EP1523671A2 - Vorrichtung und verfahren zur messung kritischer abmessungen mittels eines teilchenstrahls - Google Patents

Vorrichtung und verfahren zur messung kritischer abmessungen mittels eines teilchenstrahls

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Publication number
EP1523671A2
EP1523671A2 EP03764488A EP03764488A EP1523671A2 EP 1523671 A2 EP1523671 A2 EP 1523671A2 EP 03764488 A EP03764488 A EP 03764488A EP 03764488 A EP03764488 A EP 03764488A EP 1523671 A2 EP1523671 A2 EP 1523671A2
Authority
EP
European Patent Office
Prior art keywords
structural element
section
traverse
electron beam
cross sectional
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP03764488A
Other languages
English (en)
French (fr)
Inventor
Benzion Sender
Ophir Dror
Aviram Tam
Ovadya Menadeva
Roman Kris
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Applied Materials Israel Ltd
Applied Materials Inc
Original Assignee
Applied Materials Israel Ltd
Applied Materials Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Applied Materials Israel Ltd, Applied Materials Inc filed Critical Applied Materials Israel Ltd
Publication of EP1523671A2 publication Critical patent/EP1523671A2/de
Withdrawn legal-status Critical Current

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Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/26Electron or ion microscopes; Electron or ion diffraction tubes
    • H01J37/28Electron or ion microscopes; Electron or ion diffraction tubes with scanning beams
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/22Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
    • G01N23/225Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material using electron or ion
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/26Electron or ion microscopes
    • H01J2237/28Scanning microscopes
    • H01J2237/2813Scanning microscopes characterised by the application
    • H01J2237/2814Measurement of surface topography
    • H01J2237/2816Length

