EP1145601B1 - Chambre assurant une exposition electromagnetique a chauffage ameliore - Google Patents

Chambre assurant une exposition electromagnetique a chauffage ameliore Download PDF

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Publication number
EP1145601B1
EP1145601B1 EP98963029A EP98963029A EP1145601B1 EP 1145601 B1 EP1145601 B1 EP 1145601B1 EP 98963029 A EP98963029 A EP 98963029A EP 98963029 A EP98963029 A EP 98963029A EP 1145601 B1 EP1145601 B1 EP 1145601B1
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EP
European Patent Office
Prior art keywords
electromagnetic
exposure chamber
cavity
dielectric
electromagnetic field
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP98963029A
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German (de)
English (en)
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EP1145601A1 (fr
Inventor
William T. Joines
J. Michael Drozd
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Industrial Microwave Systems LLC
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Industrial Microwave Systems LLC
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Publication of EP1145601A1 publication Critical patent/EP1145601A1/fr
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    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00—Heating by electric, magnetic or electromagnetic fields
    • H05B6/64—Heating using microwaves
    • H05B6/70—Feed lines
    • H05B6/701—Feed lines using microwave applicators
    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00—Heating by electric, magnetic or electromagnetic fields
    • H05B6/64—Heating using microwaves
    • H05B6/70—Feed lines
    • H05B6/705—Feed lines using microwave tuning

