EP0761310B1 - Method and installation for milling and sifting of material - Google Patents

Method and installation for milling and sifting of material Download PDF

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Publication number
EP0761310B1
EP0761310B1 EP96111417A EP96111417A EP0761310B1 EP 0761310 B1 EP0761310 B1 EP 0761310B1 EP 96111417 A EP96111417 A EP 96111417A EP 96111417 A EP96111417 A EP 96111417A EP 0761310 B1 EP0761310 B1 EP 0761310B1
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EP
European Patent Office
Prior art keywords
mill
classifier
gas
line
coolant
Prior art date
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Expired - Lifetime
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EP96111417A
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German (de)
French (fr)
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EP0761310A1 (en
Inventor
Oliver Dietrich
Wilfried Duesberg
Manfred Stahl
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Messer Griesheim GmbH
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Messer Griesheim GmbH
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Publication of EP0761310A1 publication Critical patent/EP0761310A1/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/18Adding fluid, other than for crushing or disintegrating by fluid energy
    • B02C23/24Passing gas through crushing or disintegrating zone
    • B02C23/32Passing gas through crushing or disintegrating zone with return of oversize material to crushing or disintegrating zone
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods
    • B02C19/18Use of auxiliary physical effects, e.g. ultrasonics, irradiation, for disintegrating
    • B02C19/186Use of cold or heat for disintegrating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/18Adding fluid, other than for crushing or disintegrating by fluid energy
    • B02C23/20Adding fluid, other than for crushing or disintegrating by fluid energy after crushing or disintegrating
    • B02C23/22Adding fluid, other than for crushing or disintegrating by fluid energy after crushing or disintegrating with recirculation of material to crushing or disintegrating zone
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S241/00Solid material comminution or disintegration
    • Y10S241/14Grinding in inert, controlled atmosphere
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S241/00Solid material comminution or disintegration
    • Y10S241/37Cryogenic cooling

Definitions

  • the invention relates to a method for grinding and classifying regrind according to the preamble of claim 1 and one for implementation device suitable for the method.
  • DE-PS 38 33 830 C2 shows a device of the applicant for the Production of extremely fine dusts with particle sizes down to less than 10 Micrometer in which a classifier is integrated.
  • EP 0 044 507 A1 describes a process in which labels are applied to plastic parts Views are separated.
  • EP 0 317 935 B1 there is a device shown in which the cold gas emerging from a mill by a Cyclone is freed from particles.
  • DE-OS 23 18 549 that is Cold grinding ground material is classified by a sieving device.
  • the writings mentioned in the prior art relate either others rely on the production of extremely fine dusts Based on tasks.
  • EP 0 044 507 A1 does not refer to particle size but separated according to material properties.
  • EP 0 610 162 A2 describes a device for cryogenic decomposition and screening of solid waste, in which the waste by Brittle contact with a cryogenic coolant, crushed in a mill and then into individual components using a view is classified.
  • the classifiers are in a closed pneumatic Cycle arranged and with a dry carrier medium operated. This prevents water from getting on the cooled Regrind condensed.
  • the invention is therefore based on the object, a method and a To create device with which the production of fine goods cost-saving and can be carried out with less time.
