EP1166287A1 - Parafoudre perfectionne a base de varistances electriques - Google Patents
Parafoudre perfectionne a base de varistances electriquesInfo
- Publication number
- EP1166287A1 EP1166287A1 EP00971467A EP00971467A EP1166287A1 EP 1166287 A1 EP1166287 A1 EP 1166287A1 EP 00971467 A EP00971467 A EP 00971467A EP 00971467 A EP00971467 A EP 00971467A EP 1166287 A1 EP1166287 A1 EP 1166287A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- varistors
- coating
- composite material
- stack
- envelope
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01C—RESISTORS
- H01C7/00—Non-adjustable resistors formed as one or more layers or coatings; Non-adjustable resistors made from powdered conducting material or powdered semi-conducting material with or without insulating material
- H01C7/18—Non-adjustable resistors formed as one or more layers or coatings; Non-adjustable resistors made from powdered conducting material or powdered semi-conducting material with or without insulating material comprising a plurality of layers stacked between terminals
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01C—RESISTORS
- H01C7/00—Non-adjustable resistors formed as one or more layers or coatings; Non-adjustable resistors made from powdered conducting material or powdered semi-conducting material with or without insulating material
- H01C7/10—Non-adjustable resistors formed as one or more layers or coatings; Non-adjustable resistors made from powdered conducting material or powdered semi-conducting material with or without insulating material voltage responsive, i.e. varistors
- H01C7/12—Overvoltage protection resistors
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49002—Electrical device making
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49002—Electrical device making
- Y10T29/49082—Resistor making
- Y10T29/49085—Thermally variable
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49002—Electrical device making
- Y10T29/49082—Resistor making
- Y10T29/49087—Resistor making with envelope or housing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49002—Electrical device making
- Y10T29/49082—Resistor making
- Y10T29/49087—Resistor making with envelope or housing
- Y10T29/49096—Resistor making with envelope or housing with winding
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49002—Electrical device making
- Y10T29/49082—Resistor making
- Y10T29/49087—Resistor making with envelope or housing
- Y10T29/49098—Applying terminal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49002—Electrical device making
- Y10T29/49082—Resistor making
- Y10T29/49099—Coating resistive material on a base
Definitions
- the present invention relates to the field of surge arresters. It applies in particular to lightning arresters for medium voltage, typically to electrical networks of nominal voltage greater than 1 kV effective between phases.
- Surge arresters are devices designed to be connected between an electrical line, in particular at medium or high voltage, and earth, to limit the amplitude and the duration of the overvoltages appearing on the line.
- overvoltages can be due for example to atmospheric phenomena, such as lightning, or induction phenomena in the conductors. These overvoltages can also be due to operations on the live line.
- Surge arresters are generally formed by stacking different varistors, most often nowadays by stacking several discs based on zinc oxide, whose electrical resistivity is highly non-linear depending on the applied voltage.
- these varistors do not let practically any current pass as long as the voltage at their terminals is less than a conduction threshold and on the other hand, let pass a very strong current, which can reach several tens of kA, when the voltage applied to their terminals exceeds the aforementioned conduction threshold.
- the number of varistors used in the arrester is such that the operating voltage on the power line is less than the conduction threshold of the stack of varistors.
- the surge arrester can permanently support the operating voltage, without significant current leakage, and on the other hand makes it possible to drain the discharge currents of very high intensity which may appear temporarily on the line in the event of overvoltage. accidental.
- Surge arresters known today generally include:
- Document GB-A-2 073 965 has proposed, for example, to produce this envelope using a heat-shrinkable material.
- EP-A-0 231245 and US-A-4 456 942 have proposed to produce the envelope surrounding the varistors using an elastomeric material, formed in particular by overmolding.
- EP-A-0 274 674 proposed to overmold an envelope made of a composite material based on elastomer, EPDM, silicone, or other resin, loaded or not, on a stack of varistors.
- the document EP-A-0 196 370 proposed to produce the envelope on a varistor body by pouring a synthetic resin formed for example of epoxy resin, polymer concrete, silicone resin, or an elastomer, or by covering the body of varistors with a shrinkable plastic tube, or by providing this stack with a layer of synthetic resin.
