form of a pressing roller 15 of small diameter, and mounted free to rotate.
- a stainless steel roller coated with a rubber coating is used.
- This pressure roller 15 in combination with the transfer roller RT1 makes it possible to apply sufficient pressure to the wire (F) which at a minimum allows the wire to maintain its flat section when the direction of the wire changes (from its ascending portion to its descending portion), or even to obtain a better flattening of the wire.
- a single pressure roller 15 one could use several (at least two) pressure rollers judiciously arranged on the periphery of the first transfer roller RT1.
- upstream of the finishing unit 8 (WEF) are mounted two fixed rods 13'a and 13'b similar to the rods 13a and 13b and making it possible to improve the flattening of the multifilament yarn before the drying operations and cooking.
- Multifilament Yarns of the Invention two types of polyurethane multifilament yarns, referenced below A and B, were produced by means of the installation of the Figure 1 previously described. In both cases, these were yarns composed of polyurethane filaments obtained from MDl, PTG and 40H.
- the operating parameters (temperatures, rate of stretching) of the units 9, 10 and 11 respectively of drying, stretching and cooking are not indicated, because these parameters are fixed in the usual way and known by the skilled in the art, and moreover these parameters are identical for the two types of yarn A and B. It should also be pointed out that heating the multifilament yarn in the drying 9 and cooking 10 units also makes it possible, but not only, to fix the wire.
- the parameters (17) and (18) are average values measured on a plurality of samples.
- Parameter (18) [average thickness (e)] was also calculated on the basis of several samples, and is an approximate value given as an indication in order to compare the order of magnitude of the thickness with the width in section of the wire, it being specified that the thickness of the wire varies more or less over the section as a function of the more or less homogeneous distribution of the filaments (f) over the width of the wire.
- the thickness values (e1; e2; e3) were equal to (89.64 ⁇ m; 67.33 ⁇ m; 77.51 ⁇ r ⁇ ).
- This stretching contributes to the maintenance of the flattened section of the mutifilamentary wire.
- this stretching ratio is more generally greater than or equal to 1/1, 2.
- the invention is however not limited to this particular limit value of 1 / 1.2. In other embodiments covered by the invention, the stretching ratio could be lower than this ratio by 1 / 1.2. Subsequently, the thread does not undergo stretching when it passes through the following washing units (T3 to Tn ).
- FIG. 7 shows a second alternative embodiment of an installation for the production of multifilament yarns of the invention.
- the same references have been kept for the elements which are common to the two installations in FIGS. 1 and 7.
- the main differences between the two installations in FIGS. 1 and 7 will now be detailed.
- FIG. 7 In the coagulation bath 6, the installation of FIG. 7 comprises three successive combs 12, and a single rod 13 (instead of the two rods 13a and 13b in FIG. 1) for the pre-flattening of the filaments in the bath of coagulation, upstream of the shaping cylinder 7. Between the shaping cylinder (7) and the first transfer roller
- FIG. 7 no longer includes an accompanying roller 7 '.
- the flat multifilament yarn (F) is tensioned so as to maintain its flat cross section by means of four rods 14a, 14b, 14, 14d (instead of three rods in FIG. 1).
- the pressure roller 15 of Figure 1 has been omitted.
- the multifilament yarn (F) is kept in tension in its vertical paths (ascending and descending) between each transfer roller (RT1, RT2, RT3, ...) and the rollers R1 or R2 of each washing unit, by being deflected by means of four rods 14a to 14d (tensioning means 14 ').
- the finishing unit 8 "WEF” has been modified so as to apply to both sides of the wire F a liquid solution S making it possible to lubricate the wire and make it anti-static (use of two application devices 8a and 8b, of the “kiss roll” type on either side of the multifilament yarn). Drying (9) -Doy stretching-Cooking (11) -Winding (12)
- FIG. 7 After the finishing unit 8, the installation of FIG. 7 is identical to the installation of FIG. 1. For the sake of simplification, in FIG. 7, the stretching units 10, cooking 11, and winding 12, were not represented.
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Artificial Filaments (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0312021A FR2861091B1 (en) | 2003-10-15 | 2003-10-15 | FLAT MULTIFILAMENTAL ELASTOMERIC WIRE, METHOD AND INSTALLATION FOR THE PRODUCTION THEREOF |
PCT/EP2004/011553 WO2005035842A1 (en) | 2003-10-15 | 2004-10-14 | Method and installation for producing a flat multifilament elastomer thread |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1673495A1 true EP1673495A1 (en) | 2006-06-28 |
EP1673495B1 EP1673495B1 (en) | 2009-12-09 |
Family
ID=34385170
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP04790409A Expired - Fee Related EP1673495B1 (en) | 2003-10-15 | 2004-10-14 | Method and installation for producing a flat multifilament elastomer thread |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP1673495B1 (en) |
DE (1) | DE602004024556D1 (en) |
FR (1) | FR2861091B1 (en) |
WO (1) | WO2005035842A1 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BR112018073755A2 (en) | 2016-05-20 | 2019-08-20 | A&At Uk Ltd | non-round spun spun filaments and methods and devices for producing them |
CN109735984B (en) * | 2019-02-21 | 2024-01-02 | 连云港纶洋单丝科技有限公司 | Preparation method and production device of high-strength coated fishing line |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5007193A (en) * | 1990-01-17 | 1991-04-16 | E. I. Du Pont De Nemours And Company | Fishing lure with improved elastomeric skirt |
US6248197B1 (en) * | 1996-07-02 | 2001-06-19 | E. I. Du Pont De Nemours And Company | Method for producing a shaped multifilament, non-thermoplastic, elastomeric yarn |
DE19829164A1 (en) * | 1998-06-30 | 2000-03-30 | Bayer Faser Gmbh | Elastane threads and process for their manufacture |
-
2003
- 2003-10-15 FR FR0312021A patent/FR2861091B1/en not_active Expired - Fee Related
-
2004
- 2004-10-14 EP EP04790409A patent/EP1673495B1/en not_active Expired - Fee Related
- 2004-10-14 DE DE602004024556T patent/DE602004024556D1/en active Active
- 2004-10-14 WO PCT/EP2004/011553 patent/WO2005035842A1/en active Application Filing
Non-Patent Citations (1)
Title |
---|
See references of WO2005035842A1 * |
Also Published As
Publication number | Publication date |
---|---|
FR2861091A1 (en) | 2005-04-22 |
EP1673495B1 (en) | 2009-12-09 |
WO2005035842A1 (en) | 2005-04-21 |
FR2861091B1 (en) | 2006-05-05 |
DE602004024556D1 (en) | 2010-01-21 |
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