Definitions

  • This invention relates to electromagnetic energy and more particularly to providing uniform electromagnetic exposure.
  • microwave signals for applications in many industrial and medical settings
  • Some of these applications include using microwave power for. heat treating various materials, polymer and ceramic curing, sintering, plasma processing, and for providing catalysts in chemical reactions.
  • Also of interest is the use of microwaves for sterilizing various objects.
  • These applications require electromagnetic exposure chambers or enclosures with relatively uniform power distributions. Uniform power distributions within the chambers help to prevent "hot” or “cold” spots which may cause unnecessary destruction or waste of sample material.
  • Some of these applications also require that substances be passed through--rather than simply placed in--microwave chambers.
  • the prior art includes various attempts to achieve more uniform exposure of samples to microwave fields.
  • Commercial microwave ovens utilize "mode stirrers", which are essentially paddle wheels that help create multiple modes within a microwave chamber.
  • mode stirrers are essentially paddle wheels that help create multiple modes within a microwave chamber.
  • Many researchers have analyzed the use of multimode chambers for increasing uniformity of exposure. See Iskander et. al, FDTD Simulation of Microwave Sintering of Ceramics in Multimode Cavities, IEEE MICROWAVE THEORY AND TECHNIQUES, Vol. 42, No. 5, May 1994, 793-799.
  • Some have suggested that the limited power uniformity achievable by mode stirring at a single frequency may be enhanced by using a band of frequencies. See Lauf et. al, 2 to 18 GHz BroadbandMicrowave Heating Systems, MICROWAVE JOURNAL, Nov. 1995, 24-34.
  • a slab loaded structure has been used in a few limited applications as a microwave applicator. Specifically, a slab loaded guide has been tested for radiating microwaves into tissue-like samples. See G.P. Rine et. al, Comparison of two-dimensional numerical approximation and measurement of SAR in a muscle equivalent phantom exposed to a 915 MHZ slab-loaded waveguide, INT. J. HYPERTHERMIA, Vol. 6, No. 1, 1990, 213-225.
  • Such conductive substances e.g., any ionized moisture in paper that is passed through a chamber for drying
  • microwave systems are not in use at all due to the problems posed by nonuniform fields and the need for continually open access points.
  • medical tubing is still sterilized either by chemical baths or by electron beam radiation.
  • UV electron beam
  • Microwaves are less likely to structurally damage the tubing.
  • microwaves can achieve greater depth of penetration than UV radiation. Therefore, medical tubing is more permeable to microwaves than to UV radiation.
  • microwaves can kill organisms and help destroy and remove debris throughout the tubing. UV radiation can only kill organisms at or near the tubing's surface but not effectively remove debris.
  • microwave structures are not currently employed for pre-use sterilization of medical tubing.
  • WO 98/49870 discloses a method and apparatus for electromagnetic exposure of planar or other materials.
  • a diagonal slot compensates for the effects of signal attenuation along the propagation path.
  • Adjustably variable path lengths allow peaks and valleys of the electromagnetic field in one exposure segment to compensate for peaks and valleys in another exposure segment.
  • Dielectric slabs may be used to extend the peak field region between top and bottom conducting surfaces to allow for more uniform exposure of planar materials that have a significant thickness.
  • Specialized choke flanges prevent the escape of electromagnetic energy.
  • One or more rollers between exposure segments may be enclosed by an outer surface to prevent the escape of electromagnetic energy.
  • US 2,543,053 discloses an apparatus for concentrating radiant energy in a small space in order to subject a mass of material to extremes of heat.
  • the apparatus comprises a small radio-antenna mounted at one focus of an ellipsoidal vessel, the object to be heated being located at the other focus.
  • the vessel is metallic, so as to produce reflections at high-efficiency and to focus the reflected energy at the point of utilization.
  • US 3,843,861 discloses an apparatus for the treatment of thermally treatable goods, such as extruded, long-stringed profiles of rubber of synthetic material, which are guided in a continuous passage under the effect of microwave energy by a microwave-waveguide-channel, comprising a microwave-waveguide-channel designed as a ridge channel and operating with a low limit frequency for the vulcanization for an intensive thermo-treatment of extended profiles of rubber or synthetic material having a large cross-section.