- a synthetic resin formed for example of epoxy resin, polymer concrete, silicone resin, or an elastomer
- DE-A-0 898 603 have proposed to produce the envelope surrounding the stack of varistors in composite materials composed of fibers, generally glass fibers impregnated with resin.
- document US-A-4 656 555 proposed to first form a winding of fibers based on plastic material, such as polyethylene, or glass, or even ceramic possibly impregnated with resin, for example l epoxy, then to form on the outside of this winding a housing made of weather resistant polymeric material, for example based on elastomeric polymers, synthetic rubber, thermoplastic elastomers or EPDM.
- plastic material such as polyethylene, or glass
- resin for example l epoxy
- This document more specifically proposes either to preform the weather-resistant polymer housing, then to engage the stack of varistors provided with the winding of fibers in this housing, or to first form the winding of fibers on the stack of varistors, then make the housing of weather-resistant polymer material, by molding on the winding, projection of polymer on the winding or insertion of the stack of varistors provided with the winding in a polymer bath.
- first envelope, the second envelope and the external envelope can be placed successively on the stack of varistors, or the envelopes can be formed in reverse order.
- the envelope can be molded in situ based on synthetic resin or polymeric material.
- the document states that the shell can be preformed. This document also proposes to use a sheet of prepreg fibers.
- Document EP-A-0 304 690 proposes first of all to make a filament winding of glass fibers impregnated with resin, then to form on the outside of the winding a coating of elastomeric material of EPDM type, by injection.
- Document EP-A-0 355 479 proposes placing successively on the stack of varistors, first of all a barrier formed by a plastic film, for example based on propylene, then a winding of non-conductive filaments, and finally a weather-resistant elastomer housing.
- Document DE-A-0 898 603 proposed in fact from 1964 to use glass fibers impregnated with resin to wrap varistors. More recently, we have proposed in the document FR-A-2 698 736, a method of manufacturing a lightning arrester comprising the steps which consist in stacking varistors, forming a first envelope of composite material, on the stack of varistors, which first at least semi-rigid envelope has a constant external section, along its length, compensating in particular for the surface unevenness of the stack of varistors due to deviations in alignment and to the dispersions of the dimensions of varistors and placing an external envelope with fins on the first of composite material by extruding a substantially constant outer envelope on the first envelope, then by adding annular fins to the extruded outer envelope.
- step of forming an envelope of composite material consists in: - placing a fabric of fibers on the outside of the stack of varistors, in contact with this one,
- Enamelling varistors has so far been considered essential to improve the dielectric strength and incidentally constitute a chemical barrier vis-à-vis their immediate environment.
- enameling which generally contains a high proportion of lead, typically greater than 50%, leads to a major risk of environmental pollution, if precautions, inevitably expensive, are not taken at the manufacturing level. , recovery and / or recycling of used surge arresters.
- enameling which can only be carried out before stacking, therefore individually varistor by varistor, plays a significant part in the overall cost price of current surge arresters.
- the Applicant proposes, by the present invention, to improve the existing surge arresters.
- a main object of the present invention is to produce reliable surge arresters based on varistors, without requiring enameling.
- a more incidental object of the present invention is to further reduce the cost of known surge arresters.
- the present invention provides a method of manufacturing lightning arresters of the type comprising the steps which consist in:
- the method comprises the step of placing a bead of flexible, adhesive and dielectric material on the previously formed stack, facing the different interfaces between each pair of adjacent varistors.
- the present invention also relates to the lightning arresters obtained by the implementation of the above method.
- FIG. 1 to 4 attached schematically show the various successive stages of production of a lightning arrester according to a preferred embodiment of the present invention.
- the process for manufacturing surge arresters illustrated in FIGS. 1 to 4 appended comprises the steps consisting in:
- varistors 10 centered on a common axis 12 (possibly with interposition of spacers between at least some of the pairs of adjacent varistors 10), electrically conductive parts forming electrodes, and hereinafter referred to as cimblots 20, being disposed respectively on each end of the stack, then maintenance in axial compression of the assembly;
- annular beads 30 of a bonding / sealing agent depositing annular beads 30 of a bonding / sealing agent, on the stack thus formed opposite each interface defined at the level of the junction zone between two adjacent varistors 10 (see FIG. 1);
- the bonding / sealing agent 30 deposited on the interfaces of the stack of varistors 10 is a flexible, adhesive and dielectric material. It is advantageously an elastomer or a gel, for example based on silicone or equivalent.