  • the feed is via a Hopper 1 placed on a screw conveyor 2, which is the feed feeds to a rotary valve 4 via a metal separator 3, the one cooling screw 5, which is injected 6 with liquid Coolant is filled with the feed.
  • the exit the cooling screw 5 is connected to a mill 8 via the line 7, whose outlet 9 is connected to a funnel 10, which leads into a rotary valve 11.
  • From the cellular wheel sluice 11 leads a connection 12 to the line 13, which in an external Sifter 14 opens.
  • a line 15 branches from the classifier 14 with a rotary valve 16, which opens into the funnel 1 and serves to return Kochkom.
  • Another line 17 is used for Removal of the fine material and opens into a cyclone 18, the output side is equipped with a rotary valve 19.
  • Line 20 which has a valve 21 and a blower 22 leads back into the line 13.
  • a line 23 which with is equipped with a valve 24 and in the fine material chamber 25 of the Classifier 14 opens.
  • a line branches from line 20 26, which via a valve 27 and a filter 28 into a rotary valve 29 as well as the surroundings.
  • On the funnel 10 is a line 31 connected to a filter 32 which is gaseous Coolant returns to line 7.
  • Branch off from line 31 the lines 33 and 34, which are equipped with the valves 35 and 36 are.
  • Line 34 is connected to line 20, line 33 leads to the surroundings.
  • the feed material is now transferred to the screw conveyor via the hopper 1 2 abandoned, which the feed material over the metal separator 3 introduces into the rotary valve 4, which is the feed of Cooling screw 5 feeds.
  • the liquid coolant in this case liquid nitrogen, entered into the cooling screw 5.
  • the feed material is cooled and embrittled. That on this way pretreated feed is through line 7 fed to the mill 8, which crushes the feed material. That on this Way crushed in the vaporized liquid nitrogen gas stream Regrind is via the outlet 9, the hopper 10 and the rotary valve 11 fed from which the shredded via the connection 12 Grist in the cold gas stream is conveyed into the classifier 14.
  • the Device is along the route from mill 8 via the exit 9, the funnel 10, the rotary valve 11 and the connection 12 sealed gas-tight to the environment. This is a Entry of ambient air and the associated moisture are excluded.
  • the shredded regrind gets into the cold gas stream of the Coolant via line 13 in the classifier 14, in which the oversize is separated from the fines.
  • the overcomer arrives via line 15 and the rotary valve 16 back into the hopper 1.
  • the fine goods will conveyed via line 17 into a cyclone 18 in which it is from the cold gas stream separated and discharged via the rotary valve 19.
  • the remaining cold gas passes through line 20 via the blower 22 in the form of a circuit again in line 13, which it again fed to the sifter.
  • line 20 can via the 30th continue to supply liquid nitrogen, which evaporates in line 20 to avoid any loss of cold gas within the classifier circuit to compensate.
  • the gas stream is passed through a filter 28 which is the cold gas of particles emerging from the filter polluting the environment could be liberated.
  • the separated particles can can be separated and collected via a rotary valve 29.
  • the funnel 10 also branches off in a gastight fashion Line 31, which leads through the filter 32, which in turn occurs Separates particles.
  • the gas stream emerging from the filter, which is a has low temperature, can continue in the cycle line 31 can be returned to line 7 for total consumption to reduce liquid nitrogen as a coolant.
  • excess cold gas can be supplied via line 33 to the Valve 35 is equipped to be released to the environment. It is also possible, the classifier circuit through line 34, which with the Valve 36 is equipped with additional cold gas from the grinding process supply by feeding the cold gas into line 20 possible cycle gas losses in the closed classifier circuit to compensate.
  • the classifier gas cycle is narrower and only includes the fine chamber of the classifier, the line 17 with the cyclone 18, the Line 20 with the blower 22 and the line return 23 with the valve 24.