  • US 4,999,469 discloses a test bonding apparatus comprising a rectangular waveguide having a first pair of spaced opposing side walls attached to an orthogonal pair of spaced opposing side walls which are relatively wider.
  • the waveguide includes an input portion, an intermediate bonding chamber portion and a terminating end portion which disposed in communication with one another. Coupled to the input portion is a microwave source and a coolant source for propagating consistently through the bonding chamber portion microwave energy having a predominant frequency associated with a predetermined wavelength, and a flow of coolant fluid.
  • the relatively wider side walls in the bonding chamber portion of the waveguide having disposed along their longitudinal centrelines respective aligned slots. Each of the slots has opposing longitudinal edges disposed adjacent open ends of respective quarter wavelength chokes which are supported externally of the waveguide.
  • a high impedance is established at each of the slots for preventing leakage of microwave energy therefrom.
  • an aligned pair of dielectric clamping plates are supported by respective dielectric grid-like structures which permit passage of microwave energy and coolant fluid longitudinally through the bonding chamber portion.
  • the terminating end portion is provided with a matched load for dissipating microwave energy and with a screened output aperture for permitting egress of heat carrying coolant fluid.
  • the present invention provides an electromagnetic exposure chamber for heating a substance, the chamber characterized by: an exterior conducting surface that has two substantially planar surfaces and an elliptical end, the elliptical end perpendicular to the two substantially planar surfaces, the exterior conducting surface forming an interior cavity; a first opening opposite the elliptical end for delivering an electromagnetic field to the interior cavity, the exterior conducing surface directing the electromagnetic field to a focal region of the interior cavity; and a second opening through each of the two substantially planar surfaces of the exterior conducting surface, the second opening being aligned with the focal region of the interior cavity.
  • the openings to the focal region allow sample material to be passed through this region of focused heating.
  • the present invention utilizes dielectric slabs to provide a relatively uniform electromagnetic field to a cavity between two or more dielectric slabs.
  • Each dielectric slab is a thickness equal to or nearly equal to a quarter of a wavelength of the electromagnetic field in the dielectric slab.
  • sample material is introduced into the cavity between the two dielectric slabs.
  • This sample material may be introduced through one or more openings in the dielectric slabs.
  • specialized choke flanges prevent the leakage of energy from this cavity.
  • FIG. 1 illustrates an electromagnetic exposure chamber in accordance with the present invention.
  • the electromagnetic exposure chamber 10 comprises an exterior surface 11 surrounding dielectric slabs 12 and 14.
  • Dielectric slabs 12 and 14 may be parallel or not parallel.
  • the exterior surface 11 and dielectric slabs 12 and 14 form a cavity 16.
  • the cavity 16 is filled with air or other dielectric material.
  • the cavity 16 is filled with Styrofoam to provide stability to the electromagnetic exposure chamber 10.
  • the electromagnetic exposure chamber has an opening 17 through which electromagnetic energy (not shown) is propagated.
  • the opening 17 may be attached to a traditional waveguide (not shown).
  • FIG 2. illustrates another electromagnetic exposure chamber in accordance with the present invention.
  • the electromagnetic exposure chamber 20 comprises an exterior surface 11 surrounding dielectric slabs 12, 13, 14, and 15.
  • Dielectric slabs 12 and 14 may be parallel or may not be parallel.
  • Dielectric slabs 13 and 15 may be parallel or may not be parallel.
  • the dielectric slabs 12, 13, 14, and 15 form cavity 16.
  • the electromagnetic exposure chamber 20 has an opening 17.
  • FIG 3. illustrates another electromagnetic exposure chamber in accordance with the present invention.
  • the electromagnetic exposure chamber 30 comprises an exterior surface 11 and dielectric slabs 12 and 14.
  • the exterior surface 11 has a continuous, curved side 18 such that the inside surface of said side is an elliptical surface with a focal region 19.
  • the dielectric slabs 12 and 14 and exterior surface 11 form a cavity 16.
  • the electromagnetic exposure chamber 30 has an opening 17.
  • Dielectric slabs 12 and 14 may be formed of titania (TiO 2 ) ( ⁇ r specified at 96.0 ⁇ 5%).
