EP1405345A2 - Organisches, elektrolumineszierendes display und dessen herstellung - Google Patents
Organisches, elektrolumineszierendes display und dessen herstellungInfo
- Publication number
- EP1405345A2 EP1405345A2 EP02752995A EP02752995A EP1405345A2 EP 1405345 A2 EP1405345 A2 EP 1405345A2 EP 02752995 A EP02752995 A EP 02752995A EP 02752995 A EP02752995 A EP 02752995A EP 1405345 A2 EP1405345 A2 EP 1405345A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- electrode
- insulating layer
- layer
- windows
- structured
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 21
- 238000005538 encapsulation Methods 0.000 claims abstract description 10
- 229920001002 functional polymer Polymers 0.000 claims abstract description 6
- 239000010410 layer Substances 0.000 claims description 103
- 238000000034 method Methods 0.000 claims description 31
- 239000000758 substrate Substances 0.000 claims description 22
- 239000002346 layers by function Substances 0.000 claims description 12
- 229920002120 photoresistant polymer Polymers 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 8
- 239000002904 solvent Substances 0.000 claims description 8
- 239000004642 Polyimide Substances 0.000 claims description 6
- 229920001721 polyimide Polymers 0.000 claims description 6
- 238000011161 development Methods 0.000 claims description 5
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- AMGQUBHHOARCQH-UHFFFAOYSA-N indium;oxotin Chemical compound [In].[Sn]=O AMGQUBHHOARCQH-UHFFFAOYSA-N 0.000 claims description 2
- 229910052709 silver Inorganic materials 0.000 claims description 2
- 239000004332 silver Substances 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 abstract description 22
- 239000011159 matrix material Substances 0.000 abstract description 10
- 229910052751 metal Inorganic materials 0.000 description 27
- 239000002184 metal Substances 0.000 description 27
- 238000005516 engineering process Methods 0.000 description 10
- 239000010408 film Substances 0.000 description 8
- 238000007740 vapor deposition Methods 0.000 description 6
- 239000011521 glass Substances 0.000 description 5
- 239000011810 insulating material Substances 0.000 description 5
- 239000012044 organic layer Substances 0.000 description 5
- 239000010406 cathode material Substances 0.000 description 4
- 239000011368 organic material Substances 0.000 description 4
- 238000013461 design Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 230000005525 hole transport Effects 0.000 description 3
- -1 hydroxyquinoline aluminum Chemical compound 0.000 description 3
- 238000007641 inkjet printing Methods 0.000 description 3
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- 238000007639 printing Methods 0.000 description 3
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- 238000009834 vaporization Methods 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 238000003848 UV Light-Curing Methods 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 238000009125 cardiac resynchronization therapy Methods 0.000 description 2
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- 229920001609 Poly(3,4-ethylenedioxythiophene) Polymers 0.000 description 1
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- 150000007513 acids Chemical class 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
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- 229920000553 poly(phenylenevinylene) Polymers 0.000 description 1
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- 238000012545 processing Methods 0.000 description 1
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Classifications
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K59/00—Integrated devices, or assemblies of multiple devices, comprising at least one organic light-emitting element covered by group H10K50/00
- H10K59/10—OLED displays
- H10K59/17—Passive-matrix OLED displays
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K59/00—Integrated devices, or assemblies of multiple devices, comprising at least one organic light-emitting element covered by group H10K50/00
- H10K59/10—OLED displays
- H10K59/17—Passive-matrix OLED displays
- H10K59/173—Passive-matrix OLED displays comprising banks or shadow masks
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K59/00—Integrated devices, or assemblies of multiple devices, comprising at least one organic light-emitting element covered by group H10K50/00
- H10K59/10—OLED displays
- H10K59/17—Passive-matrix OLED displays
- H10K59/179—Interconnections, e.g. wiring lines or terminals
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K50/00—Organic light-emitting devices
- H10K50/80—Constructional details
- H10K50/84—Passivation; Containers; Encapsulations
- H10K50/841—Self-supporting sealing arrangements
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K59/00—Integrated devices, or assemblies of multiple devices, comprising at least one organic light-emitting element covered by group H10K50/00
- H10K59/80—Constructional details
- H10K59/87—Passivation; Containers; Encapsulations
- H10K59/871—Self-supporting sealing arrangements
Definitions
- the invention relates to a passive matrix driven display based on electroluminescent polymers with a structured matrix of pixels and a structured second electrode, and the production thereof.