Definitions

  • This invention relates to systems and methods for inspecting objects such as but not limited to semiconductors wafers, reticles, during fabrication and, in particular, for inspecting structural elements such as lines, contacts, trenches and the like.
  • Integrated circuits are very complex devices that include multiple layers. Each layer may include conductive material, isolating material while other layers may include semi-conductive materials. These various materials are arranged in patterns, usually in accordance with the expected functionality of the integrated circuit. The patterns also reflect the manufacturing process of the integrated circuits.
  • Integrated circuits are manufactured by complex multi-staged manufacturing processes. During this multi-staged process resistive material is (i) deposited on a substrate/ layer, (ii) exposed by a photolithographic process, and (iii) developed to produce a pattern that defines some areas to be later etched.
  • a "critical dimension” is usually the width of a patterned line, the distance between two patterned lines, the width of a contact and the like.
  • One of the goals of the inspection process is to determine whether the inspected objects includes deviations from these critical dimensions. This inspection is usually done by charged particles beam imaging that provide the high resolution required to measure said deviations.
  • a typical inspected structural element is a line that has two opposing sidewalls.
  • the measurement of the bottom width of the line involves measuring the top width of the line as well as measuring its sidewalls.
  • Measurement of a structural element line critical dimensions using only a top view may result in faulty results, especially when one of the sidewalls has a negative sidewall angle such that an upper end of the sidewall obscures a lower end of that sidewall.
  • NanoSem 3D of Applied Materials from Santa Clara is a fully automated CD-SEM that has a column that allows electronic tilting as well as mechanical tilting of the scanning electron beam to scan the wafer surface with various tilt angles from several directions .
  • Critical dimension measurement may involve illuminating an test object by multiple tilted beams and processing the detected waveforms to define critical dimensions.
  • Multiple measurements have some disadvantages. First, they reduce the throughput of the inspection system, especially when the measurement involves changing the tilt of scanning electron beam. Such a change may require a de-Gauess stage, as well as an electron beam stabilization stage. A further disadvantage of multiple measurements- results from degradation (for example shrinkage and carbonization) of the measured structural element, as well as unwanted charging of the measured structural element .
  • the invention provides various scanning schemes that enable to selectively reduce the amount of measurements required for determining cross sectional features of structural elements.
  • 014] The invention provides a method for determining a cross sectional feature of a structural element having a sub-micron cross-section (at least one of the cross section dimensions are below one micron) , the cross section is defined by an intermediate section that is located between a first and a second traverse sections.
  • the method includes: (a) determining a first traverse section cross sectional feature in response to one or more scans of the structural element with an electron beam that is tilted at one or more corresponding tilt angle, such as to illuminate at least the top section and a first transverse section; (b) selecting, in response to a first parameter, whether to (i) determine a second traverse section cross sectional feature in response to the first traverse cross sectional feature, or (ii) to determine the second traverse section cross sectional feature in response to one or more scans of the structural element with an electron beam that is tilted at one or more corresponding tilt angle, such as to illuminate at least the top section and the second transverse section; and (c) determining the second traverse section cross sectional feature in response to the selection.
  • At one of the tilted angles can be substantially zero and even zero.
  • the tilt angle can be achieved by electrical tilt and/or mechanically tilt or a combination of both.
  • Mechanical tilt can be achieved by tilting the inspected object and/or the electron beam column (or a portion of said column) or a combination of both.
  • the invention provides a method for determining a cross sectional feature of a structural element having a sub-micron cross section, the cross section is defined by an intermediate section that is located between a first and a second traverse section.
  • the method includes: (a) scanning the structural element with an electron beam that is tilted at first positive angle in relation to an imaginary line perpendicular to the structural element, to provide a first set of data; (b) scanning the structural element with an electron beam that is tilted at second positive angle in relation to an imaginary line perpendicular to the structural element, to provide a second set of data, if the height of the structural element in not known or not estimated; (c) determining a first traverse section cross sectional feature in response of at least the first set of data; (d) determining a second traverse section cross sectional feature in response to the first traverse cross sectional feature, if a first parameter has a certain value; (e) whereas if the first parameter has another value performing the steps of: (e.l) scanning the
  • the invention provides an system for determining a cross sectional feature of a structural element having a sub-micron cross section, the cross section is defined by an intermediate section that is located between a first and a second traverse sections, the system includes: (a) first means for generating an electron beam; (b) second means for scanning the electron beam across a structural element of a measured object and for determining a tilt angle of the electron beam; whereas the second means is connected to and controlled by a processor; (c)a detector, connected to the processor, the detector is positioned such as to detect electrons emitted from the structural element as a result of an interaction with the electron beam.
  • the processor is operable to: (d.l) determine a first traverse section cross sectional feature in response to one or more scans of the structural element with an electron beam that is tilted at one or more corresponding tilt angle, such as to illuminate at least the top section and a first transverse section; (d.2) select, in response to a first parameter, whether to (i) determine a second traverse section cross sectional feature in response to the first traverse cross sectional feature, or (ii) to determine the second traverse section cross sectional feature in response to one or more scans of the structural element with an electron beam that is tilted at one or more corresponding tilt angle, such as to illuminate at least the top section and the second transverse section; and (d.3) determine the second traverse section cross sectional feature in response to the selection.
  • Figure la is a schematic illustration of a critical dimension scanning electron microscope, in accordance with an embodiment of the invention.
  • Figure lb is a perspective view of an objective lens according to another embodiment of the invention.
  • Figure 2a illustrates a perspective as well as a cross sectional view of a line
  • Figure 2b illustrates a cross section of another line that has a top section, a first traverse section that is positively oriented and a negatively oriented second traverse section;
  • Figures 3a - 3c are schematic illustration of waveforms that represent a relatively wide positively oriented traverse section, a relatively narrow traverse section and a negative oriented traverse section;
  • Figures 4-5 are illustrative flow charts of methods for determining a cross sectional feature of a structural element having a sub-micron cross section, in accordance with an embodiment of the invention
  • Figure 6a is a cross sectional view illustrating an exemplary relationship between two electron beam (tilted at a first and a second positive angle) and a structural element;
  • Figure 6b is a cross sectional view illustrating an exemplary relationship between two electron beams (tilted at a first and a second negative angle) and a structural element;
  • Figure 7 illustrates a cross section and some features that are measured by scanning the cross section with a tilted beam, in accordance to an aspect of the invention