  • the exterior surface 11 is formed of a conducting material such as aluminum. It is important that the presence of air gaps be minimized at the interfaces between exterior surface 11 and dielectric slabs 12 and 14.
  • FIG. 4 illustrates a uniform electromagnetic field across a dimension of an electromagnetic exposure chamber in accordance with the present invention.
  • the magnitude of the electric field 42, 44, and 46 in FIG. 4 is illustrated by vector arrows pointing in the vertical direction.
  • the frequency of the electromagnetic wave (the operating frequency) can be 915 MHZ, 2.45 GHz, or any other frequency depending on the desired application.
  • the electromagnetic exposure chamber is designed for and operated at the same frequency (i.e., the operating frequency is equal to the design frequency).
  • the electromagnetic exposure chamber is designed such that the thickness t of slabs 12 and 14 are each equal to a 1/4 of the wavelength of the electromagnetic field 42 and 44 in the slabs 12 and 14.
  • a 1/4 wavelength is the distance between a point in the mode where the magnitude of the electric field is equal to zero and the next nearest point in the mode where the magnitude of the electric field is at a maximum.
  • FIG. 5 illustrates, if the thickness t of slab 12 or 14 is slightly greater than ⁇ /4, the peak of the electric field occurs within the slab 12 or 14 rather than at the edge of slab 12 or 14.
  • FIG. 6 illustrates, if the thickness t of slab 12 or 14 is slightly less than X/4, then the peak of the electric field within cavity 16 exceeds the magnitude of the field at the edge 43 or 45 of the cavity 16, but is still relatively uniform across the cavity 16.
  • FIG. 5 and FIG. 6 illustrate a relatively uniform electromagnetic field in a cross section of an electromagnetic exposure chamber in accordance with the present invention. Therefore, the phrase "equal to a 1/4 of a wavelength" is hereinafter intended to mean equal to or about equal to a 1/4 of a wavelength.
  • An advantage of the present invention is that the electric field is at a maximum at the inside edge 43 or 45 of the dielectric slab 12 or 14 (the outside edges of the cavity 16) and is uniform (or nearly uniform) throughout the cavity 16.
  • the usable volume of the cavity is increased.
  • the peak of the electromagnetic field is wider.
  • the peak of the electromagnetic field is narrow. That is, the magnitude of the electromagnetic field significantly decreases at the outside edges 43 and 45 of the cavity 16.
  • the electromagnetic exposure chamber should also be designed and operated such that the electromagnetic wave is in a singular mode.
  • the best way to ensure that the electromagnetic wave is in a singular mode is to limit the overall width w. (Width w combines the width of the cavity 16 and the thicknesses t of the dielectric slabs 12 and 14).
  • the width of the cavity 16 (and hence cavity 16's usable volume) will be maximized by minimizing the width of the dielectric slabs 12 and 14. It will be appreciated by those skilled in the art that a 1/4 of a wavelength at a given frequency is relatively smaller in a material that has a relatively large dielectric constant. Therefore, the width of the cavity 16 is maximized if the relative dielectric constant of the dielectric slabs 12 and 14 is increased. In sum, if the dielectric constant of the slabs is increased, the thickness t of the dielectric slabs 12 and 14 is decreased and the width of the cavity 16 is increased.
  • the overall width w should be equal to or less than 2t[1 + ( ⁇ r1 / ⁇ r2 - 1) 1/2 ], where E r1 is the dielectric constant of the dielectric slabs 12 and 14, E r2 is the dielectric constant of the material in the cavity 16, and 2t is the combined thickness of the dielectric slabs 12 and 14.
  • FIG. 5 illustrates a relatively uniform electromagnetic field in a cross section of an electromagnetic exposure chamber in accordance with the present invention.
  • the electromagnetic exposure chamber should be designed and operated at near the same frequency. If the electromagnetic exposure chamber is operated at above the design frequency (or if the dielectric slabs 12 and 14 are built too thick), the magnitude at the edge 43 or 45 of the cavity 16 is no longer at a maximum.
  • the field shown in FIG. 5 occurs if the electromagnetic exposure chamber is operated at a frequency slightly greater than the design frequency.
  • the peak of the electric field occurs within the slab 12 or 14 rather than at the edge 43 or 45 of the slab 12 or 14.
  • the electric field 46 in the cavity 16 will exhibit a slight downward bow but will still be relatively uniform across the cavity 16.
  • FIG. 6 illustrates another relatively uniform electromagnetic field in a cross section of an electromagnetic exposure chamber in accordance with the present invention.
