EP0363971A3 - Verfahren zur Entfernung von Terpenen aus etherischen Ölen - Google Patents

Verfahren zur Entfernung von Terpenen aus etherischen Ölen Download PDF

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Publication number
EP0363971A3
EP0363971A3 EP19890119001 EP89119001A EP0363971A3 EP 0363971 A3 EP0363971 A3 EP 0363971A3 EP 19890119001 EP19890119001 EP 19890119001 EP 89119001 A EP89119001 A EP 89119001A EP 0363971 A3 EP0363971 A3 EP 0363971A3
Authority
EP
European Patent Office
Prior art keywords
essential oils
terpenes
adsorbent
loaded
separating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP19890119001
Other languages
English (en)
French (fr)
Other versions
EP0363971A2 (de
EP0363971B1 (de
Inventor
Jan Dr. Cully
Erwin Dr. Schütz
Heinz-Rüdiger Dr. Vollbrecht
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
SKW Trostberg AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SKW Trostberg AG filed Critical SKW Trostberg AG
Publication of EP0363971A2 publication Critical patent/EP0363971A2/de
Publication of EP0363971A3 publication Critical patent/EP0363971A3/de
Application granted granted Critical
Publication of EP0363971B1 publication Critical patent/EP0363971B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/022—Refining

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Gas Separation By Absorption (AREA)
  • Lubricants (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

Es wird ein Verfahren zur Entfernung von Terpenen aus etheri­ schen Ölen beschrieben, wobei man
  • a) die terpenhaltigen etherischen Öle mit einem polaren Feststoff (Adsorbens) kontaktiert,
  • b) eine Abtrennung des beladenen Adsorbens von der flüssi­ gen, mit Terpenen angereicherten Phase vornimmt und
  • c) das mit etherischem Öl beladene Adsorbens einer Extrak­ tion mit verdichtetem CO₂ unterwirft.
    • Auf diese Weise kann man die Terpene weitgehend entfernen und gleichzeitig die etherischen Öle in hoher Ausbeute und guter Qualität gewinnen.
    EP89119001A 1988-10-14 1989-10-12 Verfahren zur Entfernung von Terpenen aus etherischen Ölen Expired - Lifetime EP0363971B1 (de)

    Applications Claiming Priority (2)

    Application Number Priority Date Filing Date Title
    DE3834988 1988-10-14
    DE3834988A DE3834988A1 (de) 1988-10-14 1988-10-14 Verfahren zur entfernung von terpenen aus etherischen oelen

    Publications (3)

    Publication Number Publication Date
    EP0363971A2 EP0363971A2 (de) 1990-04-18
    EP0363971A3 true EP0363971A3 (de) 1991-03-20
    EP0363971B1 EP0363971B1 (de) 1995-04-19

    Family

    ID=6365099

    Family Applications (1)

    Application Number Title Priority Date Filing Date
    EP89119001A Expired - Lifetime EP0363971B1 (de) 1988-10-14 1989-10-12 Verfahren zur Entfernung von Terpenen aus etherischen Ölen

    Country Status (10)

    Country Link
    US (1) US5061502A (de)
    EP (1) EP0363971B1 (de)
    JP (1) JP2541670B2 (de)
    AT (1) ATE121447T1 (de)
    DE (2) DE3834988A1 (de)
    ES (1) ES2070877T3 (de)
    GR (1) GR3015902T3 (de)
    MX (1) MX171557B (de)
    RU (1) RU1769761C (de)
    ZA (1) ZA897691B (de)

    Families Citing this family (13)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    US6124477A (en) * 1996-06-27 2000-09-26 Bioavailability Systems, Llc Anti-first-pass effect compounds
    US20040058982A1 (en) * 1999-02-17 2004-03-25 Bioavailability System, Llc Pharmaceutical compositions
    US6248776B1 (en) * 1997-08-26 2001-06-19 Bioavailability Systems, L.L.C. Anti-first-pass effect compounds
    US6063809A (en) * 1997-08-26 2000-05-16 Bioavailability Systems, Llc Anti-first-pass effect compounds
    GB0027047D0 (en) 2000-11-06 2000-12-20 Ici Plc Process for reducing the concentration of undesired compounds in a composition
    JP2003001002A (ja) * 2001-06-18 2003-01-07 Higashimaru Shoyu Co Ltd 液状物の抽出方法
    ITMI20031390A1 (it) * 2003-07-08 2005-01-09 Turispharma S R L Metodo di estrazione di strutture molecolari attive da resine naturali e/o da oli essenziali.
    US7727401B2 (en) 2004-11-09 2010-06-01 Air Products And Chemicals, Inc. Selective purification of mono-terpenes for removal of oxygen containing species
    ATE466065T1 (de) * 2006-02-10 2010-05-15 Carotech Sdn Bhd Verfahren zur gewinnung hochangereicherter naturstoff-fraktionen aus palmöl unter verwendung von superkritischen und beinahe superkritischen flüssigmedien
    CA2926093C (en) * 2013-10-28 2019-11-12 Totally Natural Solutions Ltd Fractionation of hop oils using liquid and supercritical carbon dioxide.
    EP3002327A1 (de) * 2014-10-02 2016-04-06 Sensient Flavors Limited Verfahren zur Modifikation der Zusammensetzung von ätherischen Ölen
    US11078137B1 (en) * 2019-03-08 2021-08-03 Buddies IP Holding, Inc. Sustainable terpene extraction method
    CN111363624B (zh) * 2020-03-26 2022-06-21 华东理工大学 一种精油脱萜烯的方法

