EP0924008A1 - Production rapide d' articles de forme complexe par moulage de précision à la cire perdue - Google Patents

Production rapide d' articles de forme complexe par moulage de précision à la cire perdue Download PDF

Info

Publication number
EP0924008A1
EP0924008A1 EP98310605A EP98310605A EP0924008A1 EP 0924008 A1 EP0924008 A1 EP 0924008A1 EP 98310605 A EP98310605 A EP 98310605A EP 98310605 A EP98310605 A EP 98310605A EP 0924008 A1 EP0924008 A1 EP 0924008A1
Authority
EP
European Patent Office
Prior art keywords
cores
casting
wax
assembly
core
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP98310605A
Other languages
German (de)
English (en)
Other versions
EP0924008B1 (fr
Inventor
Furqan Zafar Shaikh
Bryan Christopher Stoll
Joseph Carl Schim
Neal James Corey
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ford Global Technologies LLC
Original Assignee
Ford Global Technologies LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ford Global Technologies LLC filed Critical Ford Global Technologies LLC
Publication of EP0924008A1 publication Critical patent/EP0924008A1/fr
Application granted granted Critical
Publication of EP0924008B1 publication Critical patent/EP0924008B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D29/00Removing castings from moulds, not restricted to casting processes covered by a single main group; Removing cores; Handling ingots
    • B22D29/001Removing cores
    • B22D29/003Removing cores using heat
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22CFOUNDRY MOULDING
    • B22C7/00Patterns; Manufacture thereof so far as not provided for in other classes
    • B22C7/02Lost patterns
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22CFOUNDRY MOULDING
    • B22C9/00Moulds or cores; Moulding processes
    • B22C9/02Sand moulds or like moulds for shaped castings
    • B22C9/04Use of lost patterns