- Shallow depth is another essential criterion. Many devices even require a display depth of less than one millimeter. Due to the limited capacity of the batteries in the mobile devices, only a low power consumption of the displays is required. Another criterion is good readability, even at a large angle between the display surface and the viewer, as well as readability in different ambient lighting conditions. The ability to display multicolored or full-color information is becoming increasingly important. And last but not least, of course, is the lifespan of the components important prerequisites for use in the various devices. The importance of the individual requirement criteria for the displays is weighted differently depending on the areas of application.
- LC displays liquid crystal displays
- the technology of the LCDs also has serious disadvantages.
- LC displays are not self-emitting and can therefore only be read or recognized easily in particularly favorable ambient lighting conditions. In most cases, this requires backlighting, which in turn multiplies the thickness of the flat screen.
- the majority of the electrical power consumption is then used for the lighting, and a higher voltage is required for the operation of the lamps or fluorescent tubes. This is usually generated with the aid of "voltage-up converters" from the batteries or accumulators.
- Another disadvantage is the greatly restricted viewing angle of simple LCDs and the long switching times of individual pixels, which are typically a few milliseconds and are also strongly temperature-dependent Delayed image build-up, for example, is extremely disruptive when used in transportation or video applications.
- OLEDs have two technologies that differ in the type and processing of organic materials.
- low molecular weight organic materials such as hydroxyquinoline aluminum III salt (Alq 3 ) can be used, which are mostly applied to the corresponding substrate by thermal evaporation.
- Displays based on this technology are already commercially available and z. Zt. mainly used in automotive electronics. Since the production of these components involves numerous process steps under high vacuum, this technology has disadvantages due to high investment and maintenance costs, as well as relatively low throughput,
- organic light-emitting diodes Since 1990, an OLED technology has therefore been developed which uses polymers as organic materials, which can be applied to the substrate from a solution by wet chemistry. The vacuum steps required to produce the organic layers are eliminated with this technique.
- Typical polymers are polyaniline, PEDOT (Bayer), poly (p-phenylene-vinylene), poly (2-methoxy-5- (2'-ethyl) -hexyloxy-p-phenylene-vinylene) or polyalkylfluorenes, and numerous derivatives from that.
- the layer structure of organic light-emitting diodes is typically carried out as follows:
- a transparent substrate for example glass
- a transparent electrode for example indium tin oxide, ITO
- the transparent electrode is then structured using a photolithographic process, which later defines the shape of the luminous pixel.
- One or more organic layers consisting of electroluminescent polymers, oligomers, low molecular weight compounds (see above) or mixtures thereof are then applied to the substrate with the structured electrode.
- Polymeric substances are mostly applied from the liquid phase by knife coating or spin coating, and more recently also by various printing techniques.
- Low molecular weight and oligomeric substances are mostly deposited from the gas phase by vapor deposition or "physical vapor deposition" (PVD).
- the total layer thickness can be between 10 nm and 10 ⁇ m and is typically between 50 and 200 nm.
- a counter electrode is then placed on these organic layers.
- the cathode is applied, which usually consists of a metal, a metal alloy or a thin insulator layer and a thick metal layer.
- the vapor deposition by thermal evaporation, electron beam evaporation or sputtering is usually used in turn to produce the cathode layers.
- the challenge in the production of structured displays is in particular to structure the layer structure described above in such a way that a matrix of individually controllable pixels is created.
- ITO is extremely insensitive to typical photoresists and developer liquids and can be easily etched using acids such as HBr. Let it be structures with a resolution of a few micrometers can be easily generated.
- the individual functional layers can be structured onto the substrate by means of a shadow mask, so that the individual pixels are formed.
- a shadow mask For the stripe-shaped structuring of the metal cathode (perpendicular to the underlying ITO stripes), evaporation by means of a shadow mask technique also lends itself.
- An alternative method for structuring the metal cathode is the technique of isolating separators. Immediately after structuring the ITO anode, a series of isolating bars with a sharp tear-off edge are applied to the substrates perpendicular to the ITO strips using a lithographic technique. After the organic layers have been deposited, the metal cathode is evaporated over a large area (i.e. without the use of a shadow mask), the metal film tearing off at the sharp edges of the separating webs. In this way, isolated metal strips (rows) are formed, perpendicular to the underlying ITO anode (columns). If a voltage is applied to a specific ITO anode column and a metal cathode row, the organic emitter layer lights up at the crossing point between row and column. These dividers can have different cross sections.
- European patent 0 892 028 A2 describes a method in which a layer of an insulating material is first applied to the ITO substrate, in which windows are embedded at the locations where the pixels are later to be located.
- This insulating material can e.g. act as photoresist, which is modified so that it is not wetted by the polymer solutions.
