EP0658317B1 - Rod-shaped smoking article - Google Patents

Rod-shaped smoking article Download PDF

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Publication number
EP0658317B1
EP0658317B1 EP94115638A EP94115638A EP0658317B1 EP 0658317 B1 EP0658317 B1 EP 0658317B1 EP 94115638 A EP94115638 A EP 94115638A EP 94115638 A EP94115638 A EP 94115638A EP 0658317 B1 EP0658317 B1 EP 0658317B1
Authority
EP
European Patent Office
Prior art keywords
tobacco
smoking product
product according
sheet
leaf
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP94115638A
Other languages
German (de)
French (fr)
Other versions
EP0658317A3 (en
EP0658317A2 (en
Inventor
Peter Walter Kossmehl
Edgar Mentzel
Henning Dr. Seidel
Wolfgang Wildenau
Hans Noe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HF and PhF Reemtsma GmbH and Co
Original Assignee
HF and PhF Reemtsma GmbH and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE4334222A external-priority patent/DE4334222C3/en
Application filed by HF and PhF Reemtsma GmbH and Co filed Critical HF and PhF Reemtsma GmbH and Co
Publication of EP0658317A2 publication Critical patent/EP0658317A2/en
Publication of EP0658317A3 publication Critical patent/EP0658317A3/en
Application granted granted Critical
Publication of EP0658317B1 publication Critical patent/EP0658317B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/02Cigars; Cigarettes with special covers

Definitions

  • the invention relates to a rod-shaped smoke product with one strand - shaped core of shredded smoking tobacco, by one Jacket made from a paper manufacturing process Is surrounded by tobacco wraps.
  • tobacco wraps also called leaves from reconstituted tobacco, according to paper manufacturing processes e.g. according to US-A-4, 182, 349.
  • one is basically in one first stage stem of tobacco plant, tobacco stems and others at components of tobacco that cannot be used in cigarette production especially fine fractions but also tobacco leaves frayed and with, for example, heated water or other aqueous Liquids of certain temperatures mixed or washed out, after which the water-soluble Extract containing ingredients is subtracted; in a second stage, the cellulose components are optionally after further intermediate stages such as homogenization, repeated Screening or cleaning, along with fillers and others Addition after further intermediate stages on the sieve of one Given paper making device. On the so obtained The concentrated tobacco extract is applied to the raw film and this processed into the final tobacco foil.
  • tobacco films produced by such an extract process have so far been used in stretched form of smoking tobacco used in cigarettes or cigarillos, where primarily those that are unsuitable for the production of cigarettes Use fine particles and ribs as a smokable material could.
  • tobacco films have been used because of their uniform structure and better mechanical properties used as cover pages for cigarillos.
  • US 3 729 009 A were tobacco films analogous to a paper manufacturing process from tobacco rib material on the one hand and tobacco leaf waste like tobacco dust on the other hand in a ratio of 3: 1 used and the addition of one of these components Extract obtained in one on the dried end product related amount of 50 wt.% provided, due to the inadequate Taste, which also accounts for the largest proportion of tobacco rib material based, to improve taste up to 3% by weight of carbamide and up to 4% by weight of a C16 to C18 fatty acid soap, based on the weight of the existing tobacco ribs, admitted.
  • These tobacco wraps can also be added of about 20% by weight of foreign cellulose and produced as Cover or binder for cigarillos can be used.
  • EP 0 495 567 A was used to produce a rod-shaped smoke product with a binder or cover sheet made of tobacco foil with a content of up to 5% tobacco stem suggested the extract only in a limited amount, namely not more than 20% by weight (based on the weight of the Tobacco foil).
  • too taste quality or the aroma of such Product to be desired.
  • the invention has for its object a novel To propose a smoking product of the type mentioned at the beginning, which one first, the typical flavor expected by the smoker satisfied, the smoke products so far coated with tobacco films could not be reached, and which the other Improved secondary smoke quality.
  • a smoking product of the type mentioned at the beginning which one first, the typical flavor expected by the smoker satisfied, the smoke products so far coated with tobacco films could not be reached, and which the other Improved secondary smoke quality.
  • the tobacco foil formed jacket with regard to the physical film characteristics is designed so that the smoke product on usual Cigarette and cigarillo production systems economical can be manufactured and thus the requirements regarding Tear strength and elongation of such a jacket production fulfilled, with a further glow rate and porosity Enable control of the smoking offer.
  • a smoking product which is designed according to the main claim, being particularly preferred embodiments are listed in the subclaims.
  • the use of smoking products is also considered proposed new plug-in cigarillos.
  • TF-1 Process with proportional extract recycling and use of Tobacco stems or of tobacco stem or tobacco rib material and lamina tobacco material, as well as one for tobacco film production new method called "TF-2" without Extract recycling and use of only lamina tobacco material, combined with an almost quantitative circulation cold water soluble tobacco extracts in the wire section of a Papermaking plant.
  • the tobacco foils are preferably used for the cover sheet outer wrapping of the rod-shaped smoke product, according to the "TF-1" process and those for the binder, i.e. the (inner) Wrapping the core of the rod-shaped smoke product, according to the "TF-2" process manufactured.
  • the paper-making process 75 to 100% by weight of tobacco foil produced according to TF-1 from im essentially from (a) tobacco cellulose and (b) tobacco extract existing tobacco components.
  • the tobacco cellulose is made from a shredded leaf or cut tobacco mixture, from scrap tobacco (scrap), from tobacco stems and from Received tobacco rib material, the aroma-intensive components, namely the leaf-tobacco mixture and the tobacco greens with one Particle size of about 1 to 5 and preferably 1.5 to 4 mm on the one hand and those that are more decisive for the cellulose content Components, namely tobacco rib material on the other hand in one Weight ratio of 1: 1.1 to 1: 5 are present.
  • the tobacco extract is made from a shredded leaf-tobacco mixture and received tobacco rib material.
  • tobacco cellulose is the one for the production of Tobacco wrap required proportion of tobacco rib material somewhat higher what in terms of the physical properties of the Tobacco cellulose is required.
  • the relationship should from leaf or cut tobacco mixture to tobacco rib or Tobacco stem material does not exceed a value of 1: 5, otherwise the flavor-determined smoking properties of the tobacco foil be adversely affected.
  • this may be the case by adding flavors of tobacco during the last Step of the film production process can be compensated.
  • the tobacco foil Extract in an amount of more than 20% by weight of the tobacco foil the cellulose material obtained in this process is applied becomes. If the extract has an increased proportion of a lamina tobacco extract contains those for the final smoking product required aroma components enriched.
  • Tobacco film consists essentially of its tobacco content made of lamina tobacco material. This is related to the tobacco foil in an amount of 75 to 80% by weight together with 10 to 20% by weight Long-fiber foreign cellulose crushed and almost complete Circulation of cold water soluble tobacco extracts in the Sieve section of a paper production plant on this as raw film receive.
  • the usual additives such as required Binder, fillers and those that influence the burn-up Agents and flavorings can be present in an amount of up to 15% by weight. both in the production of the raw film and later in the Conditioning these can be added.
  • the tobacco foil is relevant to its taste Tobacco blend composition of the composition of the Leaf or cut tobacco mixture of the tobacco or Core of the rod-shaped smoke product corresponds. This is on the one hand to achieve the desired flavor - preferably "American Blend" - required, on the other hand in With regard to a simple, inexpensive manufacture of the rod-shaped smoke product is an advantage overall because with the same coat of tobacco both the shell and the core can be manufactured. You can also deviate from the Tobacco blend composition of the tobacco foil from the blend composition change the tobacco.
  • Both can be used as additives in the production Tobacco films according to TF-1 and TF-2 common binders such as methyl cellulose, Dextrins, pectins, alginates, starches, gums, amylose, Carboxymethyl cellulose, honey, corn syrup or other polysaccharides be used.
  • common binders such as methyl cellulose, Dextrins, pectins, alginates, starches, gums, amylose, Carboxymethyl cellulose, honey, corn syrup or other polysaccharides be used.
  • a filler Calcium carbonate or titanium dioxide can be used.
  • As a burn Influencing agents are mostly alkaline earth carbonates and Alkali salts of weak organic acids such as alkali citrates or acetates used.
  • Flavoring substances that are tobacco-own or extracts from tobacco mixtures can subsequently be used as flavorings, for example by an on-line application of the finished tobacco foils by means of the application device from Kaymich (GB) (Kaymich applicator model FDU3 SYSM).
  • the flavoring is preferably carried out in an alcoholic solution, preferably on the inside of the tobacco films, in order to avoid undesired optical effects, over the entire surface or in longitudinal strips.
  • This subsequent film flavoring can be carried out both with the tobacco film according to TF-1 and with the tobacco film according to TF-2.
  • the strand is Shredded tobacco core with only one according to the TF-1 process obtained tobacco wrapped.
  • Another one Embodiment of the invention consists of the strand-shaped Core-laid coat made of one or more layers of tobacco foil both using the TF-1 method or both using the TF-2 method have been obtained, although it is preferred the one layer and in particular the outer layer or the Manufacture cover sheet according to the TF-1 process, while the the inner layer or the binder is obtained using the TF-2 process has been.
  • the cover page is the outermost layer of the jacket formed around the strand-shaped core, spiral arranged, while the inner sheet around the strand-shaped core formed position of the jacket, in the axial Direction has an adhesive seam.
  • this smoking product should generally have the technical data listed in Table II below: general area preferably Diameter in mm 6 - 9 7.8 - 8.1 length in mm 50-250 55-75 Mass glow rate in mg / min 50-70 60 Packing density of the filling tobacco (core) in mg / cm 3 190-270 210-240
  • the cutting width of the inlay or filling tobacco preferably has the following values: Average of the mix 2.2 mm Virginia 2.2 mm Orient 2.5 mm Burley 2.0 mm
  • the pH of the measured in an aqueous slurry Tobacco foil is 7.0.
  • the covering or the jacket of the smoke product according to the invention may have an end porosity, in one embodiment, that is greater than 30 and less than 1,000 Coresta units.
  • This Product is like a conventional cigarillo, can be smoked by itself but also put in a usual cigarette filter sleeve and then to be smoked.
  • the invention can to manufacture the tobacco films of the jacket so that the Porosity of the jacket formed from the cover sheet and binder is in the range of 10,000 to 30,000 Coresta units, therefore has a very large porosity, so that this smoking product is not smokable by itself and only as a plug-in cigarillo usual known sleeves can be inserted and smoked.
  • the one according to the invention which can be smoked by itself rod-shaped smoke product according to the first variant in one for Cigarillos usual length are made; it can with one Filter mouthpiece of the usual type, i.e. also with a ventilated one Filters, which are preferably laser-perforated, are provided, which takes into account the trend towards the lights cigarillo.
  • the inventive Rod-shaped smoke product can also be oversized Lengths are made to it according to DE PS 42 06 507 depending To be able to divide smoking habits; according to DE PS 41 07 027 beveled at the end to better match it To be able to use sleeves.
  • a rod-shaped smoke product with a single-layer jacket as a cigarillo with a diameter of 8.0 mm and a strand length of 70 mm was produced.
  • the tobacco insert or the strand-shaped core consisted of a tobacco mixture with about 1.8% tobacco nicotine and a stuffing density of 210 mg / cm 3 , the average cutting width of the core tobacco of 60% by weight of the mixture being 2.2 mm.
  • the one-layer jacket was one in the axial direction glued tobacco film made using the extraction paper process TF-1 had been obtained.
  • cover sheet Porosity in Coresta units 103 Basis weight 47.7 g / m 2 extract 27.5% by weight CaCO 3 6.3% by weight TiO 2 4.4% by weight Sodium acetate 1.6% by weight rib 33.3% by weight Lamina 14.2% by weight Foreign cellulose 12.7% by weight
  • a rod-shaped smoke product was produced in the manner of a two-layer cigarillo with a diameter of 8.0 mm and a strand length of 70 mm.
  • the tobacco insert (core) again consisted of a tobacco mixture with about 1.8% tobacco nicotine and a plug density of 210 mg / cm 3 , the average cutting width of 60% by weight of the mixture again being 2.2 mm.
  • Both the binder and cover sheet consisted of tobacco foils that was obtained by the extraction paper method "TF-1" were; the cover sheet was spiral at an angle of 30 ° the page laid out.
  • the physical properties of the cover sheet corresponded to the tobacco film according to Example 1; the tobacco foil used as a binder and its composition are listed in Table IV below: Folder Porosity in Coresta units 76 Basis weight 41.8 g / m 2 extract 15.4% by weight CaC0 3 5.7% by weight Ti0 2 3.5% by weight Sodium acetate 2.0% by weight rib 42.9% by weight Lamina 16.7% by weight Foreign cellulose 13.8% by weight
  • a smoke product was produced analogously to Example 2, wherein however, the cover sheet and cover sheet were interchanged.
  • a smoke product was produced analogously to Example 2, which however with a ventilated (18% filter ventilation) monoacetate filter 20 mm long and 36% retention (Retention) was provided.
  • a smoking product was produced analogously to Example 2, but the binder was obtained by a paper production process without extract recycling according to TF-2 and had a porosity of 133 Coresta units and a weight of 52 g / m 2 .
  • the tobacco mixture consisted of 100% lamina tobacco. Based on its dry weight, the tobacco film also contained 75% by weight of laminate tobacco in addition to 10% by weight of long-fiber foreign cellulose CaCO 3: 8.0% by weight TiO 2 : 3.8% by weight Na acetate: 1.8% by weight Extract: 1.4% by weight
  • a smoking product was produced in the same way as in Example 2, but the cover sheet was produced using a different recipe according to TF-1; the individual values were: porosity 78 Coresta units Weight 48.2 g / m 2 extract 29.3% by weight CaCO 3 5.8% by weight TiO 2 1.7% by weight Na acetate 2.2% by weight Foreign cellulose 15.0% by weight Ribs 27.6% by weight Virginia Lamina 18.4% by weight
  • a smoke product was produced analogously to Example 6, wherein but the cover sheet is not made of tobacco rib material and lamina, but using the appropriate amount, namely 46% by weight of tobacco stems was produced.
  • a smoke product was produced analogously to Example 6, wherein however, the tobacco rib fraction of 27.6% by weight by the same Amount of tobacco stems was replaced.
  • the inner tobacco film optionally also made of can consist of several layers.
  • the outermost layer or the inner layer or tobacco foil be highly porous, with the respective other layer less is porous; mixed forms with regard to porosity are also feasible as long as an overall smokable product is obtained becomes.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Forging (AREA)
  • Paper (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Artificial Filaments (AREA)