- the varistors 10 are unglazed varistors.
- the varistors 10 can include a protective film of thin enamel intended to protect the varistors during the manufacturing process of the arrester, in particular in order to avoid any pollution of the varistors during the manufacturing process of the perfume.
- Conventional enamel layers typically have a thickness of the order of 100 ⁇ m.
- Such a protective film according to the present invention can typically have a thickness of the order of ⁇ A to 1/3 of this conventional thickness.
- the protective film can be removable, that is to say removed, once the risks of pollution become non-existent during the manufacturing process.
- the protective film is made of a lead-free material.
- the beads of material 30 preferably formed from silicone sealant allow:
- the cords 30 allow in a way to repair any possible defect at the edges of the varistors; the cords 30 of silicone sealant thus advantageously replace conventional enameling at the interfaces between the pairs of adjacent varistors;
- each bead 30 of silicone sealant has an axial width of approximately 5 mm and a comparable thickness, preferably less than 5 mm.
- the beads 30 are preferably deposited in the form of a single turn in a single-component silicone sealant, necessarily compatible with the material of the varistors 10 very advantageously formed based on zinc oxide. To this end, preferably, the material 30 does not contain acetic acid.
- nozzles are suitably offset or a dispensing nozzle 32 fixed in rotation but capable of being displaced axially cyclically with a pitch equal to the distance separating two cords 30, and the stack of varistors 10 and end cimblots 20 is kept animated in axial compression with a rotational movement around the axis 12.
- the material making up the beads 30 is formed from a silicone sealant sold by the company Dow Corning under the reference 7091.
- This silicone sealant has excellent adhesion without primer and a neutral polymerization base.
- This silicone sealant allows a temperature range of - 55 ° C to + 150 ° C, and ⁇ has an elongation of 500% and a dielectric strength of 16 kV per mm.
- the ribbon 40 of prepreg fabric preferably wound at 45 ° with 50% overlap preferably has a resin content of between a third and a half by mass.
- the prepreg fabric ribbon 40 consists of a fabric whose resin mass rate is of the order of 35% has a nominal mass of 470 g / m 2 and a reinforcing structure based on glass fibers having a nominal mass of 305 g / m 2 in a satin type structure 8.
- the bonding / sealing agent forming the beads 50 deposited on the composite tape 40 can be formed from the same material, preferably silicone sealant or equivalent, as that used to make the beads 30 and described above.
- the material 50 is chosen to have lubricant, adhesive, dielectric, and filling properties, in order to facilitate the engagement of the external envelope 60 to adhere perfectly thereto, ensure dielectric functions, and perfectly fill the interface between the composite coating 40 and the external envelope 60.
- the material 50 deposited on the composite coating 40 can optionally be placed in a helix. However, as illustrated in FIG. 3, preferably the material 50 is deposited in the form of annular beads.
- the material 50 is preferably deposited using several nozzles or a nozzle 32 fixed in rotation but displaced axially cyclically with a pitch equal to the distance separating two beads 50, and setting in rotation of the preformed assembly lightning arrester around axis 12.
- cords 50 are deposited respectively at the two ends of the stack to ensure complete filling of the surface irregularities between the composite tape 40 and the outer envelope 60, over the entire length of the arrester, as well as to guarantee a perfect seal of the arrester.
- the outer casing 60 of elastomer is an envelope with external annular fins making it possible to extend the line of flight on the outside of the arrester.
- the number of fins as well as their profile and spacings can vary depending on the requirements for resistance to pollution, and of course the nominal voltage of the arrester.
- annular fins are characterized by zones of greater rigidity at the level of its fins.
- outer envelope 60 as a conforming mold by radial compression of the body of the arrester during the polymerization step of the resin of the prepreg tape 40 makes it possible to obtain perfect adhesion between the different layers of internal materials and allows both to guarantee a good seal and the absence of partial radial discharge for the device.
- this polymerization step is carried out under axial compression at a temperature of the order of 130 ° C. and for a duration of the order of 1 h.