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  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Disintegrating Or Milling (AREA)
  • Crushing And Grinding (AREA)
  • Combined Means For Separation Of Solids (AREA)
  • General Preparation And Processing Of Foods (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)

Abstract

The grinding and sifting process involves passing the material through a coolant and grinding it in a mill (8). The ground material is then taken to a sieve (14) designed to keep out the ambient air, and in particular the moisture in it. This is done in a closed process. The sieve is supplied with the same gas coolant as the mill so that losses from the sieve gas circuit can easily be made good. The upper portion left on the sieve is fed back to the mill. There is a line on the output side of the mill which leads back to the input side.

Description

Die Erfindung betrifft ein Verfahren zum Mahlen und Sichten von Mahlgut nach dem Oberbegriff des Anspruches 1 sowie eine für die Durchführung des Verfahrens geeignete Vorrichtung.The invention relates to a method for grinding and classifying regrind according to the preamble of claim 1 and one for implementation device suitable for the method.

Nach dem Stand der Technik wird beim Kaltmahlen zu zerkleinerndes Mahlgut, insbesondere Kunststoff, durch Kühlen mit einem Kühlmittel versprödet und zur Zerkleinerung einer Mühle zugeführt. Das zerkleinerte Mahlgut verläßt die Mühle in kaltem Zustand, wird aufgefangen und zwischengelagert, wobei eine Anpassung der Temperatur des Mahlgutes an die Umgebungstemperatur erfolgt. Während dieser Lagerung kann sich an dem Mahlgut gebildete Elektrostatik abbauen. Um die sich anschließende Sichtung des Mahlgutes zu verbessern, wird in vielen Fällen ein Trennmittel hinzugefügt. Dieses wird dem Mahlgut untergemischt. Beim Sichten wird das Überkom vom Feingut getrennt und kann dem Mahlprozeß erneut zugeführt werden. Während sich die Temperatur des Mahlgutes bei der Zwischenlagerung der Umgebungstemperatur anpaßt, kondensiert Wasser aus der Umgebungsluft an den Partikeln des Mahlgutes. Hierdurch wird die Sichtfähigkeit des Mahlgutes sehr eingeschränkt. Auf ein zwischenzeitliches Trocknen und ein Hinzufügen von Trennmitteln kann daher für die Sichtung beim bisherigen Kaltmahlen nicht verzichtet werden. Die damit verbundenen Arbeitsschritte sind Zeit- und Kostenaufwendig. According to the state of the art, what is to be comminuted during cold grinding Regrind, especially plastic, by cooling with a coolant embrittled and fed to a mill for comminution. The crushed Grist leaves the mill in a cold state, is collected and temporarily stored, with an adjustment of the temperature of the ground material to the ambient temperature. During this storage electrostatics formed on the regrind can degrade. To the itself subsequent sighting of the regrind is improved in many A release agent is added to cases. This is mixed into the regrind. When sifting, the commodity is separated from the fines and can be fed to the grinding process again. While the temperature the ground material during the intermediate storage of the ambient temperature adapts, water from the ambient air condenses on the particles of the regrind. This makes the ground material very visible limited. Interim drying and adding of separating agents can therefore be used for the screening in previous cold grinding not be waived. The work steps involved are Time and cost consuming.

So muß die Produktion von Feingut für die Dauer der Zwischenlagerung unterbrochen werden und es entstehen Kosten für den Einsatz von Trennmittel und den damit verbundenen Arbeitsaufwand.So the production of fine goods for the duration of the intermediate storage be interrupted and there are costs for the use of Release agent and the work involved.

Die DE-PS 38 33 830 C2 zeigt eine Vorrichtung der Anmelderin für die Herstellung extrem feiner Stäube mit Teilchengrößen bis zu kleiner 10 Mikrometer, in die ein Sichter integriert ist. Die EP 0 044 507 A1 beschreibt ein Verfahren, bei dem Etiketten von Kunststoffteilen durch Sichten abgetrennt werden. In der EP 0 317 935 B1 ist eine Vorrichtung dargestellt, in der das aus einer Mühle austretende Kaltgas durch einen Zyklon von Partikeln befreit wird. In der DE-OS 23 18 549 wird das durch Kaltmahlen zerkleinerte Mahlgut durch eine Siebeinrichtung klassiert. Die im Stand der Technik genannten Schriften beziehen sich entweder auf die Herstellung von extrem feinen Stäuben oder ihnen liegen andere Aufgaben zugrunde. So wird in der EP 0 044 507 A1 nicht nach Teilchengröße sondern nach Materialeigenschaft getrennt.DE-PS 38 33 830 C2 shows a device of the applicant for the Production of extremely fine dusts with particle sizes down to less than 10 Micrometer in which a classifier is integrated. EP 0 044 507 A1 describes a process in which labels are applied to plastic parts Views are separated. In EP 0 317 935 B1 there is a device shown in which the cold gas emerging from a mill by a Cyclone is freed from particles. In DE-OS 23 18 549 that is Cold grinding ground material is classified by a sieving device. The writings mentioned in the prior art relate either others rely on the production of extremely fine dusts Based on tasks. For example, EP 0 044 507 A1 does not refer to particle size but separated according to material properties.

Aus der EP 0 610 162 A2 ist eine Einrichtung zur kryogenen Zerlegung und Sichtung von festen Abfällen vorbekannt, bei dem der Abfall durch Kontakt mit einem kryogenen Kühlmittel versprödet, in einer Mühle zerkleinert und anschließend mittels Sichtem in einzelne Komponenten klassiert wird. Die Sichter sind in einem geschlossenen pneumatischen Kreislauf angeordnet und werden mit einem trockenen Trägermedium betrieben. Hierdurch wird verhindert, dass Wasser an dem gekühlten Mahlgut kondensiert.EP 0 610 162 A2 describes a device for cryogenic decomposition and screening of solid waste, in which the waste by Brittle contact with a cryogenic coolant, crushed in a mill and then into individual components using a view is classified. The classifiers are in a closed pneumatic Cycle arranged and with a dry carrier medium operated. This prevents water from getting on the cooled Regrind condensed.

Der Erfindung liegt daher die Aufgabe zugrunde, ein Verfahren und eine Vorrichtung zu schaffen, mit denen die Produktion von Feingut kostensparend und mit geringerem Zeitaufwand durchgeführt werden kann. The invention is therefore based on the object, a method and a To create device with which the production of fine goods cost-saving and can be carried out with less time.