Definitions

  • This invention relates to rapidly fabricating a run of functional durable parts having hollow complex interiors, and more particularly to making such parts using easily formed and easily removable resin bonded sand or salt cores.
  • Non-durable plastic prototypes of complex parts have become commonplace; techniques such as stereolithography or cubital prototyping have been used where a non-functional plastic part is fashioned but limited in what can be done with such plastic part.
  • Such plastic parts can be used to evaluate aesthetic aspects or fit and assembly of the design, but cannot be subjected to evaluation tests that require harsh operating conditions or high temperatures such as that needed to evaluate an internal combustion engine head or block.
  • a method of repetitively forming rapid prototype metal castings that are fully durable and functional metal parts of a complex shape, comprising the steps of: (a) making an assembly of resin-bonded particulate cores spaced from each other, one core arcuately encompassing at least one end of another core to define at least one hidden space therebetween; (b) making an easily machined die set to receive and support said assembly of cores in spaced relation for defining a casting cavity around and between said cores, including said at least one hidden space; (c) injecting fluidised wax into said cavity under a controlled sustained pressure to fill said cavity without entrapping gases and to form a wax pattern for the casting; (d) using said wax pattern with said assembly of cores therein to form a shell mould thereabout and thence draining the wax from the mould to permit a metal casting to be formed in place of the wax pattern with the assembly of cores still in place, and (e) removing from the casting all of the particulate cores in said casting by reversing the
  • the present invention provides rapid fabrication of complex hollow metal castings, such as engine heads, blocks, manifolds and transmission cases.
  • This invention has an advantage that it provides a method for rapidly making up to 100,000 castings of a complex hollow part using the same aluminium die sets, the produced parts being fully durable and functional parts with the method combining the rapid core making and core removal capabilities of resin bonded sand or salt cores and the rapid pattern making capabilities of the lost wax investment casting technique.
  • This method allows for extreme ease and economy for modifying the interior flow characteristics of an engine head without need for changing the exterior shape of such head, leading to nimble manufacturing of engine families.
  • the process of this invention does not require expensive repetitive machining of several slabs or laminations each time a single pattern is to be made, as in stratiform rapid prototyping (best suited cost-wise to making three or less prototypes) and does not require machining eight or more sets of steel dies to create moulds for each exterior or interior sand core characteristic (best suited to making hundreds of thousands of castings to justify the cost).
  • the process herein described allows for faster and easier economic fabrication of 4-40,000 (even up to 100,000) castings by requiring machining of fewer die sets from aluminium metal or equivalent material; the die sets are limited to four: three for making non-fused resin bonded core elements, and one for making the wax pattern. This process combines the faster core making capabilities of particulate bonded cores and the repetitively faster pattern making of the lost wax investment technique.
  • an assembly or family 10 of particulate bonded cores is formed to define passages within an internal combustion engine head; the assembly here consists of three intake cores 11, three exhaust cores 12 and an annular water jacket core 13.
  • the assembly is unique because it does not comprise fused ceramic cores normally required to withstand the hydrostatic forces of fluid wax, but rather bonded particulate salt or sand cores capable of withstanding the controlled injected wax of this invention as well as molten metal.
  • the intake passage core 11 is shown as having an enlarged common intake end 14 and a bifurcated end 15 to define two intake ports; such core, as well as the exhaust cores, are formed by blowing particles mixed with resin binder into a two-way two-piece die set that defines the core shape.
  • the formed cores when cured, will have a modulus of rupture of 2500-3200 psi, a bulk density of about 1.92 g/cc, and a porosity of about 26%.
  • a die set 18 is made to define a pattern or casting cavity 34 around the core assembly 10 (see Figures 2-4 and 8-13).
  • Die set 18, as well as the die sets for the cores, are made of aluminium or other material that is easily machined.
  • the exhaust passage core 12 is a curved single body having an outlet end 16 designed to be keyed into the die side part 20 of die set 18 for supporting such end and has another core end 17 designed to be supported on the base die part 19 on a wall 25 that defines the shape of the combustion chamber.
  • Figure 2 illustrates how one of the intake cores 11 is supported on the die set 18 (the die set 18 being comprised, as shown in Figure 3, of a base part 19 left side part 20, a top part 21a, another top part 21b, and end parts 22, 23).
  • the other end 14 of such core is keyed at 28 into a groove formed into both side and base die parts.
  • the annular water jacket core 13 has a primary longitudinally extending wall 26 which extends between the rows of intake and exhaust cores; annular webs or walls 27, 28 extend from wall 26 and wrap around such respective cores while spaced therefrom.
  • Core walls 27 are much thicker than walls 28 because they define water channels adjacent the exhaust port which demands greater heat extraction.
  • the ends of water jacket wall 26 have core extensions 29, 30 to define passages that connect the water jacket to a fluid circulating system.
  • Core 13 thus provides annular walls around each intake and exhaust core, but in spaced relation. The space therebetween can be quite thin - as little as 3-4 mm.
  • cores 11 and 12 have one end within and arcuately encompassed by the annular webs 27 or 28 and have another end that curvingly projects around and to the outside of such web walls. This creates a spaced relationship that defines hidden spaces or gaps 31 and 32 therebetween. Such thin spaces promote increased heat transfer to the water jacket when replaced by metal, such as aluminium, in the final casting. Such thin spaces have heretofore presented a difficult problem to accurately form with pattern material.
  • Inlets 33 for injecting hot fluid wax into casting cavity 34 is shown in Figure 4 as step three of the process.
  • the cavity 34 also includes spaces 39 opposite the inlets to allow for complete filling by the wax.
  • the interior cavity does not need to have any draft angles or relief tapers incorporated.
  • Hot wax is injected under a controlled injection pressure between 300-500 psi with the wax at a temperature in the range of 130-140°F.
  • the wax is preferably a mineral base pattern wax or any investment casting was.
  • An injection apparatus 35 is utilised to force the wax into the ingate 36 and through the plurality of inlets 33, which are sized to a diameter of about one half inch.