- the arrester obtained for the implementation of the aforementioned process comprises:
- varistors 10 preferably with zinc oxide, unglazed (or only coated with a fine lead-free and therefore non-polluting enamel film, used only to facilitate the manufacturing process of the varistors), possibly associated with one or more intermediate metal spacers, - a metal contact electrode 20 at each end,
- a composite coating 40 obtained by simple helical winding of a ribbon of fabric of glass fibers preimpregnated with synthetic resin, an outer envelope of elastomer 60, and
- the present invention does not is not limited to the particular embodiment which has just been described but extends in all variants in accordance with its spirit.
- the ribbon 40 of fabric of glass fibers pre-impregnated with synthetic resin can be deposited on the stack of varistors 10 provided with beads 30 of silicone sealant, not in a helix, but in the form of rings placed opposite of the interface between each pair of adjacent varistors.
- the resulting assembly is preferably further provided with an outer casing having good dielectric strength, for example based on a silicone overmolding, or else an envelope deposited by expansion then retraction, or a heat-shrinkable envelope.
- the ribbon 40 of prepreg fabric can be deposited both in the form of rings facing the connection interfaces between each pair of adjacent varistors, then a superimposed propeller as illustrated in Figure 2.
Landscapes
- Engineering & Computer Science (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Thermistors And Varistors (AREA)
- Insulating Bodies (AREA)
- Apparatuses And Processes For Manufacturing Resistors (AREA)
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9913270A FR2800903B1 (fr) | 1999-10-25 | 1999-10-25 | Parafoudre perfectionne a base de varistances electriques |
FR9913270 | 1999-10-25 | ||
PCT/FR2000/002930 WO2001031661A1 (fr) | 1999-10-25 | 2000-10-20 | Parafoudre perfectionne a base de varistances electriques |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1166287A1 true EP1166287A1 (fr) | 2002-01-02 |
EP1166287B1 EP1166287B1 (fr) | 2006-12-13 |
Family
ID=9551293
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP00971467A Expired - Lifetime EP1166287B1 (fr) | 1999-10-25 | 2000-10-20 | Procede de fabrication de parafoudres et parafoudre a base de varistances electriques |
Country Status (14)
Country | Link |
---|---|
US (1) | US7272885B2 (fr) |
EP (1) | EP1166287B1 (fr) |
CN (1) | CN1267940C (fr) |
AT (1) | ATE348393T1 (fr) |
AU (1) | AU1031701A (fr) |
BR (1) | BR0007455A (fr) |
CA (1) | CA2356383C (fr) |
DE (1) | DE60032345D1 (fr) |
ES (1) | ES2278636T3 (fr) |
FR (1) | FR2800903B1 (fr) |
PT (1) | PT1166287E (fr) |
TR (1) | TR200101835T1 (fr) |
WO (1) | WO2001031661A1 (fr) |
ZA (1) | ZA200104867B (fr) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8117739B2 (en) * | 2004-01-23 | 2012-02-21 | Cooper Technologies Company | Manufacturing process for surge arrester module using pre-impregnated composite |
US7653371B2 (en) | 2004-09-27 | 2010-01-26 | Qualcomm Mems Technologies, Inc. | Selectable capacitance circuit |
DE102005007146A1 (de) * | 2005-02-11 | 2006-08-24 | Siemens Ag | Verfahren zur Ummantelung eines Varistorblockes mit einer elektrisch isolierenden Umhüllung sowie Varistorblock für einen Überspannungsableiter |
FR2907365B1 (fr) * | 2006-10-20 | 2011-07-22 | Astrium Sas | Dispositif et procede de bobinage filamentaire de tubes de grande longueur et tubes de grande longueur realises par ce procede. |
BR112018069972A8 (pt) | 2016-09-28 | 2022-12-27 | Hitachi Energy Switzerland Ag | Para-raios e método de fabricação associado |
CN108439982B (zh) * | 2018-05-14 | 2021-06-15 | 济南大学 | 一种轴向复合负温度系数热敏陶瓷材料及其制备方法 |