Ausgehend von dem im Oberbegriff des Anspruchs 1 berücksichtigten Stand der Technik ist die Aufgabe erfindungsgemäß gelöst mit dem im kennzeichnenden Teil des Anspruchs 1 angegebenen Merkmalen.Starting from that considered in the preamble of claim 1 State of the art, the object is achieved with the im characterizing part of claim 1 specified features.

Mit dem erfindungsgemäßen Verfahren und der Vorrichtung ist es nunmehr möglich, Feingut in einem geschlossenen Prozeß und ohne Zwischenlagerung zu produzieren. In der Mühle anfallendes gasförmiges Kühlmittel kann gleichzeitig für den Sichterkreislauf eingesetzt werden. It is now with the method and the device according to the invention possible, fine material in a closed process and without intermediate storage to produce. Gaseous gas accumulating in the mill Coolant can also be used for the classifier circuit.

Vorteilhafte Weiterbildungen der Erfindung sind in den Unteransprüchen angegeben.
Die Zeichnungen veranschaulichen eine Vorrichtung zur Durchführung des erfindungsgemäßen Verfahrens in schematischer Form.
Advantageous developments of the invention are specified in the subclaims.
The drawings illustrate a device for carrying out the method according to the invention in schematic form.

Es zeigen:

Figur 1:
Eine Vorrichtung bei der ein Sichter an eine Mühle an geschlossen ist,
Figur 2:
eine Abwandlung der Vorrichtung in Figur 1.
Show it:
Figure 1:
A device in which a classifier is connected to a mill,
Figure 2:
a modification of the device in Figure 1.

In der in Figur 1 dargestellten Vorrichtung wird das Aufgabegut über einen Trichter 1 auf eine Förderschnecke 2 aufgegeben, welche das Aufgabegut über einen Metallabscheider 3 einer Zellenradschleuse 4 zuführt, die eine Kühlschnecke 5, welche durch eine Eindüsung 6 mit flüssigem Kühlmittel beschickt wird, mit dem Aufgabegut gefüllt. Der Ausgang der Kühlschnecke 5 ist über die Leitung 7 mit einer Mühle 8 verbunden, deren Ausgang 9 mit einem Trichter 10 in Verbindung steht, welcher in eine Zellenradschleuse 11 führt. Von der Zellenradschleuse 11 führt eine Verbindung 12 zu der Leitung 13, welche in einen externen Sichter 14 mündet. Vom Sichter 14 zweigt sich eine Leitung 15 mit einer Zellenradschleuse 16 ab, welche in den Trichter 1 mündet und zur Rückführung von Überkom dient. Eine weitere Leitung 17 dient zum Abführen des Feingutes und mündet in einen Zyklon 18, der ausgangsseitig mit einer Zellenradschleuse 19 ausgestattet ist. Die Leitung 20, die ein Ventil 21 und ein Gebläse 22 aufweist, führt wieder in die Leitung 13. Von der Leitung 20 zweigt sich eine Leitung 23 ab, welche mit einem Ventil 24 ausgestattet ist und die in die Feingutkammer 25 des Sichters 14 mündet. Weiterhin zweigt sich von der Leitung 20 eine Leitung 26 ab, welche über ein Ventil 27 und ein Filter 28 in eine Zellenradschleuse 29 sowie die Umgebung mündet. An der Leitung 20 befindet sich eine Zufuhr 30 für flüssiges Kühlmedium. An dem Trichter 10 ist eine Leitung 31 mit einem Filter 32 angeschlossen, welche gasförmiges Kühlmittel in die Leitung 7 rückführt. Von der Leitung 31 zweigen sich die Leitungen 33 und 34 ab, welche mit den Ventilen 35 und 36 ausgestattet sind. Leitung 34 steht mit der Leitung 20 in Verbindung, Leitung 33 führt in die Umgebung.In the device shown in Figure 1, the feed is via a Hopper 1 placed on a screw conveyor 2, which is the feed feeds to a rotary valve 4 via a metal separator 3, the one cooling screw 5, which is injected 6 with liquid Coolant is filled with the feed. The exit the cooling screw 5 is connected to a mill 8 via the line 7, whose outlet 9 is connected to a funnel 10, which leads into a rotary valve 11. From the cellular wheel sluice 11 leads a connection 12 to the line 13, which in an external Sifter 14 opens. A line 15 branches from the classifier 14 with a rotary valve 16, which opens into the funnel 1 and serves to return Überkom. Another line 17 is used for Removal of the fine material and opens into a cyclone 18, the output side is equipped with a rotary valve 19. Line 20, which has a valve 21 and a blower 22 leads back into the line 13. From the line 20 branches off a line 23, which with is equipped with a valve 24 and in the fine material chamber 25 of the Classifier 14 opens. Furthermore, a line branches from line 20 26, which via a valve 27 and a filter 28 into a rotary valve 29 as well as the surroundings. Located on line 20 there is a feed 30 for liquid cooling medium. On the funnel 10 is a line 31 connected to a filter 32 which is gaseous Coolant returns to line 7. Branch off from line 31 the lines 33 and 34, which are equipped with the valves 35 and 36 are. Line 34 is connected to line 20, line 33 leads to the surroundings.

