EP0325541B1 - Procédé d'isolation entre zones de production d'un puits et dispositif de mise en oeuvre de ce procédé - Google Patents
Procédé d'isolation entre zones de production d'un puits et dispositif de mise en oeuvre de ce procédé Download PDFInfo
- Publication number
- EP0325541B1 EP0325541B1 EP89400163A EP89400163A EP0325541B1 EP 0325541 B1 EP0325541 B1 EP 0325541B1 EP 89400163 A EP89400163 A EP 89400163A EP 89400163 A EP89400163 A EP 89400163A EP 0325541 B1 EP0325541 B1 EP 0325541B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- well
- membrane
- tubing string
- confinement
- axial
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims description 30
- 230000008569 process Effects 0.000 title description 6
- 239000012528 membrane Substances 0.000 claims description 110
- 238000004519 manufacturing process Methods 0.000 claims description 93
- 238000002347 injection Methods 0.000 claims description 35
- 239000007924 injection Substances 0.000 claims description 35
- 230000009471 action Effects 0.000 claims description 34
- 239000012530 fluid Substances 0.000 claims description 24
- 238000000926 separation method Methods 0.000 claims description 19
- 239000000463 material Substances 0.000 claims description 17
- 229920001971 elastomer Polymers 0.000 claims description 15
- 239000000806 elastomer Substances 0.000 claims description 15
- 238000011065 in-situ storage Methods 0.000 claims description 12
- 229920001296 polysiloxane Polymers 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000004132 cross linking Methods 0.000 claims description 7
- 239000003822 epoxy resin Substances 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 238000012856 packing Methods 0.000 claims description 5
- 229920000647 polyepoxide Polymers 0.000 claims description 5
- 229920006295 polythiol Polymers 0.000 claims description 5
- 229920001568 phenolic resin Polymers 0.000 claims description 4
- 239000005011 phenolic resin Substances 0.000 claims description 4
- 238000009826 distribution Methods 0.000 claims description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims 1
- 240000005428 Pistacia lentiscus Species 0.000 description 15
- 239000013521 mastic Substances 0.000 description 14
- 239000000565 sealant Substances 0.000 description 12
- 239000004568 cement Substances 0.000 description 6
- 239000011435 rock Substances 0.000 description 6
- 238000007789 sealing Methods 0.000 description 6
- 238000005304 joining Methods 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 239000003566 sealing material Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 229920001021 polysulfide Polymers 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 150000008360 acrylonitriles Chemical class 0.000 description 2
- 230000006978 adaptation Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002825 nitriles Chemical class 0.000 description 2
- 239000005077 polysulfide Substances 0.000 description 2
- 150000008117 polysulfides Polymers 0.000 description 2
- 239000010802 sludge Substances 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- 239000004971 Cross linker Substances 0.000 description 1
- 240000000018 Gnetum gnemon Species 0.000 description 1
- 235000008612 Gnetum gnemon Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 230000003042 antagnostic effect Effects 0.000 description 1
- 239000010692 aromatic oil Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000003129 oil well Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
Images
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B33/00—Sealing or packing boreholes or wells
- E21B33/10—Sealing or packing boreholes or wells in the borehole
- E21B33/13—Methods or devices for cementing, for plugging holes, crevices or the like
- E21B33/134—Bridging plugs
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B33/00—Sealing or packing boreholes or wells
- E21B33/10—Sealing or packing boreholes or wells in the borehole
- E21B33/12—Packers; Plugs
- E21B33/126—Packers; Plugs with fluid-pressure-operated elastic cup or skirt
Definitions
- the present invention relates to a method for manufacturing in situ a seal between an inner wall portion of an oil well, or the like, and an outer wall portion of a production column (or exploitation ) of this well, as well as a device for implementing this method.
- the invention also relates to a method of isolating (or separating) between at least two production zones of a well.
- casing in English terminology -saxonne: we also speak of casing in French terminology.
- sealing is obtained by cementing the aforementioned space using, sometimes, auxiliary sealing devices called inflatable cementing packers.
- These packers are O-ring seals comprising a double elastomer wall reinforced by a metal braid; this double wall delimits an inflatable chamber using cement (or water or oil) up to 1.6 times their nominal diameter, under a maximum allowable pressure of 110 to 120 bars, via a safety valves.
- US-A-4,440,226 discloses a method of completing a well using cement and comprising the steps defined in the preamble of claim 1.
- the material to be injected consists of a crosslinking mastic, which is resistant to effluents and to the temperatures and pressures existing in the well, in particular constituted by a liquid elastomer, such as a fluorinated silicone, a polysulphide or a polythioether, or by an inflatable material, such as an epoxy or phenolic resin, also resistant to the ambient conditions existing in the well.