RU2750827C1 (ru) * | 2020-12-01 | 2021-07-05 | Олег Станиславович Клюнин | Способ изготовления баллона высокого давления и устройство для пропитки армирующего материала связующим для его осуществления |
US11894166B2 (en) | 2022-01-05 | 2024-02-06 | Richards Mfg. Co., A New Jersey Limited Partnership | Manufacturing process for surge arrestor module using compaction bladder system |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3645784A (en) * | 1969-12-18 | 1972-02-29 | Sprague Electric Co | Vitreous enamel resistor |
US4100588A (en) * | 1977-03-16 | 1978-07-11 | General Electric Company | Electrical overvoltage surge arrester with varistor heat transfer and sinking means |
DK173921B1 (da) | 1986-01-29 | 2002-02-18 | Bowthorpe Ind Ltd | Elektrisk overspændingsafledningsindretning, fremgangsmåde og apparat til fremstilling samt en anvendelse af en sådan indretning |
SE456623B (sv) * | 1987-02-23 | 1988-10-17 | Asea Ab | Ventilavledare |
FR2619244B1 (fr) | 1987-08-06 | 1992-09-04 | Sediver Ste Europ Isolateurs V | Procede de fabrication d'un parafoudre et parafoudre obtenu par ce procede |
FR2646957B1 (fr) | 1989-05-12 | 1994-02-04 | Sediver Ste Europ Isolateurs Ver | Enveloppe etanche a base d'enroulement filamentaire, et parafoudre composite en faisant application |
US5366935A (en) | 1994-03-14 | 1994-11-22 | Hubbell Incorporated | Passivating coating for metal oxide varistors |
FR2747500B1 (fr) * | 1996-04-12 | 1998-06-26 | Soule Materiel Electr | Parafoudre perfectionne a base de varistances |
WO1997041573A1 (fr) * | 1996-04-26 | 1997-11-06 | Asea Brown Boveri Ab | Bloc varistor |
US5926356A (en) | 1997-07-29 | 1999-07-20 | Hubbell Incorporated | End terminals for modular electrical assemblies with pressure relief |
-
1999
- 1999-10-25 FR FR9913270A patent/FR2800903B1/fr not_active Expired - Fee Related
-
2000
- 2000-10-20 WO PCT/FR2000/002930 patent/WO2001031661A1/fr active IP Right Grant
- 2000-10-20 CN CN00802387.5A patent/CN1267940C/zh not_active Expired - Fee Related
- 2000-10-20 DE DE60032345T patent/DE60032345D1/de not_active Expired - Lifetime
- 2000-10-20 BR BR0007455-1A patent/BR0007455A/pt not_active Application Discontinuation
- 2000-10-20 CA CA002356383A patent/CA2356383C/fr not_active Expired - Fee Related
- 2000-10-20 TR TR2001/01835T patent/TR200101835T1/ unknown
- 2000-10-20 PT PT00971467T patent/PT1166287E/pt unknown
- 2000-10-20 AT AT00971467T patent/ATE348393T1/de not_active IP Right Cessation
- 2000-10-20 ES ES00971467T patent/ES2278636T3/es not_active Expired - Lifetime
- 2000-10-20 EP EP00971467A patent/EP1166287B1/fr not_active Expired - Lifetime
- 2000-10-20 AU AU10317/01A patent/AU1031701A/en not_active Abandoned
-
2001
- 2001-06-14 ZA ZA200104867A patent/ZA200104867B/xx unknown
-
2003
- 2003-10-23 US US10/690,829 patent/US7272885B2/en not_active Expired - Fee Related
Non-Patent Citations (1)
Title |
---|
See references of WO0131661A1 * |
Also Published As
Publication number | Publication date |
---|---|
ATE348393T1 (de) | 2007-01-15 |
ZA200104867B (en) | 2002-06-14 |
CA2356383C (fr) | 2009-01-20 |
EP1166287B1 (fr) | 2006-12-13 |
TR200101835T1 (tr) | 2002-04-22 |
BR0007455A (pt) | 2001-10-30 |
US7272885B2 (en) | 2007-09-25 |
AU1031701A (en) | 2001-05-08 |
PT1166287E (pt) | 2007-02-28 |
CA2356383A1 (fr) | 2001-05-03 |
ES2278636T3 (es) | 2007-08-16 |
CN1327598A (zh) | 2001-12-19 |
FR2800903A1 (fr) | 2001-05-11 |
DE60032345D1 (de) | 2007-01-25 |
FR2800903B1 (fr) | 2001-12-21 |
US20040111867A1 (en) | 2004-06-17 |
CN1267940C (zh) | 2006-08-02 |
WO2001031661A1 (fr) | 2001-05-03 |
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Legal Events
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