- the individual drops of the solutions red, green, blue
- the individual drops of the solutions are thus enclosed after application at the corresponding points without running into one another and can therefore dry separately from one another and produce the polymer layer.
- cathode material applied last is generally made of very sensitive metals, such as calcium or aluminum, which are easily oxidized by air or moisture. This means that the lifespan of the displays is greatly reduced.
- the challenge in the production of passive matrix-driven displays is, in particular, to structure the layer structure described above in such a way that a matrix of individually controllable pixels is created by simultaneously structuring the functional layers and the cathodes, it being necessary to take into account that the cathode material is opposite Air and moisture is very sensitive.
- the above-mentioned problems are avoided according to the invention by a display according to claim 1.
- Advantageous embodiments of the display and its manufacture are the subject of the subclaims.
- the invention describes a passive matrix-driven display in which, in comparison to the prior art, the window layer for structuring the pixels has been modified in such a way that it permits simple structuring of the second electrode, the cathode, and at the same time the problem-free contacting of the cathode by air and oxygen-stable Allows fittings. Furthermore, an encapsulation is attached above the display, which only leaves one end of each cathode connector free and otherwise covers the entire window layer and the cathode, so that a display with increased service life is produced.
- a display according to the invention has the following features:
- first electrode strips running parallel to one another are located on a substrate and electrode connecting pieces are arranged transversely thereto,
- windows being arranged in this layer above the first electrode strip and each delimiting a functional layer located therein,
- a second, strip-shaped electrode is applied transversely to the first electrode strips and contacts the respective functional layer in the windows and the electrode connecting pieces, -
- An encapsulation is present that the insulating
- the invention describes a display in which, in contrast to the prior art, the window layer for structuring the image pixels has been modified in such a way that it has extensions between the electrode connection pieces or windows are arranged in the window layer above the electrode connection pieces, which contact the electrode connection pieces by the second Allow electrode (cathode).
- the additionally structured electrode connecting pieces like the first electrode strips, preferably consist of the air and moisture-stable ITO. Because these cathode connecting pieces are led out under the encapsulation, the cathode material, which usually consists of sensitive metals, is not exposed to the air, which considerably increases the service life of a display.
- shadow mask technology lends itself to the strip-like structuring of the metal cathode (perpendicular to the underlying ITO strips).
- the metal strips are produced by thermal evaporation in a vacuum using a mask with strip-shaped openings.
- This gap can lead to back-vaporization of the shadow mask and thus considerably limits the minimum distance between the cathode strips.
- the widening of the window layer between the electrode connecting pieces or alternatively the windows in the window layer above the electrode connecting pieces prevent or significantly reduce the back-vaporization of the shadow mask.
- a display according to the invention has the following features:
- a second and a third insulating layer are arranged one above the other on the first insulating layer and shaped into strip-shaped webs, transverse to the first electrode strips between the windows,
- the second electrode is arranged between the webs and is structured by these in strips.
- the cathode when the cathode material is evaporated over a large area, the cathode is structured by tearing off the metal film at the edges of the separating webs, which in the case of a two-layer design each consist of a foot 15 and a cap 20.
- the window layer is guided according to the invention over the ITO electrode connectors and either additional windows in the window layer or recesses in the window layer are provided over the ITO connectors, so that the Separators at the edge of the window layer do not have to overcome a step, which could lead to instabilities in the separator structure (see FIG. 3).
- the dividers are therefore always built on a base of the window layer. Both versions of the window layer still allow contacting of the cathode connection pieces by the cathode.
- the method for producing the display according to the invention essentially comprises a new structuring of the window layer according to the invention after application of the first electrode strips and the electrode connecting pieces.
- two different techniques are used to structure the metal cathode.
- the metal cathode is vapor-deposited using a shadow mask.
- the strip-shaped separating webs are first produced over the window layer, then the functional polymers are preferably printed into the windows and then the structured cathode is produced by evaporating and tearing off the metal film at the edges of the separating webs.
- Figure 1 shows an inventive design of the window layer with windows over the electrode connectors.
- Figure 2 shows another embodiment of the window layer with extensions between the electrode connectors.
- FIG. 3 shows the edge which separating webs, which are structured according to the prior art, have to be overcome when they are guided between the electrode connecting pieces.
- FIG. 4 shows the back-vaporization of a shadow mask when the second electrode is applied in the region of the edges of the window layer in the case of a conventional structuring of the window layer.
- FIG. 5 shows the structure of a display according to the invention with dividers and a novel structuring of the window layer with a window.
- Figure 6 shows the complete structure of the display with an encapsulation, which leaves one end of the air-stable electrode connectors free.
- FIGS. 7A to 7E each show in cross section the structure of a substrate at various stages in the production of the display according to the invention with a shadow mask.