Abstract

A rod-like smoking product with a strand-like filler rod of comminuted smoking tobacco and which is enclosed by a mantle of reconstituted tobacco sheets. At least one of these tobacco sheets is essentially obtained from 75 to 100% by weight of tobacco-inherent constituents including tobacco extract obtained from leaf or cut tobacco blend and tobacco rib material, and tobacco cellulose obtained from cut tobacco blend or scrap and stalk or rib material where the ratio of leaf and scrap material to stalk and rib material is in the range of 1:1.1 to 1:5.

Description

Die Erfindung betrifft ein stabförmiges Rauchprodukt mit einen strangförmigen Kern aus zerkleinerten Rauchtabak, der von einen Mantel aus nach einen Papierherstellungsverfahren hergestellten Tabakfolien umgeben ist.The invention relates to a rod-shaped smoke product with one strand - shaped core of shredded smoking tobacco, by one Jacket made from a paper manufacturing process Is surrounded by tobacco wraps.

Es ist allgemein bekannt, Tabakfolien, die auch als Blätter aus rekonstituiertem Tabak bezeichnet werden, nach Papierherstellungsverfahren z.B. gemäß US-A-4, 182, 349 herzustellen. Bei derartigen Verfahren werden grundsätzlich in einer ersten Stufe Stengel der Tabakpflanze, Tabakrippen und andere bei der Cigarettenherstellung nicht verwertbare Tabakbestandteile insbesondere Feinstanteile aber auch Tabakblätter zerfasert und mit beispielsweise erwärmten Wasser oder anderen wässrigen Flüssigkeiten bestimmter Temperaturen vermischt bzw. ausgewaschen, wonach mittels einer Siebvorrichtung der die wasserlöslichen Bestandteile enthaltende Extrakt abgezogen wird; in einer zweiten Stufe werden die Cellulosebestandteile gegebenenfalls nach weiteren Zwischenstufen wie Homogenisieren, nochmaligem Sieben oder Reinigen, zusammen mit Füllstoffen und anderen Zusätzen nach weiteren Zwischenstufen auf das Sieb einer Papierherstellungsvorrichtung gegeben. Auf die so erhaltene Rohfolie wird der eingeengte Tabak-Extrakt aufgebracht und diese zur endgültigen Tabakfolie verarbeitet.It is well known tobacco wraps, also called leaves from reconstituted tobacco, according to paper manufacturing processes e.g. according to US-A-4, 182, 349. In such procedures, one is basically in one first stage stem of tobacco plant, tobacco stems and others at components of tobacco that cannot be used in cigarette production especially fine fractions but also tobacco leaves frayed and with, for example, heated water or other aqueous Liquids of certain temperatures mixed or washed out, after which the water-soluble Extract containing ingredients is subtracted; in a second stage, the cellulose components are optionally after further intermediate stages such as homogenization, repeated Screening or cleaning, along with fillers and others Addition after further intermediate stages on the sieve of one Given paper making device. On the so obtained The concentrated tobacco extract is applied to the raw film and this processed into the final tobacco foil.

Die nach derartigen Extrakt-Verfahren hergestellten Tabakfolien wurden bislang einmal in kleingeschnittener Form zur Streckung von Rauchtabak in Cigaretten oder Cigarillos eingesetzt, wobei man in erster Linie die für die Cigarettenherstellung ungeeigneten Feinanteile und Rippen als rauchbares Material einsetzen konnte. Zum anderen wurden derartige Tabakfolien wegen ihrer gleichmäßigen Struktur und besseren mechanischen Eigenschaften als Deckblätter für Cigarillos verwendet.The tobacco films produced by such an extract process have so far been used in stretched form of smoking tobacco used in cigarettes or cigarillos, where primarily those that are unsuitable for the production of cigarettes Use fine particles and ribs as a smokable material could. On the other hand, such tobacco films have been used because of their uniform structure and better mechanical properties used as cover pages for cigarillos.