  • the injection of hot wax is sustained at such pressure for a time period of about 120-240 seconds until all of the wax fills the voids in the cavity 34 without entrapment of any gases.
  • the wax typically will become solidified in a period of 120-300 seconds because of the heat sink provided by the aluminium die assembly.
  • the injection apparatus 35 after appropriate formation of a skin on the wax pattern 37, is removed and the ingate 36 is separated. After the wax pattern 37 has solidified to a sufficient condition, the parts 19-23 of the die set 18 are separated from the wax pattern 37; the wax pattern 37 still retains the bonded particulate cores 11, 12 and 13, which can be seen at the pattern surface where the cores intersect the exterior of the wax pattern.
  • a shell mould 40 is formed about the wax pattern 37 containing the core assembly 10 as step four of the process.
  • the mould 40 is created by multiple dipping of the pattern into a ceramic slurry 38, draining the excess slurry, applying a refractory stucco, and drying or gelling the coating. This is repeated until a shell of about .3 inches or greater is achieved.
  • the slurry preferably consists of a ceramic flour in colloidal silica which forms a layer 41 that is then sprinkled with a fine sand. After drying, the stuccoed silica/ceramic layer mould is then dipped into another ceramic slurry and then into a fluidised bed containing granular molochite to thereby stucco the surface again to form other layers 42.
  • the slurry may be composed of refractory binders and refractory fillers or solids.
  • the refractory binders can be silica sols, ethyl silicate, sodium and potassium silicate and gypsum type plasters.
  • Common refractory fillers that can be used in the process are silica, fused silica, zircon, and aluminium silicate.
  • the stucco in many cases, is the same type of refractory as the dip coat, but it has a much larger grain size. The stucco is applied to the wet surface of the slurry to provide a mechanical key for the next coating and to minimise the drying stresses in the slurry coating, thus preventing cracking of the coating.
  • the slurries are kept in suspension by use of a continually rotating drum with paddle mixture arrangement or by use of pneumatic prop mixers.
  • the primary coat is most important to ensure that good surface finish and details are obtained; subsequent coats are used to build the shell thickness and strength in order to withstand de-waxing and metal pressures.
  • the stucco is applied either by raining or by using a fluidised bed. In the raining process, stucco particles are allowed to fall in a raindrop pattern using a diffuser. Fluidised beds use a vertical drum with a porous brick bottom; air at low pressure and high volume passes through the brick and up the bed of stucco material.
  • the effect of this air flow is to impart fluid characteristics to the stucco bed allowing the pattern assembly to be immersed in the stucco material as if it were a liquid. Fine stucco is used for the first coating and second coating, while coarser stuccos are used for backup coats.
  • Drying of the shell 40 is important; it begins with applying at constant velocity, temperature and humidity to remove the surface binder liquid (a constant rate drying). This is followed by a falling rate drying period which results in capillary transfer of the binder liquid from inside of the shell to the surface.
  • Control of humidity and temperature is important. Temperature control affects pattern expansion and contraction which can cause the shell to crack.
  • Humidity is preferably controlled to 50% and air velocity is controlled to 60-1200 ft/min.
  • the wax pattern 37 is removed from the layered shell mould 40 by shock firing, steam autoclaving, or other heating technique, which drains the wax through suitable drain openings 50 in the shell. Once the wax is removed, leaving the part cavity 34 vacant, molten metal, such as aluminium, is poured into the cavity 34, as part of step four, through a sprue 51, to produce the required cast object, such as the finished cylinder head 43 shown in figure 7.
  • Removal (melting) of the pattern 37 is done during the mould firing cycle.
  • the strength of the solid mould must be adequate to withstand the expansion stresses of the wax pattern.
  • the wax pattern material then burns off in the firing furnace.
  • Firing is carried out in an oxidised environment so that no carbon is left on the mould surface and may be accomplished by several techniques including autoclaving, flash firing and microwave de-waxing.
  • Shell firing is then carried out after the moulds are de-waxed to increase the mould strength, along with heating and removing of residual pattern material prior to the final operation of pouring the metal.
  • the moulds are heated in an oxidised atmospheric condition to a temperature of 1600-2000°F depending upon specific foundry requirements.
  • Firing and preheat temperatures depend on the shell material and the type of material being poured. Aluminium castings typically are poured at a heated shell temperature of 400-600°F and steel at 1600-2000°F. The metal is poured slowly into the hot shell without causing turbulence. While the shell is heated to a temperature of 400°F, as described earlier, metal (1200°F for aluminium 356) is poured through the gating system to fill up the cavities and the risers. The metal is then left to cool in atmospheric conditions. In the case of a cylinder head, a chill may be used to draw heat away from the relatively large sections of the cylinder head.
  • the final casting 43 still retains the particulate bonded cores therein which can now easily be removed as step five by subjecting the casting to a heat treatment cycle; the resin or other bonding agent, holding the particulates together, is reversed so that the sand or salt becomes freeflowing and easily pours from the openings, such as 46-49 of the casting, by gravity (as shown in Figure 7).
  • Such heat treatment may also be employed to concurrently treat the aluminium metal to enhance its metallurgical characteristics. It is important to keep in mind that cleaning the casting of core material is not carried out by use of hammers or salt baths, but rather by simple use of inquiescent water at 62°F that completely dissociates the bonded cores in less than 12 minutes. Hotter or pressurised water will further reduce dissolution time.
  • the described process also promotes economical nimble manufacturing of a family of engine heads or blocks. Only new sets of cores need be made to change the flow characteristics of a head or block, the exterior configuration defined by the pattern die set 18 can remain the same and continue to be used to make up to at least 100,000 wax patterns for different members of an engine family. This is a significant economic breakthrough.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Molds, Cores, And Manufacturing Methods Thereof (AREA)
EP98310605A 1997-12-22 1998-12-22 Production rapide d' articles de forme complexe par moulage de précision à la cire perdue Expired - Lifetime EP0924008B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US99592897A 1997-12-22 1997-12-22
US995928 1997-12-22