In Figur 2 sind gleichen Vorrichtungsmerkmalen die selben Bezugszeichen zugeordnet. Sie zeigt eine Vorrichtung in der sich die Leitung 20 lediglich in die Leitungen 23 und 26 fortführt und das Einmünden der Leitung 20 in das Leitungsstück 13 entfällt. Die Zufuhr 30 mündet in die Leitung 23.In Figure 2, the same device features are the same reference numerals assigned. It shows a device in which the line 20 is located only continues in lines 23 and 26 and the confluence of Line 20 in the line section 13 is omitted. The feed 30 opens into the Line 23.

Bei Betrieb wird nun das Aufgabegut über den Trichter 1 auf die Förderschnecke 2 aufgegeben, welche das Aufgabegut über den Metallabscheider 3 in die Zellenradschleuse 4 einbringt, die das Aufgabegut der Kühlschnecke 5 zuführt. Über die Eindüsung 6 wird das flüssige Kühlmittel, in diesem Fall flüssiger Stickstoff, in die Kühlschnecke 5 eingegeben. Hierdurch wird das Aufgabegut gekühlt und versprödet. Das auf diese Art und Weise vorbehandelte Aufgabegut wird durch die Leitung 7 der Mühle 8 zugeführt, welche das Aufgabegut zerkleinert. Das auf diese Weise im Gasstrom des verdampften flüssigen Stickstoffes zerkleinerte Mahlgut wird über den Ausgang 9 dem Trichter 10 und der Zellenradschleuse 11 zugeführt, von der aus über die Verbindung 12 das zerkleinerte Mahlgut im Kaltgasstrom in den Sichter 14 gefördert wird. Die Vorrichtung ist entlang der Wegstrecke von der Mühle 8 über den Ausgang 9, den Trichter 10, die Zellenradschleuse 11 sowie der Verbindung 12 gegenüber der Umgebung gasdicht abgeschlossen. Hierdurch ist ein Eintritt von Umgebungsluft und der damit verbunden Feuchtigkeit ausgeschlossen. In dem in der Zeichnung dargestellten Beispiele ist die Förderung des gemahlenen Gutes in den Sichter 14 durch den Gasstrom des verdampfenden Kühlmittels durch die Leitung 12 gewährleistet. Jedoch ist es auch vorstellbar anstelle eines solchen Gasstromes als Treibmittel für die Förderung des zerkleinerten Mahlgutes auch andere Vorrichtungselemente wie beispielsweise eine weitere Förderschnecke einzusetzen. Das zerkleinerte Mahlgut gerät im Kaltgasstrom des Kühlmittels über die Leitung 13 in den Sichter 14, in dem das Überkorn vom Feingut getrennt wird. Das Überkom gelangt über die Leitung 15 und die Zellenradschleuse 16 in den Trichter 1 zurück. Das Feingut wird über die Leitung 17 in einen Zyklon 18 gefördert, in dem es vom Kaltgasstrom getrennt und über die Zellenradschleuse 19 abgeführt wird. Das verbleibende Kaltgas gelangt durch die Leitung 20 über das Gebläse 22 in Form einer Kreislaufführung erneut in die Leitung 13, die es erneut dem Sichter zugeführt. In die Leitung 20 kann über die Zufuhr 30 weiterhin flüssiger Stickstoff, welcher in der Leitung 20 verdampft, zugeführt werden, um eventuelle Kaltgasverluste innerhalb des Sichterkreislaufes zu kompensieren. Es ist auch möglich, einen Teilstrom des Kaltgases aus der Leitung 20 über die Leitung 23 mit dem Ventil 24 der Feingutkammer 25 des Sichters 14 zuzugeben. Eventuell im Sichterkreislauf anfallender Überdruck kann über die Leitung 26 mit dem Ventil 27 abgeführt werden. Hierzu wird der Gasstrom über ein Filter 28 geleitet, welches das aus dem Filter austretende Kaltgas von Partikeln welche die Umwelt belasten könnten befreit. Die abgetrennten Partikel können über eine Zellenradschleuse 29 ausgesondert und gesammelt werden. Von dem Trichter 10 zweigt sich ebenfalls gasdicht ausgebildet die Leitung 31 ab, welche über den Filter 32 führt, der wiederum anfallende Partikel abtrennt. Der aus dem Filter austretende Gasstrom, welcher eine niedrige Temperatur aufweist, kann im Kreislauf über die Weiterführung der Leitung 31 in die Leitung 7 rückgeführt werden um den Gesamtverbrauch an flüssigen Stickstoff als Kühlmittel zu reduzieren.During operation, the feed material is now transferred to the screw conveyor via the hopper 1 2 abandoned, which the feed material over the metal separator 3 