  • the field shown in FIG. 6 occurs if the electromagnetic exposure chamber is operated at a frequency slightly less than the design frequency (or if the dielectric slabs are built too thin).
  • the peak of the electric field 46 within the cavity 16 exceeds the magnitude of the electric field at the edge 43 or 45 of the cavity 16, but is still relatively uniform across the cavity 16.
  • the electromagnetic exposure chamber is operated at well above the design frequency (or if width w is too wide), the electromagnetic wave will no longer be in its singular mode. However, if width w is less than 2t[1 + ( ⁇ r1 / ⁇ r2 - 1) 1/2 ], the electromagnetic field will still be in its singular mode.
  • FIG 7 illustrates a choke flange 71 appropriate for a circular opening 70.
  • Choke flange 71 may consist of a hollow or dielectrically filled conducting structure. Choke flange 71 is shorted to the exterior conducting surface 11 at a distance d of ⁇ /4 from the outer perimeter of the opening 70. ⁇ /4 is measured with reference to the value of ⁇ r of the material inside the hollow or dielectrically filled choke flange 71. Although ideally the distance d should be equal to ⁇ /4, choke flange 71 will still operate in accordance with the present invention if d is slightly greater or slightly less than ⁇ /4.
  • FIG. 8 illustrates a choke flange 81 adapted to a rectangular opening 80.
  • the choke flange 81 may consist of a hollow or dielectrically filled structure that is either in the shape of a rectangle (not shown), a piecewise simulation of a rectangle 81 only, or a modified rectangle 81 and 82 with rounded comers 82.
  • the modified rectangle 81 and 82 with rounded comers 82 can be formed from a single piece of metal or separate pieces of metal. In the case of separate pieces of metal, the separate pieces of metal may have gaps therebetween.
  • the choke flange 81 is shorted to the exterior conducting surface 11 at a distance d of ⁇ /4 from the outer perimeter of opening 80.
  • ⁇ /4 is measured with reference to the value of ⁇ r of the material inside the conducting structure 81.
  • the distance d may be slightly greater or slightly less than ⁇ /4. Losses from opening 80's comers will typically be negligible. If desired, however, these negligible losses may be further eliminated by designing choke flange 81 to include rounded comers 82 of radius d short circuited at a distance d equal to or nearly equal to ⁇ /4 from opening 80's corners.
  • opening/choke flange combinations will depend on the application.
  • the choice of choke flange shape will depend on the opening shape which in turn will depend in part on the shape of the substance to be introduced into cavity 16.
  • FIG. 9 illustrates an exemplary embodiment of the present invention that is particularly useful for sterilizing tubing and other applications.
  • a side 18 of exterior conducting surface 11 is formed in an elliptical shape.
  • the elliptical shape of side 18 reflects the electromagnetic field to a focal region 19.
  • a circular opening 70 is at a distal end of the focal region 19.
  • a substance, such as tubing, may then be introduced into the focal region 19 of cavity 16 for exposure to a relatively uniform electromagnetic field.
  • the embodiment illustrated in FIG. 9 is well adapted for sterilizing test tubes, or other elongated objects.
  • a single mode electromagnetic field may be delivered to the cavity by means well known in the art.
  • the field should be polarized so that the electric field is oriented perpendicular to the longitudinal axis of the focal region.
  • a tapered (i.e. gradually increasing in width) waveguide (not shown) is used to deliver the electromagnetic wave (not shown) from a traditional waveguide (not shown) to the opening 17 of the electromagnetic exposure chamber.
  • the width of the cavity 16 will exceed that of the waveguide.
  • the dielectric slabs 12 and 14 extend into the horned waveguide in which case the dielectric slabs 12 and 14 are not parallel. If the dielectric slabs 12 and 14 are not parallel, this increases the usable volume of the cavity 16 and elongates the focal region 19.
  • This embodiment and other embodiments are also useful for sintering.
  • Sintering often requires the heating of substances with relatively high melting points. Microwave heating offers the possibility that the heating times required for sintering may be significantly reduced.
  • a substance to be sintered must be heated relatively evenly to permit even densification and to avoid cracking.
  • RTP rapid thermal processing
  • semiconductor wafers require relatively uniform, but rapid, heating.
  • the present invention enables enhanced field uniformity for helping to promote more uniform thin-film deposition in the context of semiconductor processing and in other thin-film deposition contexts.