- a crosslinking mastic which is resistant to effluents and to the temperatures and pressures existing in the well, in particular constituted by a liquid elastomer, such as a fluorinated silicone, a polysulphide or a polythioether, or by an inflatable material, such as an epoxy or phenolic resin, also resistant to the ambient conditions existing in the well.
- said axial confinement, separation and ejection membrane has an annular zone of least resistance which is intended to tear under the action of the injection pressure, the portions of the membrane thus torn closing off the above-mentioned channels and preventing the reflux of the fluids expelled by the injection pressure into this space, which is thus completely filled with the sealing material.
- said axial confinement, separation and ejection membrane is very deformable and non-tearable so as to adapt by simple deformation, under the action of pressure injection, irregularities in the internal surface of the well.
- said chamber defined by the axial confinement, separation and ejection membrane together with said portion of the external wall of the column, contains a liquid elastomer, such as a fluorinated silicone, a polysulfide or a polythioether, which adapts to irregularities in the wall of the well and which is resistant to effluents as well as to the temperatures and high pressures existing in the well.
- a liquid elastomer such as a fluorinated silicone, a polysulfide or a polythioether
- said chamber defined by the axial confinement, separation and ejection membrane together with said portion of the outer wall of the column, contains an inflatable material, such as an epoxy resin or phenolic, also resistant to the ambient conditions existing in the well.
- an inflatable material such as an epoxy resin or phenolic
- the two radial confinement membranes have internal and external ends which cooperate with means allowing their joining to the production column, said joining means ensuring the fixing of the internal and external ends or the sliding of these. ci along the production column, under the action of the inflation pressure of each radial confinement membrane, or the fixing of one and the sliding of the other.
- the present invention further relates to a method of isolation (or separation) between at least two production zones of a well, separated by an axial gap, characterized in that one manufactures in situ between the well and a column production of this well, a seal at least at each of the ends of the aforementioned gap between the two production areas, using the method and the implementation device in accordance with the foregoing provisions.
- zones Z1 and Z2 illustrated in FIG. 6 To isolate (or separate) two production zones, such as zones Z1 and Z2 illustrated in FIG. 6, from a well P, it is necessary to prevent any communication between them by the annular space 5 separating the well P of its production column T over the entire height H of the interval between the two zones Z1 and Z2.
- the present invention provides a solution which, although not intended to systematically replace the
- the aim of the cementing technique is to reduce it as much as possible (for example, by limiting it - for practical reasons of surface exploitation - to the only upper part of the well, as illustrated schematically by the reference C in Figure 6 ) with significant advantages (compared to the assisted cementing technique, possibly by the use of inflatable cementation packers), some of which have been mentioned under A) to E).
- the insulation between two zones Z1 and Z2 is obtained by manufacturing in situ seals 18 at the ends of the gap H separating the two zones, each joint being obtained by a prior step of delimitation of the annular space intended to be occupied by the seal, followed by a step of injecting into the annular space thus delimited, a material capable not only of completely filling this space, but also of adapting perfectly to the irregularities in the rock delimiting the internal wall of the well.
- the crosslinking time can be between approximately 1 hour and approximately 24 hours, depending on the temperature existing at the injection of the sealant as well as the needs of the operation.
- the in situ manufacturing process for the seal provides for the separation of the sealant from the mud during injection, while ejecting the mud from the space which must be occupied by the sealant.
- a device 1 essentially comprising two means for confining the annular space to be sealed and means for separating the putty to be injected from the mud, and for ejecting it. this outside the space that needs to be filled with putty.
- the containment means consist of two identical elastomeric annular membranes, 2, which are applied against the external surface of the production column T.
- each confinement membrane 2 and the production column T there is a chamber 6 inflatable using a pressurized fluid, such as water or oil, which expands the membrane radially (cf. FIG. 2) under the action of the inflation pressure, until it comes into contact with the wall of the well P, thus delimiting the space 5 to be sealed.
- a pressurized fluid such as water or oil
- the internal ends 3 (relative to the space 5) of each of these membranes are fixedly secured to the column T by means (not shown, as known to technicians in the field). material) which at the same time inject the inflation fluid into the containment membranes.
- the device for implementing the method according to the invention comprises a third membrane 8, the ends 9 and 10 of which are connected to the internal ends 3 of the containment membranes 2 and fixedly secured to the column T together with the ends 3.
- the presence of the membrane 8 therefore makes it possible to effect the injection of the mastic 11 (of course, through the wall of the production column T) in the chamber 20 delimited between the membrane 8 and the column T, so that that -this does not come into contact with the mud existing in space 5.