introduces into the rotary valve 4, which is the feed of Cooling screw 5 feeds. The liquid coolant, in this case liquid nitrogen, entered into the cooling screw 5. As a result, the feed material is cooled and embrittled. That on this way pretreated feed is through line 7 fed to the mill 8, which crushes the feed material. That on this Way crushed in the vaporized liquid nitrogen gas stream Regrind is via the outlet 9, the hopper 10 and the rotary valve 11 fed from which the shredded via the connection 12 Grist in the cold gas stream is conveyed into the classifier 14. The Device is along the route from mill 8 via the exit 9, the funnel 10, the rotary valve 11 and the connection 12 sealed gas-tight to the environment. This is a Entry of ambient air and the associated moisture are excluded. In the examples shown in the drawing is the Conveying the ground material in the classifier 14 through the gas flow of the evaporating coolant guaranteed by line 12. However, it is also conceivable as instead of such a gas stream Blowing agents for the conveyance of the crushed ground material also others Device elements such as another screw conveyor use. The shredded regrind gets into the cold gas stream of the Coolant via line 13 in the classifier 14, in which the oversize is separated from the fines. The overcomer arrives via line 15 and the rotary valve 16 back into the hopper 1. The fine goods will conveyed via line 17 into a cyclone 18 in which it is from the cold gas stream separated and discharged via the rotary valve 19. The remaining cold gas passes through line 20 via the blower 22 in the form of a circuit again in line 13, which it again fed to the sifter. In line 20 can via the 30th continue to supply liquid nitrogen, which evaporates in line 20 to avoid any loss of cold gas within the classifier circuit to compensate. It is also possible to use a partial flow of the cold gas from line 20 via line 23 with the valve 24 of the Admit fine material chamber 25 of classifier 14. Possibly in the classifier circuit Any excess pressure can be via line 26 to the valve 27 are dissipated. For this purpose, the gas stream is passed through a filter 28 which is the cold gas of particles emerging from the filter polluting the environment could be liberated. The separated particles can can be separated and collected via a rotary valve 29. The funnel 10 also branches off in a gastight fashion Line 31, which leads through the filter 32, which in turn occurs Separates particles. The gas stream emerging from the filter, which is a has low temperature, can continue in the cycle line 31 can be returned to line 7 for total consumption to reduce liquid nitrogen as a coolant.

Alternativ kann überschüssiges Kaltgas über die Leitung 33, die mit dem Ventil 35 ausgestattet ist, an die Umgebung abgegeben werden. Es ist auch möglich, den Sichterkreislauf durch die Leitung 34, die mit dem Ventil 36 ausgestattet ist, mit weiterem Kaltgas aus dem Mahlprozeß zu versorgen, indem das Kaltgas in die Leitung 20 eingespeist wird um eventuelle Kreisgasverluste im ebenfalls geschlossenen Sichterkreislauf zu kompensieren.Alternatively, excess cold gas can be supplied via line 33 to the Valve 35 is equipped to be released to the environment. It is also possible, the classifier circuit through line 34, which with the Valve 36 is equipped with additional cold gas from the grinding process supply by feeding the cold gas into line 20 possible cycle gas losses in the closed classifier circuit to compensate.

In Figur 2 ist der Sichtergaskreislauf enger gefaßt und umfaßt lediglich die Feingutkammer des Sichters, die Leitung 17 mit dem Zyklon 18, die Leitung 20 mit dem Gebläse 22 sowie die Leitungsrückführung 23 mit dem Ventil 24.In Figure 2, the classifier gas cycle is narrower and only includes the fine chamber of the classifier, the line 17 with the cyclone 18, the Line 20 with the blower 22 and the line return 23 with the valve 24.