    Citations (3)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    US2712008A (en) * 1951-06-29 1955-06-28 Justus G Kirchner Production of terpeneless essential oils
    US3867262A (en) * 1973-05-21 1975-02-18 Us Agriculture Production of terpeneless essential oils
    EP0206738A2 (de) * 1985-06-19 1986-12-30 The Procter & Gamble Company Verfahren zur Herstellung von Zitrusaroma und Aromazusammensetzungen

    Family Cites Families (8)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    US3294550A (en) * 1961-10-12 1966-12-27 Robert M Ikeda Production of full-flavored stable essential oils
    US3477856A (en) * 1965-11-10 1969-11-11 Us Agriculture Process for extraction of flavors
    JPS5410539A (en) * 1977-06-24 1979-01-26 Matsushita Electric Works Ltd Door
    JPS59117593A (ja) * 1982-12-24 1984-07-06 長谷川香料株式会社 天然精油の精製方法
    JPS6135802A (ja) * 1984-07-27 1986-02-20 Daicel Chem Ind Ltd 有機物の抽出方法
    JPH0664032B2 (ja) * 1985-10-12 1994-08-22 出光石油化学株式会社 超臨界流体による混合物からの特定成分の分離方法
    JPS63118399A (ja) * 1986-11-07 1988-05-23 株式会社資生堂 テルペンレス精油
    JPS6416A (en) * 1986-12-23 1989-01-05 Santen Pharmaceut Co Ltd Remedy for arthritis

    Patent Citations (3)

    * Cited by examiner, † Cited by third party
    Publication number Priority date Publication date Assignee Title
    US2712008A (en) * 1951-06-29 1955-06-28 Justus G Kirchner Production of terpeneless essential oils
    US3867262A (en) * 1973-05-21 1975-02-18 Us Agriculture Production of terpeneless essential oils
    EP0206738A2 (de) * 1985-06-19 1986-12-30 The Procter & Gamble Company Verfahren zur Herstellung von Zitrusaroma und Aromazusammensetzungen

    Non-Patent Citations (4)

    * Cited by examiner, † Cited by third party
    Title
    CHEMICAL ABSTRACTS, vol. 99, no. 12, September 1983 Columbus, Ohio, USA ref. no. 93512A *
    CHEMIE. INGENIEUR. TECHNIK. vol. 56, 1984, WEINHEIM DE Seiten 794 - 795; D.Gerard: "Kontinuierliche Deterpenierung ätherischer Oele durch Gegenstromextration mit verdichtem Kohlendioxid" *
    FOOD TECHNOLOGY. vol. 42, no. 6, Juni 1988, CHICAGO US Seiten 145 - 150; F.Temelli et al.: "Supercritical fluid extraction in citrus oil processing" *
    RIECHSTOFFE AROMEN KORPERPFLEGEMITTEL. no. 2-3, 1976, HANNOVER-BEMRODE DE Seiten 28 - 33; S.Anandaraman et al.: "Untersuchung über die Deterpenisierung einiger Orangen-Oele auf chromatographischem Wege" *

    Also Published As

    Publication number Publication date
    JP2541670B2 (ja) 1996-10-09
    EP0363971A2 (de) 1990-04-18
    ES2070877T3 (es) 1995-06-16
    MX171557B (es) 1993-11-05
    ATE121447T1 (de) 1995-05-15
    JPH02180997A (ja) 1990-07-13
    GR3015902T3 (en) 1995-07-31
    RU1769761C (en) 1992-10-15
    ZA897691B (en) 1990-07-25
    DE3834988A1 (de) 1990-04-19
    US5061502A (en) 1991-10-29
    EP0363971B1 (de) 1995-04-19
    DE58909186D1 (de) 1995-05-24

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