Classifications

• • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
  • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
  • F25B—REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS
  • F25B9/00—Compression machines, plants or systems, in which the refrigerant is air or other gas of low boiling point
  • F25B9/12—Compression machines, plants or systems, in which the refrigerant is air or other gas of low boiling point using 3He-4He dilution

Definitions

• the present invention relates to a method and a device for obtaining very low temperatures, less than about 1 ° K, and in particular 0.1 C K.
• the document EP-A-0327.457 which corresponds to US-A-4,991,401 and which cites as inventor one of the authors of the present invention, describes a cryostat which comprises a mixing point in which a two-phase system comprising a solution phase of 3He in 4He liquid and a liquid phase formed of pure 3He. 3He and liquid 4He are continuously introduced into a mixing point separately, and the solution is extracted from the mixing point at a speed such that 3He cannot go back to raise the 3He content of 4He and consequently making it less capable of dissolving the liquid 3He introduced.
• a mixing point is placed in an enclosure brought to within 2 ° K.
• the two fluids by mixing create a two-phase system comprising a phase rich in 3He and a diluted phase, the energy of dilution or dissolution being used for cooling, the succession of the two phases in the mixture outlet tube prevents the diffusion of the 3He dissolved against the current in the cold part of the system, while at higher temperature (above 0.5 K), the solubility of 3He in the 4He increases, the mixture has only one single phase and the speed must be sufficient so that the 3He cannot diffuse against the current.
• This cryostat has the advantage of being able to operate in the absence of gravity because it does not include a distiller, which makes it particularly advantageous for space uses.
• the cryostat can operate by rejecting into space the small amounts of mixture of 4He and 3He that it produces. In case the vehicle has to return to the ground, this mixture can also be stored in a tank, with a view to distilling it on the ground. If the cryostat is used on land, it can, of course, be coupled with a distillation installation, the assembly then operating in a closed circuit.
• a difficulty encountered in the use of this cryostat results from the need to have a superfluid helium reservoir to maintain the enclosure at less than 2 ° K, which is a complication.
• the present invention aims to provide a cryostat operating according to the method described in EP-A-0327.457 and which has a simple construction, is space-saving, and consumes little energy, and more especially is freed from the need to produce and / or store superfluid helium to cool the enclosure to 2 ° K or less.
• the invention provides a process for obtaining very low temperatures according to which 4He and 3He are continuously introduced, which are cooled using heat exchangers at a temperature of the order of 0.2 ° K or less, at the point where they are mixed to absorb heat by diluting the 3He in 4He, thus cooling the closed two-phase mixture, which mixture is extracted through a conduit designed so that 3He cannot diffuse against the current and reduce the dissolution of 3He, a process in which an adjacent heat exchanger at the mixing point is used for cooling fluids going to the coldest point by the extracted mixture circulating in opposite directions, the main feature of this process being that the 4He and 3He intended to be mixed are cooled down to their temperature supply at a temperature below 2.5 ° K by exchange with the extracted mixture, the power being absorbed by the use of a Joule-Thomson expansion of this mixture, thus allowing the system to operate with a temperature of food well above 4 ° K.
• the cooling power during the Joule-Thomson expansion depends only on the inlet and outlet pressures of the mixture. The best performances are obtained for pressures of the order of 2 to 15 bars at the inlet and from 1 to 50 millibars at the outlet.
• FIG. 1 is a theoretical diagram of the installation of the prior art
• FIG. 2 is a theoretical diagram of an installation in accordance with the invention
• FIG. 3 is an enthalpy diagram of helium 4 on which the important points of the diagram of FIG. 2 have been transferred.
• Figure 1 shows the block diagram of a practical embodiment which operates in accordance with the indications of the document EP-A-0327.457 cited above.