Mit dem erfindungsgemäßen Verfahren und der Vorrichtung ist es nunmehr möglich, in einem geschlossenen Ablauf, on-line, unter Fernhaltung von Umgebungsluft und der damit verbunden Luftfeuchtigkeit ohne weitere Zwischenschritte wie Temperieren, Trocknen und Zugabe von Trennmitteln, Feingut zu produzieren und zu sichten. Es kann daher in erheblichem Ausmaß Zeit und Kostenaufwand reduziert werden. Idealerweise wird das Verfahren mit flüssigem Stickstoff, welcher in dem Prozeß verdampft, betrieben werden. Jedoch ist es auch möglich, andere Kühlmittel, die ähnliche Eigenschaften haben, einzusetzen. Das Verfahren ist nicht auf die Anwendung von Prallmühlen beschränkt, vielmehr können auch andere Mühlen wie z. B. Mikrowirbelmühlen und Luftstrahlmühlen eingesetzt werden. Das aufgegebene Grobgut kann mit dem Verfahren und der Vorrichtung im wesentlichen bis auf 50 Mikrometer Teilchengröße in den Hauptanteilen zerkleinert werden. Mit dem erfindungsgemäßen Verfahren und der Vorrichtung wird der Eintritt von Luftfeuchtigkeit verhindert. Dadurch wird die Produktqualität verbessert und die nachfolgenden Trennstufen maßgeblich positiv beeinflußt, eine Trennmittelzugabe ist nicht erforderlich. Probleme die durch Elektrostatik entstehen, können unterbunden werden. Das zur Sichtung erforderliche Kreisgas wird dem vorgeschalteten Kaltmahlprozeß entnommen, so daß eine Doppelnutzung des Kühlmittels möglich ist. Für eine wirtschaftliche Betriebsweise ist ein Sichter 14 mit Sichtergaskreislauf erforderlich. Jedoch kann bei Vorliegen eines Sonderfalls das erfindungsgemäße Verfahren auch mit einem Sichten ohne Sichtergaskreislauf ausgeübt werden.It is now with the method and the device according to the invention possible, in a closed process, on-line, with remote control of ambient air and the associated humidity without further intermediate steps such as tempering, drying and adding Release agents to produce and sift fines. It can therefore be in considerable time and cost can be reduced. Ideally is the process with liquid nitrogen, which in the Process evaporated, operated. However, it is also possible for others Use coolants that have similar properties. The procedure is not limited to the use of impact mills, rather can also other mills such. B. micro vortex mills and Air jet mills are used. The coarse feed can with the method and the device essentially down to 50 micrometers Particle size can be crushed in the main proportions. With the method and the device according to the invention is the entrance prevented from humidity. This improves the product quality and has a significant positive influence on the subsequent separation stages, it is not necessary to add a release agent. Problems through Electrostatics can be prevented. That for sighting required cycle gas is taken from the upstream cold grinding process, so that the coolant can be used twice. For an economical mode of operation is a classifier 14 with a classifying gas circuit required. However, at The method according to the invention is also present in a special case a sighting without a sight gas cycle.

Im Falle der Verwendung von flüssigem Stickstoff als Kühlmittel werden dabei auch gleichzeitig beide Prozesse, das Mahlen und das Sichten unter dem Inertgas vorgenommen. Somit wird insbesondere bei Sauerstoff-empfindlichem Mahlgut die Explosionsgefahr eingeschränkt. Auf die bisher erforderlichen Schritte Mischen, Trennmittelzugabe und Zwischenlagern kann verzichtet werden; damit verbunden ist eine deutliche Reduzierung der Personal-, Betriebs- und Investitionskosten. Das in die Mahlanlage rückgeführte Überkorn ist bereits durch den Prozeßvorgang abgekühlt, wodurch der Verbrauch an Kühlmittel reduziert werden kann. Das Verfahren kann mit besonderem Vorteil im on-line Betrieb durchgeführt werden.In case of using liquid nitrogen as a coolant both processes at the same time, grinding and sifting made under the inert gas. This makes it especially sensitive to oxygen Regrind limits the risk of explosion. On the previously required steps of mixing, release agent addition and intermediate storage can be dispensed with; associated with this is a clear one Reduction of personnel, operating and investment costs. That in the Oversize material returned from the grinding plant is already through the process cooled, which can reduce the consumption of coolant. The method can be carried out with particular advantage in online operation become.