Der Einsatz von Tabakfolien als Umblatt oder Deckblatt für Rauchprodukte ist aus vielerlei Gründen problematisch, weil die Tabakfolien aufgrund des Tabakausgangsmaterials sensorisch unzureichend und/oder wegen der dunkleren Färbung für den Verbraucher wenig ansprechend sind. Es sind zahlreiche Versuche unternommen worden, diese Nachteile zu beheben, wie beispielsweise durch enzymatische Aufbereitung des Extraktes. Derartige Maßnahmen waren bislang wenig erfolgreich und führten auch zu Produkten, die gesetzlichen Bestimmungen nicht entsprachen. Darüber hinaus ergaben sich erhebliche Schwierigkeiten hinsichtlich der geforderten Eigenschaften derartiger Tabakfolien hinsichtlich ihrer Reißfestigkeit, ihrer Wasserbeständigkeit bzw. Speichelfestigkeit oder ganz allgemein hinsichtlich ihrer Raucheigenschaften, wie Porosität, Abbrennverhalten, Aschegehalt und insbesondere hinsichtlich des vom Verbraucher gewohnten Raucharomas.The use of tobacco foils as a binder or cover sheet for Smoking products is problematic for many reasons because the tobacco foils are sensory due to the tobacco raw material inadequate and / or because of the darker color for the Consumers are unappealing. There are numerous attempts have been attempted to address these drawbacks, such as by enzymatic preparation of the extract. Such Measures have so far been unsuccessful and have led to it Products that did not meet legal requirements. In addition, there were considerable difficulties with regard to the required properties of such tobacco films in terms of their tear resistance, their water resistance or saliva strength or more generally with regard to their Smoking properties, such as porosity, burning behavior, ash content and especially with regard to what the consumer is used to Smoke aromas.

Zur Behebung dieser Nachteile hat man einmal versucht, den Anteil an Tabakrippenmaterial gegenüber dem Anteil an Tabakblattabfall, wie Tabakgrus bzw. Tabakstaub zu erhöhen, um dadurch eine bessere Verarbeitbarkeit auf Papierherstellungsvorrichtungen mit entsprechend besserer Reißfestigkeit zu ermöglichen. Der bei diesen Tabakfolien auftretende "kratzige" Geschmack wurde durch die Beigabe tabakfremder Chemikalien gemindert. Zum anderen wurde vorgeschlagen, den Extrakt aus tabakeigenen Stoffen entsprechend zu behandeln oder den Anteil an Tabakrippenmaterial zu verringern.To overcome these drawbacks, one has tried the portion of tobacco rib material compared to the proportion of tobacco leaf waste, such as tobacco greens or tobacco dust to increase better processability on papermaking equipment with correspondingly better tear strength. The "scratchy" taste that occurs with these tobacco films was reduced by adding non-tobacco chemicals. On the other hand, it was proposed to extract the tobacco Treat substances appropriately or share to reduce tobacco rib material.

Im einzelnen wurde entsprechend der zuerst erwähnten Verfahrensweise z.B. gemäß LU 66 490 A eine papierähnliche Tabakfolie auf einer Langsiebpapiermaschine aus 60 Gew.% gemahlenen Tabakrippen, 30 Gew.% Tabakblattabfall wie Grus bzw. Staub und 10 Gew.% Sulfatzellstoff hergestellt; da diese Tabakfolie geschmacklich unzulänglich war, wurden zur Geschmacksverbesserung, bezogen auf die Trockensubstanz 5 Gew.% metallorganische Chelat- oder Komplexverbindungen zugesetzt. Nach US 3 729 009 A wurden analog nach einem Papierherstellungsverfahren Tabakfolien aus Tabakrippenmaterial einerseits und Tabakblattabfall wie Tabakstaub andererseits in einem Mengenverhältnis von 3 : 1 eingesetzt und die Zugabe eines aus diesen Komponenten gewonnenen Extraktes in einer auf das getrocknete Endprodukt bezogene Menge von 50 Gew.% vorgesehen, wobei wegen des unzulänglichen Geschmackes, der auch auf den größten Anteil am Tabakrippenmaterial beruht, zur Geschmacksverbesserung bis zu 3 Gew.% Carbamid und bis zu 4 Gew.% einer C16 bis C18 Fettsäureseife, bezogen jeweils auf das Gewicht der vorhandenen Tabakrippen, zugegeben. Diese Tabakfolien können auch unter Zusatz von etwa 20 Gew.% Fremdcellulose hergestellt und als Deckblatt oder Umblatt für Cigarillos verwendet werden. Da der Zusatz von metallorganischen Chelaten bzw. von Carbamid und Fettsäureseifen nicht zu geschmacklich akzeptablen und auch wegen gesetzlicher Verordnungen bezüglich zulässiger Zusätze zu nicht marktfähigen Produkten geführt hat, wurde die oben erwähnte weitere Alternative vorgeschlagen, indem man z.B. gemäß GB 1 093 696 A vorschlug, eine als Cigarrendecke geeignete Tabakfolie aus Blatt- und Stammkomponenten sowie Tabakstaub im Verhältnis von 3 : 1 einzusetzen und den aus diesen Komponenten erhaltenen Extrakt zu zentrifugieren und nur einen Teil der wässrigen Phase dem Cellulosematerial zuzuführen.In detail, according to the first-mentioned procedure e.g. according to LU 66 490 A a paper-like tobacco foil on a Fourdrinier paper machine made from 60% by weight Tobacco ribs, 30% by weight of tobacco leaf waste such as greens or dust and 10% by weight sulfate pulp produced; because this tobacco foil tastes good was inadequate, were used to improve taste, based on the dry matter 5 wt.% organometallic Chelate or complex compounds added. According to US 3 729 009 A were tobacco films analogous to a paper manufacturing process from tobacco rib material on the one hand and tobacco leaf waste like tobacco dust on the other hand in a ratio of 3: 1 used and the addition of one of these components Extract obtained in one on the dried end product related amount of 50 wt.% provided, due to the inadequate Taste, which also accounts for the largest proportion of tobacco rib material based, to improve taste up to 3% by weight of carbamide and up to 4% by weight of a C16 to C18 fatty acid soap, based on the weight of the existing tobacco ribs, admitted. These tobacco wraps can also be added of about 20% by weight of foreign cellulose and produced as Cover or binder for cigarillos can be used. Since the Addition of organometallic chelates or carbamide and Fatty acid soaps are not too tasty and too due to legal regulations regarding admissible additives has led to non-marketable products, the above suggested another alternative, e.g. proposed according to GB 1 093 696 A, one as a cigar blanket suitable tobacco foil from leaf and stem components as well Use tobacco dust in a ratio of 3: 1 and that out centrifuge the extract obtained from these components and only part of the aqueous phase of the cellulose material feed.

Letztlich wurde nach der EP 0 495 567 A zur Herstellung eines stabförmigen Rauchproduktes mit einem Umblatt oder Deckblatt aus Tabakfolie mit einem Gehalt bis nur zu 5 % Tabakstengel vorgeschlagen, den Extrakt nur in einer begrenzten Menge, nämlich nicht über 20 Gew.% (bezogen auf das Gewicht der Tabakfolie) wieder aufzubringen. Auch hier läßt die geschmackliche Qualität oder das Aroma eines derartigen Produktes zu wünschen übrig.Ultimately, EP 0 495 567 A was used to produce a rod-shaped smoke product with a binder or cover sheet made of tobacco foil with a content of up to 5% tobacco stem suggested the extract only in a limited amount, namely not more than 20% by weight (based on the weight of the Tobacco foil). Here, too taste quality or the aroma of such Product to be desired.

Alle diese Produkte haben den Nachteil, daß einmal das zur Herstellung der Tabakfolien eingesetzte Tabakmaterial zu unliebsamen Geschmacksrichtungen führt und der aufdringliche und schwere Geruch des Nebenrauches von vielen Rauchern nicht akzeptiert wird. Diese geschmackliche und ebenso die geruchliche Beeinträchtigung wird bei einem Tabakprodukt mit einer Ummantelung aus beispielsweise zwei Tabakfolien noch verstärkt, weil diese etwa 20 Gew.% des Tabakproduktes gegenüber dem Kern aus zerkleinertem Rauchtabak ausmachen und somit den Geschmackseindruck des Hauptrauches erheblich beeinflussen bzw. mindern, ebenso den Geruchseindruck des Nebenrauches. All these products have the disadvantage that Production of the tobacco films used tobacco material to unpleasant Flavors leads and the pushy and heavy smell of secondary smoke not accepted by many smokers becomes. This taste and also the smell A tobacco product with a Wrapping from, for example, two tobacco foils intensified because this is about 20% by weight of the tobacco product against the core of shredded smoking tobacco and thus the taste impression of the main smoke considerably influence or reduce, as well as the smell impression of Secondary smoke.

Der Erfindung liegt die Aufgabe zugrunde, ein neuartiges Rauchprodukt der eingangs erwähnten Art vorzuschlagen, welches einmal die vom Raucher erwartete typische Geschmacksrichtung befriedigt, die bislang von mit Tabakfolien ummantelten Rauchprodukten nicht erreicht werden konnte, und welches zum anderen die Qualität des Nebenrauches verbessert. Letzlich wird ein derart ummanteltes Rauchprodukt vorgeschlagen, bei dem der aus Tabakfolien gebildete Mantel hinsichtlich der physikalischen Folien-Kenndaten so ausgebildet ist, daß das Rauchprodukt auf üblichen Cigaretten- bzw. Cigarillo-Fertigungsanlagen wirtschaftlich hergestellt werden kann und somit die Anforderungen bezüglich Reißfestigkeit und Dehnung einer derartigen Mantelherstellung erfüllt, wobei ferner Glimmgeschwindigkeit und Porosität eine Steuerung des Rauchangebots ermöglichen.The invention has for its object a novel To propose a smoking product of the type mentioned at the beginning, which one first, the typical flavor expected by the smoker satisfied, the smoke products so far coated with tobacco films could not be reached, and which the other Improved secondary smoke quality. Ultimately, it will be like this encased smoke product proposed in which the tobacco foil formed jacket with regard to the physical film characteristics is designed so that the smoke product on usual Cigarette and cigarillo production systems economical can be manufactured and thus the requirements regarding Tear strength and elongation of such a jacket production fulfilled, with a further glow rate and porosity Enable control of the smoking offer.