Publications (2)

Publication Number Publication Date
EP0924008A1 true EP0924008A1 (fr) 1999-06-23
EP0924008B1 EP0924008B1 (fr) 2003-09-10

Family

ID=25542347

Family Applications (1)

Application Number Title Priority Date Filing Date
EP98310605A Expired - Lifetime EP0924008B1 (fr) 1997-12-22 1998-12-22 Production rapide d' articles de forme complexe par moulage de précision à la cire perdue

Country Status (4)

Country Link
EP (1) EP0924008B1 (fr)
JP (1) JPH11244994A (fr)
CA (1) CA2254505A1 (fr)
DE (1) DE69817989T2 (fr)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1600230A1 (fr) * 2004-04-15 2005-11-30 United Technologies Corporation Procédé d'élaboration d'un moule de coulée de précision
EP1764170A1 (fr) * 2005-09-13 2007-03-21 United Technologies Corporation Methode de destruction d'un modèle perdu de coulée
CN102019354A (zh) * 2010-12-27 2011-04-20 沈阳黎明航空发动机(集团)有限责任公司 带冠超薄细长叶片的定向凝固方法
CN103084541A (zh) * 2013-01-31 2013-05-08 贵州英吉尔机械制造有限公司 一种气缸盖铸件的成形工艺
CN103273010A (zh) * 2013-05-06 2013-09-04 无锡山发精铸科技有限公司 轻型燃气轮机用细晶整铸涡轮的近净形铸造方法
CN103372630A (zh) * 2012-04-25 2013-10-30 河北瑞丰动力缸体有限公司 一种发动机缸体的消失模生产工艺
CN104475680A (zh) * 2014-11-15 2015-04-01 柳州金特机械有限公司 一种精密铸造缸头的方法
CN105705274A (zh) * 2013-09-04 2016-06-22 尼玛克股份有限公司 将由轻金属熔液铸造的铸件从铸模中脱模的方法
CN106583658A (zh) * 2016-12-14 2017-04-26 江西腾勒动力有限公司 发动机缸体铸造砂芯及应用所述铸造砂芯铸造缸体的方法
CN108607953A (zh) * 2018-07-04 2018-10-02 纽威工业材料(大丰)有限公司 一种阀盖蜡模整体成形模具
CN114406190A (zh) * 2021-12-28 2022-04-29 东营一诚精密金属有限公司 一种保证熔模铸造盲孔同轴度的工艺方法