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  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Constitution Of High-Frequency Heating (AREA)
  • Apparatus For Disinfection Or Sterilisation (AREA)
  • Resistance Heating (AREA)

Claims (8)

  1. Chambre d'exposition électromagnétique (10) pour chauffer une substance, la chambre étant caractérisée par :
    une surface conductrice extérieure (11) qui possède deux surfaces substantiellement planes et une extrémité elliptique (18), l'extrémité elliptique étant perpendiculaire aux deux surfaces substantiellement planes, la surface conductrice extérieure formant une cavité intérieure (16);
    une première ouverture (17) opposé à l'extrémité elliptique pour délivrer un champ électromagnétique dans la cavité intérieure, la surface conductrice extérieure dirigeant le champ électromagnétique vers une région focale (19) de la cavité intérieure; et
    une deuxième ouverture respective (70; 80) à travers chacune des deux surfaces substantiellement planes de la surface conductrice extérieure, les deuxièmes ouvertures étant alignées avec la région focale de la cavité intérieure.
  2. Chambre d'exposition électromagnétique selon la revendication 1, caractérisée en outre par deux plaques diélectriques (12, 14), chaque plaque s'étendant depuis l'une opposée des deux surfaces substantiellement planes dans la cavité intérieure d'une distance approximativement égale à 1/4 d'une longueur d'onde du champ électromagnétique.
  3. Chambre d'exposition électromagnétique selon l'une quelconque des revendications précédentes, caractérisée en outre par une bride d'arrêt respectif (71; 81) s'étendant radialement depuis chaque deuxième ouverture.
  4. Chambre d'exposition électromagnétique selon la revendication 3, caractérisée en outre par un périmètre extérieur de la bride d'arrêt qui est espacé sélectivement d'un périmètre extérieur de la deuxième ouverture d'une distance approximativement égale à 1/4 d'une longueur d'onde du champ électromagnétique.
  5. Chambre d'exposition électromagnétique selon la revendication 4, dans laquelle la bride d'arrêt est reliée à la surface conductrice extérieure pour créer un court-circuit au niveau du périmètre extérieur de la bride d'arrêt et un circuit ouvert au niveau de la deuxième ouverture.
  6. Chambre d'exposition électromagnétique selon l'une quelconque des revendications précédentes, dans laquelle la deuxième ouverture permet l'introduction continue d'une substance dans la cavité intérieure.
  7. Chambre d'exposition électromagnétique selon la revendication 6, dans laquelle les deuxièmes ouvertures permettent à la substance de se déplacer le long de la région focale à travers la cavité intérieure.
  8. Chambre d'exposition électromagnétique selon la revendication 1, comprenant en outre un court-circuit pour contenir un champ électromagnétique.
EP98963029A 1998-12-16 1998-12-16 Chambre assurant une exposition electromagnetique a chauffage ameliore Expired - Lifetime EP1145601B1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/US1998/026215 WO2000036879A1 (fr) 1998-12-16 1998-12-16 Chambre assurant une exposition electromagnetique a chauffage ameliore

Publications (2)

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EP1145601A1 EP1145601A1 (fr) 2001-10-17
EP1145601B1 true EP1145601B1 (fr) 2005-05-04

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EP98963029A Expired - Lifetime EP1145601B1 (fr) 1998-12-16 1998-12-16 Chambre assurant une exposition electromagnetique a chauffage ameliore

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EP (1) EP1145601B1 (fr)
JP (1) JP2002532864A (fr)
AT (1) ATE295060T1 (fr)
AU (1) AU771172B2 (fr)
CA (1) CA2355152C (fr)
DE (1) DE69830083T2 (fr)
WO (1) WO2000036879A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20070111446A (ko) 2004-11-12 2007-11-21 노쓰 캐롤라이나 스테이트 유니버시티 식품 및 다른 바이오물질을 열처리하는 방법 및 장치그리고 그에 따라 제조된 생산품
GB2468901A (en) * 2009-03-26 2010-09-29 E2V Tech Microwave Oven

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2543053A (en) * 1947-12-01 1951-02-27 Int Standard Electric Corp Radiant energy high-temperature heating apparatus
US3843861A (en) * 1971-05-04 1974-10-22 Menschner Textil Johannes Wave guide channel operating with micro-wave energy
US4999469A (en) * 1990-04-02 1991-03-12 Raytheon Company Apparatus for microwave heating test coupons

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3769480D1 (de) * 1986-01-16 1991-05-29 Micro Denshi Co Ltd Mikrowellenheizvorrichtung.
US5958275A (en) * 1997-04-29 1999-09-28 Industrial Microwave Systems, Inc. Method and apparatus for electromagnetic exposure of planar or other materials

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2543053A (en) * 1947-12-01 1951-02-27 Int Standard Electric Corp Radiant energy high-temperature heating apparatus
US3843861A (en) * 1971-05-04 1974-10-22 Menschner Textil Johannes Wave guide channel operating with micro-wave energy
US4999469A (en) * 1990-04-02 1991-03-12 Raytheon Company Apparatus for microwave heating test coupons

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Publication number Publication date
AU1814199A (en) 2000-07-03
WO2000036879A1 (fr) 2000-06-22
ATE295060T1 (de) 2005-05-15
AU771172B2 (en) 2004-03-18
DE69830083T2 (de) 2005-10-06
CA2355152A1 (fr) 2000-06-22
DE69830083D1 (de) 2005-06-09
EP1145601A1 (fr) 2001-10-17
JP2002532864A (ja) 2002-10-02
CA2355152C (fr) 2008-07-22

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