- each of the containment membranes 2 has axial grooves 12 (see also FIG. 5) distributed uniformly around the periphery of each membrane. These grooves define channels 13 when the membranes come into contact with the internal wall of the well P.
- the mud existing in the space 5 is therefore ejected outside this space by the passage channels 13 under the action of the mastic injection pressure (the pressure difference between the mastic pressure and the pressure of the completion sludge existing in the space to be sealed is, for example, of the order of about 30 bars) on the membrane partition 8, which - as can be seen in Figure 3 - also has the role of guiding the distribution of the sealant 11 in space 5.
- the separation membrane 8 has an annular zone 15 of less resistance which tears under the action of the pressure d injection, when the membrane has expanded until most of the mud has been ejected through the channels 13.
- the tearing of the membrane 8 divides it into two portions 16 and 17 which seal the channels 13 at the end of the injection of the putty and which prevent the reflux of the mud towards the space 5: in this way, the crosslinking of the putty takes place in the best conditions thus obtaining a perfectly tight seal 18.
- Figures 1 to 4 schematically represent the different stages of manufacture of the seal 18, using the device 1 for implementing this method.
- FIG. 1 illustrates the phase prior to the execution of the manufacturing process, which includes the descent into the well P of the production column T equipped with a device 1 pressed against the external surface of the column: it is possible to appreciate that because of the relatively thin thickness of the membranes constituting the device 1, there is a relatively large space between the latter and the well P, which avoids the problems of ramming and damage existing with the cement packers inflatable from the prior art.
- the reduction in thickness, in particular of the containment membranes 2 is due to the fact that the latter, in the inflated state, do not constitute seals but, as has been specified above, essentially provisional means confinement of the annular space 5 to be sealed.
- FIG. 2 illustrates the first step of the process for manufacturing the seal 18, which consists in delimiting the space 5 by inflating the chambers 6 delimited between each confinement membrane 2 and the production column T.
- FIG. 3 illustrates the second phase of the process for manufacturing the seal 18, consisting in injecting the putty 11 into the chamber 20 delimited between the separation membrane 8 and the production column T.
- FIG. 4 illustrates the situation existing at the end of the second step, when the portions 16 and 17 of the separation membrane 8, torn at its zone of least resistance 15, close the passage channels 13 thus preventing the reflux of the mud through these channels and allowing the complete filling of the space 5 with the putty 11 so as to produce a perfect seal, 18.
- the invention is in no way limited to those of its modes of implementation, embodiment and application which have just been described more explicitly; on the contrary, it embraces all the variants which may come to the mind of the technician in the matter, without departing from the framework, or the scope, of the present invention.
- the injection of sealant can be done through an orifice formed in the wall of the production column T (and, of course, normally closed by a valve sensitive to a certain pressure threshold ) and this by descending inside the column an injection device
- other systems can be used for this purpose.
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- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mining & Mineral Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Fluid Mechanics (AREA)
- Physics & Mathematics (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Transformer Cooling (AREA)
- Disintegrating Or Milling (AREA)
- Extraction Or Liquid Replacement (AREA)
- Consolidation Of Soil By Introduction Of Solidifying Substances Into Soil (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR8800595 | 1988-01-20 | ||
FR8800595A FR2626040B1 (fr) | 1988-01-20 | 1988-01-20 | Procede d'isolation entre zones de production d'un puits et dispositif de mise en oeuvre de ce procede |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0325541A1 EP0325541A1 (fr) | 1989-07-26 |