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005001023A1 (de) * 2005-01-07 2006-07-20 Fev Motorentechnik Gmbh Zylinderkopfkühlmantel
CN110666100A (zh) * 2019-10-12 2020-01-10 成都铁城精密铸造有限公司 一种形成熔模复杂内腔的成型工艺
CN113426953A (zh) * 2021-07-02 2021-09-24 洛阳刘氏模具有限公司 消失模内腔水道气道复合造型铸造工艺

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2053047A (en) * 1979-07-07 1981-02-04 Rolls Royce Cores for lost wax casting
EP0092690A1 (fr) * 1982-04-22 1983-11-02 Nissan Motor Co., Ltd. Noyau de moulage pour la coulée d'un bloc-cylindres de moteur
US5140869A (en) * 1989-07-31 1992-08-25 Ford Motor Company Hollow connecting rod
US5577550A (en) * 1995-05-05 1996-11-26 Callaway Golf Company Golf club metallic head formation

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2053047A (en) * 1979-07-07 1981-02-04 Rolls Royce Cores for lost wax casting
EP0092690A1 (fr) * 1982-04-22 1983-11-02 Nissan Motor Co., Ltd. Noyau de moulage pour la coulée d'un bloc-cylindres de moteur
US5140869A (en) * 1989-07-31 1992-08-25 Ford Motor Company Hollow connecting rod
US5577550A (en) * 1995-05-05 1996-11-26 Callaway Golf Company Golf club metallic head formation

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1600230A1 (fr) * 2004-04-15 2005-11-30 United Technologies Corporation Procédé d'élaboration d'un moule de coulée de précision
EP1764170A1 (fr) * 2005-09-13 2007-03-21 United Technologies Corporation Methode de destruction d'un modèle perdu de coulée
US7240718B2 (en) 2005-09-13 2007-07-10 United Technologies Corporation Method for casting core removal
CN102019354A (zh) * 2010-12-27 2011-04-20 沈阳黎明航空发动机(集团)有限责任公司 带冠超薄细长叶片的定向凝固方法
CN103372630A (zh) * 2012-04-25 2013-10-30 河北瑞丰动力缸体有限公司 一种发动机缸体的消失模生产工艺
CN103372630B (zh) * 2012-04-25 2017-07-04 河北瑞丰动力缸体有限公司 一种发动机缸体的消失模生产工艺
CN103084541A (zh) * 2013-01-31 2013-05-08 贵州英吉尔机械制造有限公司 一种气缸盖铸件的成形工艺
CN103273010A (zh) * 2013-05-06 2013-09-04 无锡山发精铸科技有限公司 轻型燃气轮机用细晶整铸涡轮的近净形铸造方法
CN105705274A (zh) * 2013-09-04 2016-06-22 尼玛克股份有限公司 将由轻金属熔液铸造的铸件从铸模中脱模的方法
CN105705274B (zh) * 2013-09-04 2017-07-25 尼玛克股份有限公司 将由轻金属熔液铸造的铸件从铸模中脱模的方法
CN104475680A (zh) * 2014-11-15 2015-04-01 柳州金特机械有限公司 一种精密铸造缸头的方法
CN106583658A (zh) * 2016-12-14 2017-04-26 江西腾勒动力有限公司 发动机缸体铸造砂芯及应用所述铸造砂芯铸造缸体的方法
CN108607953A (zh) * 2018-07-04 2018-10-02 纽威工业材料(大丰)有限公司 一种阀盖蜡模整体成形模具
CN108607953B (zh) * 2018-07-04 2024-01-30 纽威工业材料(大丰)有限公司 一种阀盖蜡模整体成形模具
CN114406190A (zh) * 2021-12-28 2022-04-29 东营一诚精密金属有限公司 一种保证熔模铸造盲孔同轴度的工艺方法