Claims (10)

  1. Method for milling and gas-classifying material which is to be milled, in which the material which is to be milled is made brittle by a coolant and is comminuted in a mill (8), the comminuted material being fed, in the absence of ambient air, to a gas classifier (14), in which the comminuted material is classified, characterized in that the gas classifier (14) is integrated in a classifier gas circuit, which is separate from the mill (8), the classifier gas circuit being operated with the coolant which was used to make the material brittle, and the comminuted material being fed into the gas classifier (14) in an atmosphere of gaseous coolant.
  2. Method according to Claim 1, characterized in that oversize material which is separated out in the gas classifier (14) is fed back to the mill (8).
  3. Method according to one of Claims 1 or 2, characterized in that some of the coolant used in the mill (8) is fed in the gaseous state to the classifier gas circuit, in order to compensate for gas losses and refrigeration losses in the classifier gas circuit.
  4. Method according to one of Claims 1 to 3, characterized in that some of the coolant used in the mill (8) is fed back to the mill (8) in the gaseous state.
  5. Method according to one of Claims 1 to 4, characterized in that the oversize material which has been separated out in the gas classifier (14) is fed back to the milling process in the cold state.
  6. Apparatus having a mill (8) for comminuting material which is to be milled, the mill (8) being assigned a gas classifier (14) which is in communication with the mill via means which allow the comminuted material to be passed into the gas classifier (14) without contact with ambient air, characterized in that the gas classifier is integrated in a classifier gas circuit which is separate from the mill (8) and at a line (20, 23) is in communication with the outlet side of the mill (8) through a line (34) which introduces gaseous coolant into the gas classifier circuit.
  7. Apparatus according to Claim 6, characterized in that the gas classifier (14) is in communication with the mill (8) via means which feed the oversize material to the mill (8).
  8. Apparatus according to one of Claims 6 or 7, characterized in that at the outlet side of the mill (8) there is a line (31) which is in communication with the inlet side of the mill (8).
  9. Apparatus according to one of Claims 6 to 8, characterized in that a filter (32) is integrated in the line (31) which branches off from the mill (8) on the outlet side.
  10. Apparatus according to one of Claims 6 to 9, characterized in that the line (20) of the classifier gas circuit is assigned a gas outlet which comprises a filter (28) with particle outlet.
EP96111417A 1995-09-07 1996-07-16 Method and installation for milling and sifting of material Expired - Lifetime EP0761310B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19533078A DE19533078A1 (en) 1995-09-07 1995-09-07 Method and device for grinding and classifying regrind
DE19533078 1995-09-07

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EP0761310A1 EP0761310A1 (en) 1997-03-12
EP0761310B1 true EP0761310B1 (en) 2002-10-09

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US (1) US5887803A (en)
EP (1) EP0761310B1 (en)
AT (1) ATE225684T1 (en)
BR (1) BR9603679A (en)
CA (1) CA2183175C (en)
DE (2) DE19533078A1 (en)
ES (1) ES2187594T3 (en)
HU (1) HU221131B1 (en)
MX (1) MX9603467A (en)

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DE10059442A1 (en) 2000-11-30 2002-06-13 Messer Griesheim Gmbh Device and method for producing fine material from chemically active regrind
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DE102011112741B4 (en) * 2011-09-07 2015-09-03 Werner Hofmann Inert gas covered closed grinding and screening plant
WO2014127206A2 (en) * 2013-02-15 2014-08-21 Ohio State Innovation Foundation Processing of harvested plant materials for extraction of biopolymers and related materials and methods
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CN107754980A (en) * 2017-12-08 2018-03-06 扬州天地源机电制造有限公司 A kind of electrodynamic type and the tablet disintegrating device effectively avoided waste
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HUP9602384A2 (en) 1997-05-28
DE59609772D1 (en) 2002-11-14
HU221131B1 (en) 2002-08-28
BR9603679A (en) 1998-08-25
EP0761310A1 (en) 1997-03-12
CA2183175A1 (en) 1997-03-08
MX9603467A (en) 1997-03-29
CA2183175C (en) 2005-10-18
DE19533078A1 (en) 1997-03-13
ES2187594T3 (en) 2003-06-16
HUP9602384A3 (en) 1998-06-29
ATE225684T1 (en) 2002-10-15
HU9602384D0 (en) 1996-10-28
US5887803A (en) 1999-03-30

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