  • a typical CD-SEM includes an electron gun, for generating an electron beam, deflection and tilt units as well as focusing lens, for enabling scanning of a specimen with an electron beam, that may be in a certain tilt condition, while reducing various aberrations and misalignments. Electrons, such as secondary electrons that are omitted as result of an interaction between the specimen and the electron beam are attracted to a detector that provides detection signals, that are processed by a processing unit. The detection signals may be used to determining various features of the specimen, as well as form images of the inspected specimen.
  • the invention may be implemented on CD-SEMs of various architectures that may differ from each other by the amount of their parts as well as the arrangement of said parts. For example the amount of deflection units, as well as the exact structure of each unit may vary.
  • the CD-SEM may include in- lens as well as out of lens detectors or a combination of both.
  • CD-SEM 100 includes an electron gun 103 emitting an electron beam 101, which is extracted by the anode 104.
  • the objective lens 112 focuses the electron beam on the specimen surface 105a.
  • the beam is scanned over the specimen using the scanning deflection unit 102.
  • An alignment of the beam to the aperture 106 or a desired optical axis respectively can be achieved by the deflection units 108 to 111.
  • electrostatic modules in the form of charged plates or a combination of coils and electrostatic deflectors can be used.
  • Detector 16 is able to detect secondary electrons that escape from the specimen 105 at a variety of angles with relatively low energy (3 to 50 eV) . Measurements of scattered or secondary corpuscles from a specimen can be conducted with detectors in the form of scintillators connected to photomultiplier tubes or the like. Since the way of measuring the signals does not influence the inventive idea in general, this is not to be understood as limiting the invention.
  • Detection signals are processed by a processing unit (that me a part of controller 33, but this is not necessarily so) that may have image processing capabilities and is able to process the detection signals in various manners.
  • a typical processing scheme includes generating a waveform that reflects the amplitude of the detection signal versus the scan direction. The waveform is further processed to determine locations of at least one edge, and other cross sectional features of inspected structural elements.
  • the different parts of the system are connected to corresponding supply units (such as high voltage supply unit 21) that are controlled by various control units, most of them are omitted from the figure for simplifying the explanation.
  • the control units may determine the current supplied to a certain part, as well as the voltage.
  • CD-SEM 100 includes a double deflection system that includes deflection units 110 and 111.
  • the beam tilt introduced in the first deflection unit 110 can be corrected for in the second deflection unit 111. Due to this double deflection system, the electron beam can be shifted in one direction without introducing a beam tilt of the electron beam with respect to the optical axis.
  • Figure lb is a perspective view of an objective lens 120 according to another embodiment of the invention.
  • the tilt deflection is performed below (downstream direction) of the objective lens.
  • Objective lens differs from objective lens 102 by having a pole-piece arranged in a quadruple formation, positioned between the objective lens and specimen, for controlling the tilt condition of the electron beam.
  • the polpieces are electrically connected to a ring and a core that bears additional coils (not shown) that are arranged such as to concentrate a magnetic flux at the space between the polepieces, through which the electron beam passes .
  • Modern CD-SEMs are able to measure structural elements that have cross sections that have sub-micron dimensions, with an accuracy of several nanometers.
  • cross section may be of interest. These feature may include, for example: the shape of the cross section, the shape of one or more sections of the cross section, the width and/or height and/or angular orientation of the cross section sections, as well as the relationship between cross section sections .
  • the feature can reflect typical values, as well as maximal and/or minimal values. Typically the width of the bottom of a line is of interest, but this is not necessarily so and other features may be of interest .
  • Figure 2a illustrates a perspective as well as a cross sectional view of line 210.
  • Line 210 has a cross section 220 that includes a top section 224 and two substantially opposing traverse sections 222 and 226 (that correspond to the top section 214 as well as to two sidewalls 212 and 214 of line 210) that are both positively oriented at substantially opposing angles, such that the bottom of the line is not obscured by the top section 210.
  • Figure 2b illustrates a cross section 230 of another line that has a top section 234, a first traverse section 232 that is positively oriented and a negatively oriented second traverse section 236.
  • Figure 2b also illustrates the convention of positive angles, negative angles and zero angle.
  • Figures 2a-2b refer to a line
  • the method and system are applicable to determine cross sectional features (such as top CD, bottom CD, maximal CD, and the like) of various structural elements, such as contacts, recesses and the like.
  • Figures 3a - 3c are schematic illustration of waveforms 250 -
  • the waveform portion that is associated with steep sidewalls, as well as negative oriented sidewalls is relatively narrow and corresponds to the width f the scanning electron beam.
  • Figure 4 illustrates a flow chart of method 400 for determining a cross sectional feature of a structural element having a sub-micron cross section, the cross section is defined by an intermediate section that is located between a first and a second traverse sections.
  • Method 400 starts by step 420 of determining a first traverse section cross sectional feature in response to at least one scan of the structural element with an electron beam that is tilted at one or more corresponding tilt angle, such as to illuminate at least the top section and a first transverse section.
  • a single tilted scan is enough if the height of the structural element is known or estimated. Else, at least two scans (at different tilt conditions) is required.
  • the .height of the structural element may be estimated in response to a height calibration process and/or to information provided by the measured object manuf cturer.
  • the calibration process may include multiple measurements of the height of structural elements across the tested object. This process may include mapping the height of structural elements within different regions of the tested object. Said measurement may be implemented by a scanning electron microscope but this is not necessarily so and other tools, such as atomic force microscope, confocal microscopes may be used.
  • Step 420 is followed by query step 430 of checking what is the value of a first parameter, which is equivalent to checking whether a predefined first condition was fulfilled, and/or checking whether the value of the first parameter is within a predefined range or ranges.
  • the first parameter determines whether the results of step 420 can be used to estimate a feature of the second section, such as to reduce the amount of scans required for determining a feature of a cross section.
  • the first condition is fulfilled if the traverse sections may be assumed to be symmetrical.
  • the first parameter is also responsive to a suspected traverse section measurement, as steep traverse sections, as well as negative oriented traverse sections are associated with certain waveforms. The inventors found that a traverse section is suspected if the width of it substantially equals the width of the electron beam.
  • step 430 is followed by step 440 of determining a second traverse section cross sectional feature in response to the first traverse cross sectional feature. Else, step 430 is followed by step 450 of determining a second traverse section cross sectional feature in response to at least one scan of the structural element with an electron beam that is tilted at one or more corresponding tilt angle, such as to illuminate at least the top section and the second transverse section. It is noted that in many cases a single tilted scan is enough as the height of the structural element is known from the results of step 420 (if they are not estimated or previously known in advance) .