Also Published As

Publication number Publication date
DE69817989D1 (de) 2003-10-16
EP0924008B1 (fr) 2003-09-10
JPH11244994A (ja) 1999-09-14
DE69817989T2 (de) 2004-05-19
CA2254505A1 (fr) 1999-06-22

Similar Documents

Publication Publication Date Title
EP0924008B1 (fr) Production rapide d' articles de forme complexe par moulage de précision à la cire perdue
US6626230B1 (en) Multi-wall core and process
US5296308A (en) Investment casting using core with integral wall thickness control means
US20130221192A1 (en) Interchangeable mold inserts
EP1752237B1 (fr) Appareil et procédé de moulage à la cire perdue pour la fabrication de chenal de coulée
US5616293A (en) Rapid making of a prototype part or mold using stereolithography model
US20130220572A1 (en) Molding assembly with heating and cooling system
EP3558561B1 (fr) Procédé de moulage mettant en oeuvre des techniques combinées
CN107309406A (zh) 采用组合式3d打印壳模的铸造方法及该方法中使用的组合式壳模
CN111112552A (zh) 基于3d打印技术的精密铸造成型方法
AU2005269595A1 (en) Method of removing a fugitive pattern from a mold
US8567477B2 (en) Mold core for forming a molding tool
US6110602A (en) Method of making a three-dimensional object
CN110102711B (zh) 铸钢件成型工艺铸型的制造方法
CN101850401A (zh) 一种熔模及利用该熔模的精密铸造工艺
US8627876B2 (en) Molding tool with conformal portions and method of making the same
CN111730029B (zh) 一种基于3d打印的精密铸造方法
GB2253400A (en) Casting mould
CN115319022A (zh) 一种生产液压柱塞泵泵盖铸件的铸造方法
JPS63313628A (ja) 熱可塑性発泡体から成る金属鋳造用模型
JPS6030549A (ja) 細孔を有する鋳物の製造法
CN113600745B (zh) 一种利用光固化快速成型消失模进行负压铸造铸件产品的方法
JPH0237937A (ja) 細口中空部を有する鋳物の精密鋳造方法
CN114761151A (zh) 铸造模具、制造该模具的方法以及铸造方法
CN118543788A (zh) 大型风力发电机组主轴铸件的铁型铸型结构及其制作工艺

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): DE ES GB

AX Request for extension of the european patent

Free format text: AL;LT;LV;MK;RO;SI

RIN1 Information on inventor provided before grant (corrected)

Inventor name: COREY, NEAL JAMES

Inventor name: SCHIM, JOSEPH CARL

Inventor name: STOLL, BRYAN CHRISTOPHER

Inventor name: SHAIKH, FURQAN ZAFAR

17P Request for examination filed

Effective date: 19991029

AKX Designation fees paid

Free format text: DE ES GB

17Q First examination report despatched

Effective date: 20021017

GRAH Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOS IGRA

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): DE ES GB

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

RIN1 Information on inventor provided before grant (corrected)

Inventor name: COREY, NEAL JAMES

Inventor name: SCHIM, JOSEPH CARL

Inventor name: STOLL, BRYAN CHRISTOPHER

Inventor name: SHAIKH, FURQAN ZAFAR

REG Reference to a national code

Ref country code: GB

Ref legal event code: 732E

REF Corresponds to:

Ref document number: 69817989

Country of ref document: DE

Date of ref document: 20031016

Kind code of ref document: P

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: GB

Payment date: 20031124

Year of fee payment: 6

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20031221

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20031230

Year of fee payment: 6

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed

Effective date: 20040614

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20041222

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20050701

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20041222