• Pure 4He gas and 3He gas are injected under pressure (about 3 bars) and at room temperature, each in a heat exchanger 1, in contact with a superfluid helium reserve, symbolized in 2, which also carries the enclosure 3 of the cryostat, and are cooled to approximately 2 ° K.
• the two fluids are then cooled in a temperature exchanger 4, then the heat absorbed by their mixing in a mixing chamber 5 makes it possible to cool a support 6 to a temperature of the order of 0.1 ° K.
• the mixture M absorbs heat in the exchanger 4 before leaving the cryostat at an outlet pressure maintained at around 2 bars. The pressure difference with the inlet pressure is due to the pressure drop in the exchangers.
• the exchanger 4 comprises two parts, the hot part (0.5 ° K to 2 ° K) of 1 meter in length is composed of three tubes of 0.03 mm inside diameter, welded together, while that the cold part (0.1 ° K to 0.5 ° K) is formed by three tubes of 0.02 mm in diameter and 3 meters long welded together.
• FIG 2 is a schematic view of the device of Figure 1 modified according to the invention.
• the same references designate the same elements.
• Pure 4He and 3He gases are injected under pressure (between 2 and 20 bars) and at room temperature. They are then cooled to between 4 ° K and 10 ° K by exchangers 10, themselves coupled to an annex precooling machine 11. Penetrating into an external enclosure 13, the fluids are cooled to a temperature of the order of 2 ° K by the exchangers 12, themselves coupled to an intermediate enclosure 3. The interior of this enclosure is identical to that of FIG. 1.
• the mixture At the outlet of the exchanger 4, the mixture has undergone a pressure drop and is found at low pressure in an exchanger 14 where the liquid is evaporated, providing a large cooling power which is used to cool the screen limiting the enclosure 13, as well as the fluids entering through the exchangers 12.
• the mixture 11 then leaves the cryostat at low pressure (between 1 and 50 millibars) through a tube 15.
• FIG. 3 which represents an enthalpy diagram of helium 4, makes it possible to understand the physical aspect of the phenomena which occur inside the apparatus.
• This diagram relates to pure helium 4, while helium 4 and helium 3 are used either separately or as a mixture.
• the proportion of helium 3 compared to helium 4 is relatively low, around 20%, so that the diagram in Figure 3 still gives a fairly good idea of what sits.
• the enthalpy is 50 J / mole. If the outlet pressure is fixed at 30 millibars, the fluid retains its enthalpy and is found at point B at a temperature of 2 ° K, with a two-phase mixture half vapor, half liquid.
• the available cooling power is given by the difference in enthalpy between points B and C, ie about 50 J / mole. For a typical flow rate of 10 ⁇ moles / s, the power available on enclosure 3 is therefore 0.5 mW. For an inlet temperature above 7 ° K, the same reasoning leads to zero available power.
• the quantities of gas required are 1000 liters per year of helium 3 and 4000 liters per year of helium 4. If we use standard high pressure bottles (volume 5 liters, pressure 200 bars, weight 6.7 kg), the cryostat only needs one bottle of helium 3 and four bottles of helium 4 per year, which corresponds at 33.5 kg per year. This weight can be easily reduced by using high pressure cylinders made of more resistant materials.
• the simplicity of the system allows very simple control by adjusting the flow rates of the two fluids at the inlet of the cryostat. This allows the dilution to be stopped and restarted to optimize the consumption of helium gas.

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• Engineering & Computer Science (AREA)
• Physics & Mathematics (AREA)
• Mechanical Engineering (AREA)
• Thermal Sciences (AREA)
• General Engineering & Computer Science (AREA)
• Diaphragms For Electromechanical Transducers (AREA)
• Control Of Eletrric Generators (AREA)
• Glass Compositions (AREA)
• Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)

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• 1993
  • 1993-07-05 FR FR9308201A patent/FR2707375B1/fr not_active Expired - Fee Related
• 1994
  • 1994-07-04 RU RU96102156A patent/RU2117883C1/ru not_active IP Right Cessation
  • 1994-07-04 AT AT94921676T patent/ATE164441T1/de not_active IP Right Cessation
  • 1994-07-04 WO PCT/FR1994/000818 patent/WO1995002158A1/fr active IP Right Grant
  • 1994-07-04 US US08/578,656 patent/US5657635A/en not_active Expired - Fee Related
  • 1994-07-04 EP EP94921676A patent/EP0706632B1/de not_active Expired - Lifetime
  • 1994-07-04 JP JP50385195A patent/JP3304978B2/ja not_active Expired - Fee Related
  • 1994-07-04 DE DE69409236T patent/DE69409236T2/de not_active Expired - Fee Related

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