  • the values of the first parameter may be determined in various manners, such as but not limited to the following manners and/or by a combination of these manners: (i) determination by a preliminary calibration process; (ii) determination in response to the symmetry of the waveform acquired during step 420; (iii) determination in response to a correlation between waveform section associated with traverse sections, (iv) determination by finding a best matching or substantially matching waveform out of a bank of previously recorded waveforms. It is noted that the waveform may be generated in response to a scan with a tilted electron beam and/or a non-tilted electron beam. The symmetry can be given to the CD-SEM by an end user.
  • the symmetry can be measures by measuring a structural feature (or multiple structural features) , rotating the inspected object, locating the previously measured structural object and measuring it from the "opposite" direction.
  • the calibration process may include multiple measurements of both sides of multiple structural elements and determination of whether the first condition is fulfilled.
  • the first condition may be also responsive to the required accuracy of the cross sectional feature measurement.
  • the value of the first parameter may be alternatively or additionally responsive to a relationship between the width of the electron beam and a width of a waveform portion associated with either the first or second traverse portions, whereas the waveform is acquired during the step of determining a first traverse section cross sectional feature.
  • a typical first parameter value can be true or false, but this is not necessarily so, as it may have a range of values that indicate an amount of certainty. When the latter range of values is provided the fulfillment of a first condition may be further responsive to additional parameters such as the required accuracy of the overall measurements, and the like.
  • Steps 440 and 450 are followed by step 460 of determining a cross sectional feature of the structural element .
  • the cross sectional features of the top/intermediate) section are known from step 420 and/or step 440, and the first as well as the second features of the first and second traverse sections are also known, various features of the structural element can be calculated. For example, assuming that the first condition was fulfilled, the bottom critical measurement of a line is the width of the top section plus twice the horizontal projection of the first sidewall.
  • Figure 5 illustrates a flow chart of method 500 for determining a cross sectional feature of a structural element having a sub-micron cross section, the cross section is defined by an intermediate section that is located between a first and a second traverse sections.
  • Method 500 starts at step 510 of scanning the structural element with an electron beam that is tilted at first positive angle in relation to an imaginary line perpendicular to the structural element, to provide a first set of data.
  • An exemplary relationship between an electron beam 600 (tilted at a first positive angle) and a structural element 210 is illustrated in Figure 6a.
  • Step 510 is followed by query step 520 of asking if the height of structural element is known (the height of the structural element was previously measured) or is estimated (from measurements of other structural elements, for example during a height calibration process) . If the answer is negative jumping to step 530, else jumping to step 540.
  • Step 530 includes scanning the structural element with an electron beam that is tilted at second positive angle in relation to an imaginary line perpendicular to the structural element, to provide a second set of data.
  • An exemplary relationship between an electron beam 610 (tilted at a second positive angle) and a structural element 210 is illustrated in Figure 6a.
  • Step 530 is followed by step 540.
  • Step 540 involves determining a first traverse section cross sectional feature in response of at least the first set of data. Conveniently, if step 530 was skipped the feature is determined in response to the first set of data while if step 530 was performed, the determination of the feature is responsive to both data sets . It is noted that both data sets may be graphically illustrated as a waveform.
  • Step 540 is followed by a query step 550 of checking what is the value of a first parameter.
  • a first parameter is used to determine whether a second traverse section cross sectional feature can be figured out from the first traverse section cross sectional feature. As illustrated in further details in the previous pages, the determination is responsive to an estimated symmetry between the first and second traverse sections and/or to the width of these traverse sections.
  • step 550 is followed by step 560, else step 550 is followed by step 601.
  • Step 601 includes determining a second traverse section cross sectional feature in response to the first traverse cross sectional feature. Step 601 as well as step 580 are usually followed by an additional step of determining a cross sectional feature of the structural element.
  • Step 560 includes scanning the structural element with an electron beam that is tilted at first negative angle in relation to an imaginary line perpendicular to the structural element, to provide a third set of data.
  • An exemplary relationship between an electron beam 620 (tilted at first negative angle) and a structural element is illustrated in Figure 6b.
  • Step 560 is followed by query step 570 of asking if the height of structural element is known (the height of the structural element was previously measured) or is estimated (from measurements of other structural elements, for example during a height calibration process) . If the answer is negative jumping to step 580, else jumping to step 590.
  • Step 580 includes scanning the structural element with an electron beam that is tilted at second negative angle in relation to an imaginary line perpendicular to the structural element, to provide a fourth set of data.
  • An exemplary relationship between an electron beam 630 (tilted at second negative angle) and a structural element is illustrated in Figure 6b. Step 580 is followed by step 590.
  • Step 590 involves determining a second traverse section cross sectional feature in response of at least the third set of data. Conveniently, if step 580 was skipped the feature is determined in response to the third set of data while if step 580 was performed, the determination of the feature is responsive to both third and fourth data sets . It is noted that both data sets may be graphically illustrated as a waveform.
  • the intermediate section which may be a top section in the case of an elevated structural element, may be determined from each of the scanning steps. It is further noted that given the first and second traverse section cross sectional features the cross section of the structural element as well as any feature (such as but not limited to top CD, bottom CD, maximal CD) of said cross section can be determined.
  • a typical cross sectional feature is the horizontal projection of a traverse section. In cases where the tilt angle is relatively small it is assumed that the tilt angle is approximately equal to the Tangents of this angle .
  • methods 400 and 500 may include multiple measurements of one or more cross sectional features, even if the height of the structural elements in known or estimated and even if a certain cross sectional feature was measured.
  • Figure 7 illustrates a cross section and some features that are measured by scanning the cross section with a tilted beam, in accordance to an aspect of the invention.
  • Z height of line; X ⁇ - width of top of line ("top Critical dimension”) ; X ER - horizontal projection of right side wall; X EL - horizontal projection of right side wall; X B horizontal projection of the bottom of the line ("bottom Critical Dimension”); c. - positive tilt angle; ⁇ E - measured dimension of a sidewall at tilt angle a .
  • the present invention can be practiced by employing conventional tools, methodology and components. Accordingly, the details of such tools, component and methodology are not set forth herein in detail. In the previous descriptions, numerous specific details are set forth, such as shapes of cross sections of typical lines, amount of deflection units, etc . , in order to provide a thorough understanding of the present invention. However, it should be recognized that the present invention might be practiced without resorting to the details specifically set forth.