Zur Lösung dieser Aufgabe wird daher ein Rauchprodukt vorgeschlagen, welches gemäß Hauptanspruch gestaltet ist, wobei besonders bevorzugte Ausführungen in den Unteransprüchen aufgeführt sind. Insbesondere wird auch die Verwendung der Rauchprodukte als neuartige Steckcigarillos vorgeschlagen.To solve this problem, a smoking product is therefore proposed which is designed according to the main claim, being particularly preferred embodiments are listed in the subclaims. In particular, the use of smoking products is also considered proposed new plug-in cigarillos.

Grundsätzlich ist bei der Herstellung der Tabakfolien des stabförmigen Rauchproduktes gemäß Erfindung zwischen zwei unterschiedlichen Papierherstellungsverfahren zu unterscheiden, zum einen das eingangs beschriebene als "TF-1" bezeichnete Verfahren mit anteiliger Extraktrückführung und Einsatz von Tabakstengeln oder von Tabakstengel- bzw. Tabakrippenmaterial und Lamina-Tabakmaterial, sowie zum anderen ein für die Tabakfolienherstellung neues und als "TF-2" bezeichnetes Verfahren ohne Extraktrückführung und Einsatz von ausschließlich Lamina-Tabakmaterial, verbunden mit einem nahezu quantitativen Umlauf kaltwasserlöslicher Tabakauszüge in der Siebpartie einer Papierherstellungsanlage.Basically in the manufacture of tobacco films rod-shaped smoke product according to the invention between two differentiate between different paper manufacturing processes, on the one hand, the one described at the beginning as "TF-1" Process with proportional extract recycling and use of Tobacco stems or of tobacco stem or tobacco rib material and lamina tobacco material, as well as one for tobacco film production new method called "TF-2" without Extract recycling and use of only lamina tobacco material, combined with an almost quantitative circulation cold water soluble tobacco extracts in the wire section of a Papermaking plant.

Vorzugsweise werden die Tabakfolien für das Deckblatt, also der äußeren Umhüllung des stabförmigen Rauchproduktes, nach dem "TF-1"-Verfahren und die für das Umblatt, also der (inneren) Umhüllung des Kerns des stabförmigen Rauchproduktes, nach dem "TF-2"-Verfahren gefertigt. Dies ergibt überraschenderweise eine geruchliche Besserstellung des Nebenrauches des erfindungsgemäßen Produktes gegenüber dem Nebenrauch von herkömmlichen, vergleichbaren Produkten wie handelsüblichen Cigarillos. Dabei wird jedoch nicht die Menge des Nebenrauches, sondern ausschließlich seine geruchliche Qualität entscheidend verbessert; der Nebenrauch verliert seine aufdringliche, von vielen Rauchern nicht akzeptierte, dunkle, duffe Note.The tobacco foils are preferably used for the cover sheet outer wrapping of the rod-shaped smoke product, according to the "TF-1" process and those for the binder, i.e. the (inner) Wrapping the core of the rod-shaped smoke product, according to the "TF-2" process manufactured. This surprisingly gives one olfactory improvement of the secondary smoke of the invention Product compared to the secondary smoke of conventional, comparable Products such as commercially available cigarillos. However, it will not the amount of secondary smoke, but only his olfactory quality significantly improved; the secondary smoke loses its intrusive, unacceptable to many smokers, dark, fragrant note.

Dieser Effekt kann aber auch wiederum unerwarteterweise erzielt werden mit einer anderen, bevorzugten Ausführungsform gemäß Erfindung, bei der ausschließlich Tabakfolien nach "TF-1" eingesetzt werden, wobei jedoch der Deckblatt-Tabakfolie erheblich mehr Tabakextrakt zu- bzw. rückgeführt wird als der Umblatt-Tabakfolie. Insgesamt enthält dann der hier aus zwei Lagen bestehende Mantel des stabförmigen Rauchproduktes bezogen auf die Trockensubstanz eine Tabakextrakt-Menge von mehr als 20 Gew.%.However, this effect can also be achieved unexpectedly are in accordance with another preferred embodiment Invention in which only tobacco films according to "TF-1" are used be, however, the topsheet tobacco wrap considerably more tobacco extract is fed in or recycled than the tobacco leaf. In total, this contains two layers existing jacket of the rod-shaped smoke product based on the Dry matter a tobacco extract amount of more than 20% by weight.

Letztlich sind auch Kombinationen der nach beiden Verfahren hergestellten Tabakfolien zur Fertigung des stabförmigen Rauchproduktes gemäß Erfindung möglich, die zumindest anteilig die vorteilhaften, überraschenden Effekte ergeben, was den Rauchern von beispielsweise "klassischen" Cigarillos den Umstieg auf das erfindungsgemäße Produkt vermutlich erleichtert.Ultimately there are also combinations of the two methods manufactured tobacco films for the manufacture of the rod-shaped Smoking product according to the invention possible, at least in part the beneficial, surprising effects result in what the Smokers of, for example, "classic" cigarillos made the switch probably relieved of the product according to the invention.

Tabakfolie nach TF-1Tobacco film according to TF-1

Zur Herstellung des stabförmigen Rauchproduktes gemäß Erfindung ist es wesentlich, daß die nach dem Papierherstellungsverfahren gemäß TF-1 hergestellte Tabakfolie zu 75 bis 100 Gew.% aus im wesentlichen aus (a) Tabakcellulose und (b) Tabakextrakt bestehenden tabakeigenen Bestandteilen besteht. Die Tabakcellulose wird aus einer zerkleinerten Blatt- oder Schnitt-Tabakmischung, aus Tabakgrus (scrap), aus Tabakstengeln und aus Tabakrippenmaterial erhalten, wobei die aromaintensiven Komponenten, nämlich die Blatt-Tabakmischung und der Tabakgrus mit einer Teilchengröße von etwa 1 bis 5 und vorzugsweise 1,5 bis 4 mm einerseits und die für den Celluloseanteil stärker bestimmenden Komponenten, nämlich Tabakrippenmaterial andererseits in einem Gewichtsverhältnis von 1 : 1,1 bis 1 : 5 vorliegen. Der Tabakextrakt wird aus einer zerkleinerten Blatt- Tabakmischung und Tabakrippenmaterial erhalten.For the production of the rod-shaped smoke product according to the invention it is essential that the paper-making process 75 to 100% by weight of tobacco foil produced according to TF-1 from im essentially from (a) tobacco cellulose and (b) tobacco extract existing tobacco components. The tobacco cellulose is made from a shredded leaf or cut tobacco mixture, from scrap tobacco (scrap), from tobacco stems and from Received tobacco rib material, the aroma-intensive components, namely the leaf-tobacco mixture and the tobacco greens with one Particle size of about 1 to 5 and preferably 1.5 to 4 mm on the one hand and those that are more decisive for the cellulose content Components, namely tobacco rib material on the other hand in one Weight ratio of 1: 1.1 to 1: 5 are present. The tobacco extract is made from a shredded leaf-tobacco mixture and received tobacco rib material.

Ferner werden zur Herstelung der Tabakfolien bis zu 20 Gew.% und vorzugsweise 8 bis 14 Gew.% Fremdcellulose wie Weichholz-, Hanf- bzw. Flachs-Cellulose eingesetzt. Wenn die Tabakcellulose vollständig oder teilweise aus Tabakstengeln herrührt, kann der Anteil an Fremdcellulose ohne Beeinträchtigung der physikalischen Eigenschaften der Tabakfolie entsprechend verringert werden.Furthermore, up to 20% by weight and preferably 8 to 14% by weight of foreign cellulose such as softwood, hemp or Flax cellulose used. If the tobacco cellulose comes wholly or in part from tobacco stems, the Proportion of foreign cellulose without affecting the physical Properties of the tobacco foil are reduced accordingly.

Es ist vorteilhaft, wenn zur Herstellung dieser Tabakfolie etwas weniger als die Hälfte des zur Herstellung der Tabakfolie erforderlichen Tabakmaterials aus einer hochwertigen Schnitt-Tabakmischung besteht, die beispielsweise aus einer Mischung aus Virginia-Tabak, Burley-Tabak, Orient-Tabak und Blährippen von Virginia-Tabak besteht.It is advantageous if something to make this tobacco foil less than half of that used to make the tobacco foil required tobacco material from a high-quality cut tobacco mixture consists, for example, of a mixture of Virginia tobacco, Burley tobacco, oriental tobacco and blowing ribs from Virginia tobacco exists.