- FIGS. 8A to 8G each show in cross section the structure of a substrate at various stages in the manufacture of the display according to the invention with a two-layer separating web for separating the cathodes.
- FIG. 1 shows a possible embodiment of the window layer 5, round windows being located above the first electrode strip 1 and additional windows 40 being present above the electrode connection pieces 2a.
- the course of an electrode connection piece below the window layer is exemplarily indicated by a dashed line.
- FIG. 2 shows extensions 55 in the window layer 5, which are arranged between the electrode connection pieces 2a.
- the course of a second electrode strip, a cathode strip, is shown as an example.
- FIG. 3 shows the edge which the separating webs have to overcome in a window layer 5 structure corresponding to the prior art. What can be seen is a two-layer design option for the separating web with a foot 15 and a cap 20.
- FIG. 4 shows the rear vapor deposition of a shadow mask 60 when the second electrode (cathode) is being produced in the case of a window layer 5 structure which corresponds to the prior art.
- FIG. 5 shows a top view of the structure of a display according to the invention in the case of a separator structure for separating the cathodes.
- a separator structure for separating the cathodes.
- the window layer 5 has been guided over the electrode connections in such a way that the separating webs consisting of feet 15 and caps 20 have no step to overcome over the entire length of the cathode.
- Figure 6 shows the complete structure of a display according to the invention in supervision.
- An encapsulation 30 metal or glass cap
- FIG. 5 shows the ends of the first electrode strips 1 and the electrode connecting pieces 2a being left free.
- FIG. 7A shows the photolithographic structuring of a layer 5a applied over the entire area to produce the window layer 5 through the exposure mask 90.
- FIG. 7B shows the application of the functional layers in the windows of the window layer 5.
- the hole transport polymer 12 and the emitter polymer 14 are applied the second electrode, the cathode, was applied in layers lying one above the other in the windows 10 of the window layer 5, through a shadow mask 60.
- FIG. 7D shows the complete structure of the display according to the invention with the second electrode 2.
- FIG. 7E shows the subsequent encapsulation 30 over the entire component.
- FIGS. 8A to 8G show a variant of the production method mentioned above, in which the second electrode, the metal cathode, is applied by applying a metal film over a large area and tearing this film off at the edges of a two-part film. layered separator is structured.
- FIG. 8A shows, in analogy to FIG. 7A, the structuring of the window layer 5 by the shadow mask 90.
- FIG. 8B after application of a non-photosensitive layer 15A (for example polyimide) and the third insulating layer 20A (for example a photoresist), the caps 20 of the separating webs are produced by exposure using a shadow mask 100 and subsequent development.
- FIG. 8C shows the structuring of the feet 15 of the separating webs by means of a solvent which acts selectively on the layer 15A.
- the caps of the separating webs can serve as a mask, whereby the caps can also be undercut by suitable choice of the duration of action of the solvent, so that the feet of the separating webs have a smaller width than the caps.
- FIG. 8D after the three-layer structure 5, 15, 20 has been structured, the functional polymers, e.g. brought into the windows by inkjet printing.
- FIG. 8E shows the large-area vapor deposition of the second electrode 2, which is structured by tearing off the metal film at the edges of the separating webs during the vapor deposition.
- FIG. 8F shows in cross-section the structure of an embodiment of the display according to the invention after the second electrode 2 has been applied.
- the caps of the separating webs contain strips of a non-functional metal layer 2b which, when the electrode material for the second electrode is applied, are torn off at the edges of the separating webs is formed and the functional layers are not electrically contacted.
- FIG. 8G shows the encapsulation 30 subsequently applied, which covers the entire component except for parts of the electrode connecting pieces 2a and parts of the first electrode strips (see also FIG. 6).
- a large area coated with ITO glass substrate 3 is structured by a prior art lithographic process in combination with an etching process with 30 percent HBr solution so that the first electrode strips 1 and the electrode connecting pieces 2a are formed.
- a positive photoresist is spun onto the substrate and preheated on a hot plate.
- the spin parameters are chosen so that a layer with a thickness of approximately 6 ⁇ m is produced.
- window structures 10 are produced over the first electrode strip and the photoresist is additionally structured in the region of the electrode connection pieces in such a way that either the extensions 55 between the connections (see FIG. 2) or the windows 40 are formed over the connections
- any insulating, layer-forming material for example silicon dioxide
- Etching can be structured.
- the substrate pre-structured in this way is subjected to several cleaning steps by treatment with solvents and / or plasma.