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Length-Measuring Devices Using Wave Or Particle Radiation (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Testing Or Measuring Of Semiconductors Or The Like (AREA)
EP03764488A 2002-07-11 2003-07-11 Vorrichtung und verfahren zur messung kritischer abmessungen mittels eines teilchenstrahls Withdrawn EP1523671A2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US39486402P 2002-07-11 2002-07-11
US394864P 2002-07-11
PCT/US2003/021690 WO2004008255A2 (en) 2002-07-11 2003-07-11 Method and apparatus for measuring critical dimensions with a particle beam

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EP (1) EP1523671A2 (de)
JP (1) JP4493495B2 (de)
KR (1) KR101057554B1 (de)
CN (1) CN1668915B (de)
AU (1) AU2003263776A1 (de)
WO (1) WO2004008255A2 (de)

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JP2005533252A (ja) 2005-11-04
CN1668915A (zh) 2005-09-14
JP4493495B2 (ja) 2010-06-30
WO2004008255A3 (en) 2004-06-10
AU2003263776A1 (en) 2004-02-02
KR101057554B1 (ko) 2011-08-17
AU2003263776A8 (en) 2004-02-02
WO2004008255A2 (en) 2004-01-22
KR20060084787A (ko) 2006-07-25
CN1668915B (zh) 2011-06-15
WO2004008255A8 (en) 2004-07-22

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