Bezüglich der Tabakcellulose liegt der zur Herstellung der Tabakfolie erforderliche Anteil an Tabakrippenmaterial etwas höher, was im Hinblick auf die physikalischen Eigenschaften der Tabakcellulose erforderlich ist. Allerdings soll das Verhältnis von Blatt- bzw. Schnitt-Tabakmischung zu Tabakrippen- bzw. Tabakstengelmaterial nicht einen Wert von 1 : 5 überschreiten, da sonst die aromabestimmten Raucheigenschaften der Tabakfolie nachteilig beeinflußt werden. Gegebenenfalls kann dies jedoch durch die Zugabe von tabakeigenen Aromen während des letzten Schrittes des Folienfertigungsprozesses kompensiert werden. Regarding the tobacco cellulose is the one for the production of Tobacco wrap required proportion of tobacco rib material somewhat higher what in terms of the physical properties of the Tobacco cellulose is required. However, the relationship should from leaf or cut tobacco mixture to tobacco rib or Tobacco stem material does not exceed a value of 1: 5, otherwise the flavor-determined smoking properties of the tobacco foil be adversely affected. However, this may be the case by adding flavors of tobacco during the last Step of the film production process can be compensated.

Wesentlich ist, daß bei der Herstellung der Tabakfolie der Extrakt in einer Menge von mehr als 20 Gew.% der Tabakfolie auf das bei diesem Verfahren erhaltene Cellulosematerial aufgebracht wird. Wenn der Extrakt einen erhöhten Anteil eines Lamina-Tabakextraktes enthält, werden die für das endgültige Rauchprodukt erforderlichen Aromabestandteile angereichert.It is essential that in the manufacture of the tobacco foil Extract in an amount of more than 20% by weight of the tobacco foil the cellulose material obtained in this process is applied becomes. If the extract has an increased proportion of a lamina tobacco extract contains those for the final smoking product required aroma components enriched.

Tabakfolie nach TF-2Tobacco film according to TF-2

Diese nach einem anderen Papierherstellungsverfahren gefertigte Tabakfolie besteht bezüglich ihres Tabakanteils im wesentlichen aus Lamina-Tabakmaterial. Dieses wird bezogen auf die Tabakfolie in einer Menge von 75 bis 80 Gew.% zusammen mit 10 bis 20 Gew.% langfaseriger Fremdcellulose zerkleinert und bei nahezu vollständigem Umlauf der kaltwasserlöslichen Tabakauszüge in der Siebpartie einer Papierherstellungsanlage auf dieser als Rohfolie erhalten. Die weiterhin erforderlichen üblichen Zusatzstoffe wie Bindemittel, Füllstoffe und die den Abbrand beeinflussenden Mittel sowie Aromastoffe können in einer Menge bis zu 15 Gew.% sowohl bei Herstellung der Rohfolie als auch später bei der Konditionierung dieser zugesetzt werden.This was manufactured using a different paper manufacturing process Tobacco film consists essentially of its tobacco content made of lamina tobacco material. This is related to the tobacco foil in an amount of 75 to 80% by weight together with 10 to 20% by weight Long-fiber foreign cellulose crushed and almost complete Circulation of cold water soluble tobacco extracts in the Sieve section of a paper production plant on this as raw film receive. The usual additives such as required Binder, fillers and those that influence the burn-up Agents and flavorings can be present in an amount of up to 15% by weight. both in the production of the raw film and later in the Conditioning these can be added.

Es ist von Vorteil, wenn die Tabakfolie in ihrer geschmacksrelevanten Tabakmischungszusammensetzung der Zusammensetzung der Blatt- bzw. Schnitt-Tabakmischung des Einlegetabaks bzw. des Kernes des stabförmigen Rauchproduktes entspricht. Dies ist einerseits zur Erzielung der gewünschten Geschmacksrichtung - vorzugsweise "American Blend" - erforderlich, andererseits im Hinblick auf eine einfache, kostengünstige Fertigung des stabförmigen Rauchproduktes insgesamt von Vorteil, da mit der gleichen Tabak-Mischung sowohl der Mantel als auch der Kern gefertigt werden können. Man kann auch abweichend davon die Tabakmischungszusammensetzung der Tabakfolie von der Mischungszusammensetzung des Einlegetabaks abändern.It is advantageous if the tobacco foil is relevant to its taste Tobacco blend composition of the composition of the Leaf or cut tobacco mixture of the tobacco or Core of the rod-shaped smoke product corresponds. This is on the one hand to achieve the desired flavor - preferably "American Blend" - required, on the other hand in With regard to a simple, inexpensive manufacture of the rod-shaped smoke product is an advantage overall because with the same coat of tobacco both the shell and the core can be manufactured. You can also deviate from the Tobacco blend composition of the tobacco foil from the blend composition change the tobacco.

Zur Herstellung der Tabakfolie sowohl nach TF-1 als auch nach TF-2 können noch bis zu 20 Gew.% Fremdcellulose zugesetzt werden, wodurch die physikalischen Eigenschaften der Tabakfolie verbessert werden.For the manufacture of tobacco foil according to both TF-1 and Up to 20% by weight of foreign cellulose can be added to TF-2, which improves the physical properties of the tobacco foil become.

Als Zusatzstoffe können bei der Herstellung wiederum beider Tabakfolien nach TF-1 und TF-2 übliche Bindemittel wie Methylcellulose, Dextrine, Pektine, Alginate, Stärke, Gummen, Amylose, Carboxymethylcellulose, Honig, Maissirup oder andere Polysaccharide verwendet werden. Als Füllstoff kann beispielsweise Calciumcarbonat oder Titandioxyd eingesetzt werden. Als Abbrand beeinflussende Mittel werden meist Erdalkalicarbonate und Alkalisalze schwacher organischer Säuren wie Alkalicitrate oder -acetate eingesetzt.Both can be used as additives in the production Tobacco films according to TF-1 and TF-2 common binders such as methyl cellulose, Dextrins, pectins, alginates, starches, gums, amylose, Carboxymethyl cellulose, honey, corn syrup or other polysaccharides be used. For example, as a filler Calcium carbonate or titanium dioxide can be used. As a burn Influencing agents are mostly alkaline earth carbonates and Alkali salts of weak organic acids such as alkali citrates or acetates used.

Als Aromastoffe können nachträglich tabakeigene Aromastoffe oder Extrakte aus Tabakmischungen eingesetzt werden, beispielsweise durch eine on-line Beaufschlagung der an sich fertigen Tabakfolien mittels der Beaufschlagungsvorrichtung der Firma Kaymich (GB) (Kaymich-Applikator Modell FDU3 SYSM). Dabei erfolgt der Aromenauftrag vorzugsweise in alkoholischer Lösung, bevorzugt auf die Innenseite der Tabakfolien, um unerwünschte optische Effekte zu vermeiden, ganzflächig oder in Längsstreifen. Diese nachträgliche Folienaromatisierung kann sowohl bei der Tabakfolie gemäß TF-1 durchgeführt werden als auch bei der Tabakfolie gemäß TF-2. Technischen Daten der Tabakfolien TF-1 bzw. TF-2: allgemeiner Bereich vorzugsweise Dehnung in % nach DIN 53112 1 - 1,4 1,15 - 1,3 Porosität nach DIN ISO 2965 in Coresta-Einheiten 30 - 200 80 - 120 Flächengewicht nach DIN 53104 in g/m2 35 - 70 45 - 55 Feuchte nach DIN 10252 in % 8 - 15 8 - 12 Bruchlast nach DIN 53112 in g je 2,54 cm Breite mind. 1000 1350 - 1600 Flavoring substances that are tobacco-own or extracts from tobacco mixtures can subsequently be used as flavorings, for example by an on-line application of the finished tobacco foils by means of the application device from Kaymich (GB) (Kaymich applicator model FDU3 SYSM). The flavoring is preferably carried out in an alcoholic solution, preferably on the inside of the tobacco films, in order to avoid undesired optical effects, over the entire surface or in longitudinal strips. This subsequent film flavoring can be carried out both with the tobacco film according to TF-1 and with the tobacco film according to TF-2. Technical data of the tobacco films TF-1 and TF-2: general area preferably Elongation in% according to DIN 53112 1 - 1.4 1.15 - 1.3 Porosity according to DIN ISO 2965 in Coresta units 30-200 80-120 Basis weight according to DIN 53104 in g / m 2 35-70 45-55 Humidity according to DIN 10252 in% 8-15 8-12 Breaking load according to DIN 53112 in g each 2.54 cm wide at least 1000 1350 - 1600

Bei einer Ausführungsform der Erfindung ist der strangförmige Kern aus zerkleinertem Rauchtabak mit nur einer nach dem TF-1-Verfahren erhaltenen Tabakfolie ummantelt. Bei einer anderen Ausführungsform der Erfindung besteht der um den strangförmigen Kern gelegte Mantel aus ein oder mehr Lagen Tabakfolie, die sowohl beide nach dem TF-1-Verfahren oder beide nach dem TF-2-Verfahren erhalten worden sind, wobei es allerdings bevorzugt wird, die eine Lage und insbesondere die äußere Lage bzw. das Deckblatt nach dem TF-1-Verfahren herzustellen, während die innere Lage bzw. das Umblatt nach dem TF-2-Verfahren erhalten worden ist. Üblicherweise ist das Deckblatt, also die äußerste um den strangförmigen Kern gebildete Lage des Mantels, spiralförmig angeordnet, während das Umblatt, also die innerste um den strangförmigen Kern gebildete Lage des Mantels, in axialer Richtung eine Klebenaht aufweist.In one embodiment of the invention, the strand is Shredded tobacco core with only one according to the TF-1 process obtained tobacco wrapped. Another one Embodiment of the invention consists of the strand-shaped Core-laid coat made of one or more layers of tobacco foil both using the TF-1 method or both using the TF-2 method have been obtained, although it is preferred the one layer and in particular the outer layer or the Manufacture cover sheet according to the TF-1 process, while the the inner layer or the binder is obtained using the TF-2 process has been. Usually the cover page is the outermost layer of the jacket formed around the strand-shaped core, spiral arranged, while the inner sheet around the strand-shaped core formed position of the jacket, in the axial Direction has an adhesive seam.