- the hole transport polymer solution is then initially added to each window. After suitable drying, the solutions of the emitter polymers are then applied and dried using the same system (see FIG. 7B). 5. The second electrode is then produced by vapor deposition through a shadow mask 60 (see FIG. 7C).
- the component is provided, for example, with a metal or glass cap 30 and, for example, encapsulated with a UV-curing epoxy adhesive, one end of each electrode connection piece 2a being left free (see FIGS. 7E and 6).
- a layer of a second insulating material preferably a polyimide, is spun onto the substrate over a large area, followed by a brief heating, for example on a hotplate.
- the pre-structured substrates are subjected to several cleaning steps by treatment with solvents and / or plasma.
- a layer of a base metal for example calcium
- a layer of a stable, noble metal for example aluminum or silver
- the component is provided, for example, with a metal or glass cap 30 and, for example, encapsulated with a UV-curing epoxy adhesive (see FIG. 8G).
Landscapes
- Electroluminescent Light Sources (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10133685 | 2001-07-11 | ||
DE10133685A DE10133685B4 (de) | 2001-07-11 | 2001-07-11 | Organisches, elektrolumineszierendes Display und dessen Herstellung |
PCT/DE2002/002428 WO2003007377A2 (de) | 2001-07-11 | 2002-07-03 | Organisches, elektrolumineszierendes display und dessen herstellung |
Publications (1)
Publication Number | Publication Date |
---|---|
EP1405345A2 true EP1405345A2 (de) | 2004-04-07 |
Family
ID=7691392
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP02752995A Withdrawn EP1405345A2 (de) | 2001-07-11 | 2002-07-03 | Organisches, elektrolumineszierendes display und dessen herstellung |
Country Status (5)
Country | Link |
---|---|
US (1) | US7375461B2 (de) |
EP (1) | EP1405345A2 (de) |
JP (1) | JP2004535044A (de) |
DE (1) | DE10133685B4 (de) |
WO (1) | WO2003007377A2 (de) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10133686C2 (de) | 2001-07-11 | 2003-07-17 | Osram Opto Semiconductors Gmbh | Organisches, elektrolumineszierendes Display und dessen Herstellung |
KR100813833B1 (ko) * | 2002-08-23 | 2008-03-17 | 삼성에스디아이 주식회사 | 전자 발광 소자와 그 제조방법 |
DE10339941A1 (de) | 2003-08-29 | 2005-03-24 | BSH Bosch und Siemens Hausgeräte GmbH | Kältegerät mit OLED-Display |
US7495388B2 (en) * | 2004-01-08 | 2009-02-24 | Samsung Electronics Co., Ltd. | Display device, and method of manufacturing the display device |
US8212474B2 (en) * | 2004-01-08 | 2012-07-03 | Samsung Electronics Co., Ltd. | Display device, and method of manufacturing the display device |
WO2009113003A2 (en) * | 2008-03-13 | 2009-09-17 | Nxp B.V. | Luminescent component and manufacturing method |
KR20110081968A (ko) * | 2008-10-06 | 2011-07-15 | 아사히 가라스 가부시키가이샤 | 전자 디바이스용 기판, 그의 제조 방법, 이것을 이용한 전자 디바이스, 그의 제조 방법 및 유기 led 소자용 기판 |
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GB9027618D0 (en) * | 1990-12-20 | 1991-02-13 | Smiths Industries Plc | Displays |
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JP2874605B2 (ja) * | 1995-07-27 | 1999-03-24 | ヤマハ株式会社 | 電界放出型素子の製造方法 |
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JPH10288965A (ja) * | 1997-04-14 | 1998-10-27 | Casio Comput Co Ltd | 表示装置 |
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2001
- 2001-07-11 DE DE10133685A patent/DE10133685B4/de not_active Expired - Lifetime
-
2002
- 2002-07-03 WO PCT/DE2002/002428 patent/WO2003007377A2/de active Application Filing
- 2002-07-03 JP JP2003513041A patent/JP2004535044A/ja active Pending
- 2002-07-03 US US10/483,144 patent/US7375461B2/en not_active Expired - Lifetime
- 2002-07-03 EP EP02752995A patent/EP1405345A2/de not_active Withdrawn
Non-Patent Citations (1)
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See references of WO03007377A3 * |
Also Published As
Publication number | Publication date |
---|---|
DE10133685B4 (de) | 2006-05-18 |
US20040169464A1 (en) | 2004-09-02 |
JP2004535044A (ja) | 2004-11-18 |
DE10133685A1 (de) | 2003-01-30 |
WO2003007377A3 (de) | 2003-05-30 |
US7375461B2 (en) | 2008-05-20 |
WO2003007377A2 (de) | 2003-01-23 |
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