Bei einem mit zwei Tabakfolien umhüllten Kern soll dieses Rauchprodukt im allgemeinen die in der folgenden Tabelle II aufgeführten technischen Daten haben: allgemeiner Bereich vorzugsweise Durchmesser in mm 6 - 9 7,8 - 8,1 Länge in mm 50 - 250 55 - 75 Massenglimmgeschwindigkeit in mg/min 50 - 70 60 Stopfdichte des Fülltabaks (Kern) in mg/cm3 190 - 270 210 - 240 In the case of a core covered with two tobacco foils, this smoking product should generally have the technical data listed in Table II below: general area preferably Diameter in mm 6 - 9 7.8 - 8.1 length in mm 50-250 55-75 Mass glow rate in mg / min 50-70 60 Packing density of the filling tobacco (core) in mg / cm 3 190-270 210-240

Bei dem strangförmigen Kern aus zerkleinertem Rauchtabak hat vorzugsweise die Schnittbreite des Einlage- oder Fülltabaks die folgenden Werte: Mittelwert der Mischung 2,2 mm Virginia 2,2 mm Orient 2,5 mm Burley 2,0 mm In the case of the strand-shaped core made from shredded smoking tobacco, the cutting width of the inlay or filling tobacco preferably has the following values: Average of the mix 2.2 mm Virginia 2.2 mm Orient 2.5 mm Burley 2.0 mm

Der in einer wässrigen Aufschlämmung gemessene pH-Wert der Tabakfolie liegt bei 7,0.The pH of the measured in an aqueous slurry Tobacco foil is 7.0.

Die Umhüllung bzw. der Mantel des erfindungsgemäßen Rauchproduktes kann bei einer Ausführungsform eine Endporosität haben, die größer als 30 und kleiner als 1 000 Coresta-Einheiten ist. Dieses Produkt ist wie ein üblicher Cigarillo für sich abrauchbar, kann aber auch in eine übliche Cigarettenfilterhülse gesteckt und dann geraucht werden. Bei einer anderen Variante gemäß Erfindung kann man die Tabakfolien des Mantels auch so herstellen, daß die Porosität des aus Deckblatt und Umblatt gebildeten Mantels in einem Bereich von 10.000 bis 30.000 Coresta-Einheiten liegt, also eine sehr große Porosität besitzt, so daß dieses Rauchprodukt für sich nicht abrauchbar ist und nur als Steckcigarillo in übliche bekannte Hülsen eingeschoben und geraucht werden kann.The covering or the jacket of the smoke product according to the invention may have an end porosity, in one embodiment, that is greater than 30 and less than 1,000 Coresta units. This Product is like a conventional cigarillo, can be smoked by itself but also put in a usual cigarette filter sleeve and then to be smoked. In another variant according to the invention can to manufacture the tobacco films of the jacket so that the Porosity of the jacket formed from the cover sheet and binder is in the range of 10,000 to 30,000 Coresta units, therefore has a very large porosity, so that this smoking product is not smokable by itself and only as a plug-in cigarillo usual known sleeves can be inserted and smoked.

Grundsätzlich kann das erfindungsgemäße für sich abrauchbare stabförmige Rauchprodukt nach der ersten Variante in einer für Cigarillos üblichen Länge hergestellt werden; es kann mit einem Filtermundstück üblicher Art, also auch mit einem ventilierten Filter, der vorzugsweise Laser-perforiert ist, versehen werden, was dem Trend zum Lights-Cigarillo berücksichtigt. Das erfindungsgemäße, stabförmige Rauchprodukt kann auch in übergroßen Längen hergestellt werden, um es gemäß DE PS 42 06 507 je nach Abrauchgewohnheiten abteilen zu können; es kann ferner gemäß DE PS 41 07 027 am Ende abgeschrägt sein, um es besser in entsprechende Hülsen einsetzen zu können.In principle, the one according to the invention which can be smoked by itself rod-shaped smoke product according to the first variant in one for Cigarillos usual length are made; it can with one Filter mouthpiece of the usual type, i.e. also with a ventilated one Filters, which are preferably laser-perforated, are provided, which takes into account the trend towards the lights cigarillo. The inventive Rod-shaped smoke product can also be oversized Lengths are made to it according to DE PS 42 06 507 depending To be able to divide smoking habits; according to DE PS 41 07 027 beveled at the end to better match it To be able to use sleeves.

Im folgenden wird die Erfindung durch Beispiele erläutert.In the following the invention is illustrated by examples.

Beispiel 1example 1

Es wurde ein stabförmiges Rauchprodukt mit einem einlagigen Mantel als Cigarillo mit einem Durchmesser von 8,0 mm und einer Stranglänge von 70 mm gefertigt. Die Tabakeinlage bzw. der strangförmige Kern bestand aus einer Tabakmischung mit etwa 1.8 % Tabaknikotin und einer Stopfdichte von 210 mg/cm3, wobei die mittlere Schnittbreite des Kerntabaks von 60 Gew.% der Mischung bei 2,2 mm lag.A rod-shaped smoke product with a single-layer jacket as a cigarillo with a diameter of 8.0 mm and a strand length of 70 mm was produced. The tobacco insert or the strand-shaped core consisted of a tobacco mixture with about 1.8% tobacco nicotine and a stuffing density of 210 mg / cm 3 , the average cutting width of the core tobacco of 60% by weight of the mixture being 2.2 mm.

Der aus einer Lage bestehende Mantel war eine in axialer Richtung verklebte Tabakfolie, die nach dem Extraktions-Papierverfahren TF-1 erhalten worden war.The one-layer jacket was one in the axial direction glued tobacco film made using the extraction paper process TF-1 had been obtained.

Die physikalischen Eigenschaften der Tabakfolie und deren Zusammensetzung sind in der folgenden Tabelle III aufgeführt. Deckblatt Porosität in Coresta-Einheiten 103 Flächengewicht 47,7 g/m2 Extrakt 27,5 Gew.% CaCO3 6,3 Gew.% TiO2 4,4 Gew.% Natriumacetat 1,6 Gew.% Rippe 33,3 Gew.% Lamina 14,2 Gew.% Fremdcellulose 12,7 Gew.% The physical properties of the tobacco foil and its composition are listed in Table III below. cover sheet Porosity in Coresta units 103 Basis weight 47.7 g / m 2 extract 27.5% by weight CaCO 3 6.3% by weight TiO 2 4.4% by weight Sodium acetate 1.6% by weight rib 33.3% by weight Lamina 14.2% by weight Foreign cellulose 12.7% by weight

Diese Cigarillos wurden bei 60 % relativer Feuchte und 21° C auf übliche Art konditioniert und von einem Expertenpanel geraucht und wie folgt bewertet:These cigarillos were at 60% relative humidity and 21 ° C The usual type is conditioned and smoked by an expert panel and rated as follows:

Bewertung: Kräftiger "American-Blend" Geschmack mit ausgeprägter nussiger Burley-Note mit geringem Störfaktorniveau und einem kaum aufdringlichen, angenehmen Nebenrauch ohne die unerwünschte cigarrige Note. Evaluation: Strong "American blend" taste with a pronounced nutty Burley note with low interference level and hardly any pushy, pleasant secondary smoke without the unwanted cigar note.

Beispiel 2Example 2

Es wurde ein stabförmiges Rauchprodukt nach Art eines zweilagigen Cigarillos mit einem Durchmesser von 8,0 mm und einer Stranglänge von 70 mm gefertigt. Die Tabakeinlage (Kern) bestand wiederum aus einer Tabakmischung mit etwa 1.8 % Tabaknikotin und einer Stopfdichte von 210 mg/cm3, wobei die mittlere Schnittbreite von 60 Gew.% der Mischung wiederum bei 2,2 mm lag.A rod-shaped smoke product was produced in the manner of a two-layer cigarillo with a diameter of 8.0 mm and a strand length of 70 mm. The tobacco insert (core) again consisted of a tobacco mixture with about 1.8% tobacco nicotine and a plug density of 210 mg / cm 3 , the average cutting width of 60% by weight of the mixture again being 2.2 mm.

Sowohl Umblatt als auch Deckblatt bestanden aus Tabakfolien, die nach dem Extraktions-Papierverfahren "TF-1" erhalten worden waren; das Deckblatt war spiralförmig mit einem Winkel von 30° um das Umblatt aufgelegt.Both the binder and cover sheet consisted of tobacco foils that was obtained by the extraction paper method "TF-1" were; the cover sheet was spiral at an angle of 30 ° the page laid out.

Die physikalischen Eigenschaften des Deckblattes entsprachen der Tabakfolie gemäß Beispiel 1; die der als Umblatt verwendeten Tabakfolie und deren Zusammensetzung sind in der folgenden Tabelle IV aufgeführt: Umblatt Porosität in Coresta-Einheiten 76 Flächengewicht 41,8 g/m2 Extrakt 15,4 Gew.% CaC03 5,7 Gew.% Ti02 3,5 Gew.% Natriumacetat 2,0 Gew.% Rippe 42,9 Gew.% Lamina 16,7 Gew.% Fremdcellulose 13,8 Gew.% The physical properties of the cover sheet corresponded to the tobacco film according to Example 1; the tobacco foil used as a binder and its composition are listed in Table IV below: Folder Porosity in Coresta units 76 Basis weight 41.8 g / m 2 extract 15.4% by weight CaC0 3 5.7% by weight Ti0 2 3.5% by weight Sodium acetate 2.0% by weight rib 42.9% by weight Lamina 16.7% by weight Foreign cellulose 13.8% by weight

Diese Cigarillos wurden bei 60 % relativer Feuchte und 21° C auf übliche Art konditioniert und von einem Expertenpanel geraucht und wie folgt bewertet: Kräftiger "American Blend" Geschmack wie bei dem Produkt gemäß Beispiel 1 mit ausgeprägter nussiger Burley-Note mit geringen Störfaktorniveau und einem kaum aufdringlichen, angenehmen Nebenrauch ohne die unerwünschte cigarrige Note.These cigarillos were at 60% relative humidity and 21 ° C The usual type is conditioned and smoked by an expert panel and rated as follows: Powerful "American blend" taste like in the product according to Example 1 with a pronounced nutty Burley note with low interference factor level and hardly any pushy, pleasant secondary smoke without the unwanted cigar note.

Beispiel 3Example 3

Es wurde ein Rauchprodukt analog Beispiel 2 hergestellt, wobei jedoch Umblatt und Deckblatt vertauscht wurden.A smoke product was produced analogously to Example 2, wherein however, the cover sheet and cover sheet were interchanged.

Bewertung: American-Blend-Charakter, aber weniger Aroma als das Produkt nach Beispiel 1; cellulosiger Beigeschmack sowie cellulosiger Raumduftnote.Evaluation: American blend character, but less aroma than that Product according to example 1; cellulos aftertaste as well cellulos room fragrance.

Beispiel 4Example 4

Es wurde ein Rauchprodukt analog Beispiel 2 hergestellt, welches jedoch mit einem ventilierten (18 % Filterventilation) Monoacetatfilter von 20 mm Länge und einem Rückhaltevermögen von 36 % (Retention) versehen war. A smoke product was produced analogously to Example 2, which however with a ventilated (18% filter ventilation) monoacetate filter 20 mm long and 36% retention (Retention) was provided.

Bewertung: Deutlich reduzierter Kräftigkeitseindruck gegenüber dem Produkt nach Beispiel 2 bei typischem American-Blend-Aroma. Die sonst einer American-Blend-Mischung anhaftende Rauhigkeit war hier nicht mehr feststellbar.Assessment: Significantly reduced impression of strength compared to the product according to Example 2 with a typical American blend flavor. The roughness that was otherwise inherent in an American blend mixture no longer ascertainable here.

Beispiel 5Example 5

Es wurde ein Rauchprodukt analog Beispiel 2 hergestellt, wobei jedoch das Umblatt nach einem Papierherstellungsverfahren ohne Extraktrückführung nach TF-2 erhalten worden war und eine Porosität von 133 Coresta-Einheiten und ein Gewicht von 52 g/m2 aufwies. Die Tabakmischung bestand aus 100 % Lamina-Tabak Die Tabakfolie enthielt, bezogen auf deren Trockengewicht, neben 10 Gew.% langfaseriger Fremdcellulose noch 75 Gew.% Laminatabak nebst CaCO3: 8,0 Gew.% TiO2: 3,8 Gew.% Na-acetat: 1,8 Gew.% Extrakt: 1,4 Gew.% A smoking product was produced analogously to Example 2, but the binder was obtained by a paper production process without extract recycling according to TF-2 and had a porosity of 133 Coresta units and a weight of 52 g / m 2 . The tobacco mixture consisted of 100% lamina tobacco. Based on its dry weight, the tobacco film also contained 75% by weight of laminate tobacco in addition to 10% by weight of long-fiber foreign cellulose CaCO 3: 8.0% by weight TiO 2 : 3.8% by weight Na acetate: 1.8% by weight Extract: 1.4% by weight

Bewertung: American Blend; leichte Schärfe, gutes Aroma, wie bei dem Produkt gemäß Beispiel 2, Nebenrauch sehr aromatisch, wenig cellulosig.Review: American Blend; slight sharpness, good aroma, as with the product according to Example 2, secondary smoke very aromatic, little cellulosic.

Beispiel 6Example 6

Es wurde ein Rauchprodukt analog Beispiel 2 hergestellt, wobei jedoch das Deckblatt mit einer anderen Rezeptur nach TF-1 hergestellt worden war; die einzelnen Werte waren: Porosität 78 Coresta-Einheiten Gewicht 48,2 g/m2 Extrakt 29,3 Gew.% CaCO3 5,8 Gew.% TiO2 1,7 Gew.% Na-acetat 2,2 Gew.% Fremdcellulose 15,0 Gew.% Rippen 27,6 Gew.% Virginia-Lamina 18,4 Gew.% A smoking product was produced in the same way as in Example 2, but the cover sheet was produced using a different recipe according to TF-1; the individual values were: porosity 78 Coresta units Weight 48.2 g / m 2 extract 29.3% by weight CaCO 3 5.8% by weight TiO 2 1.7% by weight Na acetate 2.2% by weight Foreign cellulose 15.0% by weight Ribs 27.6% by weight Virginia Lamina 18.4% by weight

Bewertung: Blendcharakter mit einer leichten, süßen Schärfe eines typischen hocharomatisierten US-Orange-leaf-tabaks bei ausgewogener Kräftigkeit.Evaluation: Blend character with a slight, sweet sharpness of one typical highly flavored US orange leaf tobacco with balanced Vigor.

Vergleich Beispiel 7comparison Example 7

Es wurde ein Rauchprodukt analog Beispiel 6 hergestellt, wobei jedoch das Deckblatt nicht aus Tabakrippenmaterial und Lamina, sondern unter Verwendung der entsprechenden Menge, nämlich 46 Gew.% Tabakstengeln hergestellt wurde.A smoke product was produced analogously to Example 6, wherein but the cover sheet is not made of tobacco rib material and lamina, but using the appropriate amount, namely 46% by weight of tobacco stems was produced.

Bewertung: Erhöhte Schärfe bei sonst unveränderter Charakteristik des Aromas; deutlich bessere Oberflächenstruktur; die Verarbeitbarkeit war hinsichtlich der Reißfestigkeit deutlich besser.Evaluation: Increased sharpness with otherwise unchanged characteristics of the aroma; significantly better surface structure; the processability was significantly better in terms of tear strength.

Vergleich Beispiel 8comparison Example 8

Es wurd ein Rauchprodukt analog Beispiel 6 hergestellt, wobei jedoch der Tabakrippenanteil von 27,6 Gew.% durch die gleiche Menge an Tabakstengeln ersetzt wurde.A smoke product was produced analogously to Example 6, wherein however, the tobacco rib fraction of 27.6% by weight by the same Amount of tobacco stems was replaced.

Bewertung: Sensorisch wie das Produkt gemäß Beispiel 6; hinsichtlich Oberflächenstruktur und Verarbeitbarkeit entsprach das Produkt etwa dem gemäß Beispiel 7.Evaluation: Sensory as the product according to Example 6; regarding This corresponded to the surface structure and workability Product approximately that according to Example 7.

Bei einer weiteren Ausführungsform der Erfindung ist das Rauchprodukt so ausgebildet, daß die äußerste Lage des Mantels als eine mit Filter versehene Hülse aus spiralförmig gewickelter und/oder blattförmig mit axialem Überlappungsbereich jeweils zumindest teilweise verklebter Tabakfolie geformt ist, in die der von der inneren Tabakfolie umhüllte Kern aus Rauchtabak einführbar ist, wobei die innere Tabakfolie gegebenenfalls auch aus mehreren Lagen bestehen kann. Je nach den Gegebenheiten kann entweder die äußerste Lage oder die innere Lage bzw. Tabakfolie hochporös sein, wobei dann die jeweilige andere Lage weniger porös ist; auch Mischformen hinsichtlich der Porosität sind durchführbar, solange ein insgesamt abrauchbares Produkt erhalten wird.In a further embodiment of the invention that is Smoke product designed so that the outermost layer of the jacket as a filter-provided sleeve made of spirally wound and / or in sheet form with an axial overlap area in each case at least partially glued tobacco foil is formed, in which the core of smoking tobacco covered by the inner tobacco foil can be inserted is, the inner tobacco film optionally also made of can consist of several layers. Depending on the circumstances either the outermost layer or the inner layer or tobacco foil be highly porous, with the respective other layer less is porous; mixed forms with regard to porosity are also feasible as long as an overall smokable product is obtained becomes.

Claims (20)

  1. Rod-like smoking product having a strand-shaped core of chopped smoking tobacco, which is surrounded by a jacket of one or more layers of tobacco sheets produced according to a paper manufacturing process from tobacco cellulose, tobacco extract, foreign cellulose and conventional additives, wherein the outermost layer is wound around the smoking product spirally at an acute angle to the longitudinal axis of the smoking product as a strip-like-cover sheet and is at least partly adhered, and at least one of these layers enveloping the core is an axially adhered tobacco sheet, which is composed as follows:
    a) 75 to 100 % by weight components peculiar to tobacco substantially consisting of tobacco cellulose and tobacco extract, which were obtained both from a cut tobacco mixture and from tobacco rib material;
    b) 0 to 20 % wt. foreign cellulose and
    c) 0 to 15 % wt. conventional additives such as binders, fillers, agents modifying combustion, and aroma materials,
    characterised in that
    d) the tobacco cellulose originates from a cut tobacco mixture and tobacco rib material in the ratio of 1:1.1 to 1:5, and
    e) the tobacco extract is present in a quantity of more than 20 % wt. relative to the dry substance of the tobacco sheet,
    f) the tobacco extract was obtained from a chopped lamina of leaf tobacco mixture and from tobacco rib material in the ratio by mass of 1:5.
  2. Smoking product according to claim 1, characterised in that in the tobacco sheet (TF-1) the mixture ratio of chopped leaf tobacco mixture or tobacco fines to tobacco rib material is in the range from 1:1.5 to 1:2.5.
  3. Smoking product according to claim 1 or 2, characterised in that the chopped leaf tobacco mixture or tobacco fines, from which the tobacco sheet (TF-1) was obtained contains
    30 to 40 5 wt. Virginia tobacco
    35 to 55 5 wt. Burley tobacco
    5 to 10 % wt. Orient tobacco and
    1 to 10 % wt. swelling ribs of Virginia tobacco
    with a particle size of at least 1.75 mm.
  4. Smoking product according to claim 1 to 3, characterised in that the tobacco rib material from which the tobacco sheet (TF-1) was obtained consists predominantly of heat-treated Virginia tobacco ribs with a length of about 30 mm.
  5. Smoking product according to claim 1 to 4, characterised in that in the manufacture of the tobacco sheet (TF-1) the tobacco extract was applied in a quantity of more than 20 % wt. relative to the dry substance of the tobacco sheet.
  6. Smoking product according to claim 5, characterised in that the tobacco extract consists of
    a) an extract obtained at a relatively high temperature from chopped leaf tobacco and tobacco rib material,
    b) of an extract obtained at a relatively high temperature from tobacco rib material,
    c) very volatile extracted aroma substances which are water-soluble and non-water soluble.
  7. Smoking product according to claim 1 to 6, characterised in that the tobacco sheet (TF-1) contains up to 12 % wt. calcium carbonate and up to 2 % wt. sodium or potassium citrate or acetate.
  8. Smoking product according to claim 1 to 7, characterised in that a further tobacco sheet (TF-2) of the jacket is provided, which relative to the dry substance weight of the tobacco sheet consists of the following components ground wet individually or at least partly together:
    a) 75 to 80 % wt. leaf tobacco consisting substantially of lamina and
    b) 10 to 20 % wt. long-fibre cellulose and
    c) 0 to 15 % wt. conventional additives such as binders, fillers, agents modifying combustion and aroma substances.
  9. Smoking product according to claim 8, characterised in that the long-fibre cellulose was obtained from manila, sisal, flax, hemp, soft wood or their mixtures.
  10. Smoking product according to claim 8 and 9, characterised in that the tobacco sheet (TF-2) contains up to 12% wt. calcium carbonate and/or up to 4 % wt. titanium dioxide and/or up to 2 % wt. sodium or potassium citrate or acetate.
  11. Smoking product according to claim 8 to 10, characterised in that the tobacco sheet (TF-2) corresponds in its tobacco mixture composition important for taste to the composition of the cut tobacco mixture of the strand-like core.
  12. Smoking product according to claim 7 to 11, characterised in that one of the tobacco sheets of the jacket is provided as an external spirally wound cover leaf sheet, and the other tobacco sheet as an axially adhered surrounding leaf sheet.
  13. Smoking product according to claim 1 to 12, characterised in that the porosity of the jacket consisting of cover leaf and surrounding leaf is larger than 30 and less than 1000 Coresta units and is capable of being smoked on its own.
  14. Smoking product according to claim 1 to 13, characterised in that it is provided with a conventional, optionally ventilated filter mouthpiece.
  15. Use of a smoking product according to claim 1 to 13 as a cigarillo capable of being inserted into a conventional filter cigarette sleeve.
  16. Smoking product according to claim 1 to 11, characterised in that the porosity of the jacket consisting of the cover leaf and the surrounding leaf is more than 10 000 Coresta units and is not capable of being smoked on its own.
  17. Use of a smoking product according to claim 16 as a cigarillo insertable in a conventional filter cigarette sleeve.
  18. Smoking product according to claim 1 to 13 and 16, characterised in that the chopped smoking tobacco of the core has an average cut width of about 2.2 mm.
  19. Smoking product according to claim 18, characterised in that the tobacco types in the core consist of chopped smoking tobacco and have the following average cut widths:
    Burley: 2.0 mm
    Swelling tobacco: 2.1 mm
    Virginia: 2.2 mm
    Orient: 2.5 mm.
  20. Smoking product according to claim 1 to 14, 16, 18 and 19, characterised in that the outermost layer of the jacket is formed as a sleeve provided with a filter and consisting of tobacco sheet which is spiral-wound and/or at least partially adhered in the form of a leaf with an axial overlap region, into which sheet the core of smoking tobacco enveloped by the inner tobacco sheet is insertable.
EP94115638A 1993-10-07 1994-10-05 Rod-shaped smoking article Expired - Lifetime EP0658317B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE4334222 1993-10-07
DE4334222A DE4334222C3 (en) 1993-10-07 1993-10-07 Stick-shaped smoking product

Publications (3)

Publication Number Publication Date
EP0658317A2 EP0658317A2 (en) 1995-06-21
EP0658317A3 EP0658317A3 (en) 1995-08-23
EP0658317B1 true EP0658317B1 (en) 2000-08-16

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EP94115638A Expired - Lifetime EP0658317B1 (en) 1993-10-07 1994-10-05 Rod-shaped smoking article

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US (1) US5617881A (en)
EP (1) EP0658317B1 (en)
AT (1) ATE195405T1 (en)
CA (1) CA2133785C (en)
CZ (1) CZ289068B6 (en)
DE (1) DE19512535A1 (en)
EE (1) EE03145B1 (en)
HR (1) HRP940578B1 (en)
HU (2) HU9402892D0 (en)
LT (1) LT3637B (en)
LV (1) LV11097B (en)
MD (1) MD1289C2 (en)
PL (1) PL178311B1 (en)
RU (1) RU2114538C1 (en)
SI (1) SI9400378B (en)
SK (1) SK282288B6 (en)

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CN103798949B (en) * 2014-03-11 2016-02-24 云南瑞升烟草技术(集团)有限公司 A kind of modified particle preparation method for recombination tobacco leaf
US20160073686A1 (en) * 2014-09-12 2016-03-17 R.J. Reynolds Tobacco Company Tobacco-derived filter element
CN113951540A (en) 2014-09-30 2022-01-21 菲利普莫里斯生产公司 Method for producing homogenized tobacco material
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CN113749284B (en) * 2015-05-21 2023-01-13 菲利普莫里斯生产公司 Method for producing an inductively heatable tobacco rod
US11044939B2 (en) 2015-08-28 2021-06-29 Philip Morris Products S.A. Tubular elements for smoking articles
GB201707767D0 (en) 2017-05-15 2017-06-28 British American Tobacco Investments Ltd Method of making a tobacco extract
GB201707758D0 (en) 2017-05-15 2017-06-28 British American Tobacco Investments Ltd Ground tobacco composition
GB201707761D0 (en) 2017-05-15 2017-06-28 British American Tobacco Investments Ltd Method of making a tobacco extract
JP7494113B2 (en) 2017-11-28 2024-06-03 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム Aerosol-generating article having a mouthpiece with modified structure
CN108978222B (en) * 2018-07-11 2021-06-11 常州龙途新材料科技有限公司 Biodegradable composite fiber yarn capable of volatilizing fragrance and preparation and application processes
WO2020246036A1 (en) * 2019-06-07 2020-12-10 日本たばこ産業株式会社 Tobacco sheet, tobacco rod and smoking article
KR102605497B1 (en) * 2021-04-29 2023-11-22 주식회사 케이티앤지 Tobacco extract sheet, method for manufacturing the same and smoking article including the same
WO2024036779A1 (en) * 2022-08-18 2024-02-22 云南中烟工业有限责任公司 Multi-layer composite cigarette paper structure for easy flavoring and manufacturing method

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HU9402892D0 (en) 1995-01-30
LV11097A (en) 1996-04-20
CA2133785C (en) 2000-03-07
CZ289068B6 (en) 2001-10-17
LV11097B (en) 1996-08-20
CA2133785A1 (en) 1995-04-08
PL178311B1 (en) 2000-04-28
HUT71854A (en) 1996-02-28
HRP940578A2 (en) 1996-08-31
ATE195405T1 (en) 2000-09-15
LT3637B (en) 1996-01-25
EE03145B1 (en) 1999-02-15
HU214187B (en) 1998-01-28
SK122294A3 (en) 1995-04-12
EP0658317A3 (en) 1995-08-23
EP0658317A2 (en) 1995-06-21
CZ247994A3 (en) 1995-06-14
US5617881A (en) 1997-04-08
SI9400378B (en) 2001-12-31
MD1289B2 (en) 1999-08-30
MD940381A (en) 1996-02-29
SK282288B6 (en) 2002-01-07
HU9402899D0 (en) 1995-01-30
DE19512535A1 (en) 1996-10-10
MD1289C2 (en) 2000-10-31
RU2114538C1 (en) 1998-07-10
PL305350A1 (en) 1995-04-18
LTIP2044A (en) 1995-05-25
HRP940578B1 (en) 1999-10-31
RU94039293A (en) 1996-09-20
SI9400378A (en) 1995-04-30
HK1013606A1 (en) 1999-09-03

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