EP0325541B1 true EP0325541B1 (fr) | 1992-12-02 |
Family
ID=9362459
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP89400163A Expired - Lifetime EP0325541B1 (fr) | 1988-01-20 | 1989-01-19 | Procédé d'isolation entre zones de production d'un puits et dispositif de mise en oeuvre de ce procédé |
Country Status (7)
Country | Link |
---|---|
US (1) | US4913232A (es) |
EP (1) | EP0325541B1 (es) |
CA (1) | CA1337043C (es) |
DE (2) | DE68903642T2 (es) |
ES (1) | ES2010495T3 (es) |
FR (1) | FR2626040B1 (es) |
NO (1) | NO890241L (es) |
Families Citing this family (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5791416A (en) * | 1995-07-13 | 1998-08-11 | White; Kenneth M. | Well completion device and method of cementing |
FR2737533B1 (fr) * | 1995-08-04 | 1997-10-24 | Drillflex | Manchon tubulaire gonflable pour tuber ou obturer un puits ou une canalisation |
US5671809A (en) * | 1996-01-25 | 1997-09-30 | Texaco Inc. | Method to achieve low cost zonal isolation in an open hole completion |
EP1283939B1 (en) | 2000-05-22 | 2007-09-19 | Shell Internationale Researchmaatschappij B.V. | Method for plugging a well with a resin |
US6446717B1 (en) * | 2000-06-01 | 2002-09-10 | Weatherford/Lamb, Inc. | Core-containing sealing assembly |
US6612372B1 (en) | 2000-10-31 | 2003-09-02 | Weatherford/Lamb, Inc. | Two-stage downhole packer |
MY135121A (en) | 2001-07-18 | 2008-02-29 | Shell Int Research | Wellbore system with annular seal member |
FR2831597B1 (fr) * | 2001-10-30 | 2004-02-13 | Geoservices | Dispositif de completion d'une installation d'exploitation de fluides souterrains |
CA2449518C (en) * | 2001-12-12 | 2007-01-30 | Weatherford/Lamb, Inc. | Bi-directional and internal pressure trapping packing element system |
US6769491B2 (en) | 2002-06-07 | 2004-08-03 | Weatherford/Lamb, Inc. | Anchoring and sealing system for a downhole tool |
US6854522B2 (en) * | 2002-09-23 | 2005-02-15 | Halliburton Energy Services, Inc. | Annular isolators for expandable tubulars in wellbores |
GB2428062B (en) * | 2004-02-13 | 2009-07-22 | Halliburton Energy Serv Inc | Annular isolators for tubulars in wellbores |
US6840325B2 (en) | 2002-09-26 | 2005-01-11 | Weatherford/Lamb, Inc. | Expandable connection for use with a swelling elastomer |
US6827150B2 (en) * | 2002-10-09 | 2004-12-07 | Weatherford/Lamb, Inc. | High expansion packer |
US6938698B2 (en) * | 2002-11-18 | 2005-09-06 | Baker Hughes Incorporated | Shear activated inflation fluid system for inflatable packers |
US6766858B2 (en) * | 2002-12-04 | 2004-07-27 | Halliburton Energy Services, Inc. | Method for managing the production of a well |
US6834725B2 (en) | 2002-12-12 | 2004-12-28 | Weatherford/Lamb, Inc. | Reinforced swelling elastomer seal element on expandable tubular |
US6907937B2 (en) * | 2002-12-23 | 2005-06-21 | Weatherford/Lamb, Inc. | Expandable sealing apparatus |
US6988557B2 (en) | 2003-05-22 | 2006-01-24 | Weatherford/Lamb, Inc. | Self sealing expandable inflatable packers |
GB0303152D0 (en) * | 2003-02-12 | 2003-03-19 | Weatherford Lamb | Seal |
GB2398582A (en) * | 2003-02-20 | 2004-08-25 | Schlumberger Holdings | System and method for maintaining zonal isolation in a wellbore |
KR20060003023A (ko) | 2003-04-17 | 2006-01-09 | 쉘 인터내셔날 리써취 마트샤피지 비.브이. | 탄화수소 혼합물로부터의 색조물 및/또는 아스팔트오염물의 분리 방법 |
US7063164B2 (en) * | 2004-04-01 | 2006-06-20 | Schlumberger Technology Corporation | System and method to seal by bringing the wall of a wellbore into sealing contact with a tubing |
GB0417328D0 (en) * | 2004-08-04 | 2004-09-08 | Read Well Services Ltd | Apparatus and method |
US7661471B2 (en) * | 2005-12-01 | 2010-02-16 | Baker Hughes Incorporated | Self energized backup system for packer sealing elements |
DK2173967T3 (da) * | 2007-06-25 | 2012-03-26 | Vestas Wind Sys As | Forseglingsindretning til et rørarrangement |
DK178742B1 (da) | 2008-03-06 | 2016-12-19 | Maersk Olie & Gas | Fremgangsmåde og apparat til injicering af et eller flere behandlingsfluider nede i et borehul |
DK178243B1 (en) * | 2008-03-06 | 2015-09-28 | Mærsk Olie Og Gas As | Fremgangsmåde til forsegling af en ringformet åbning i et borehul |
DK178489B1 (da) * | 2008-03-13 | 2016-04-18 | Maersk Olie & Gas | Værktøj og fremgangsmåde til at aflukke åbninger eller lækager i en brøndboring |
US8051913B2 (en) * | 2009-02-24 | 2011-11-08 | Baker Hughes Incorporated | Downhole gap sealing element and method |
WO2010107812A1 (en) * | 2009-03-16 | 2010-09-23 | Baker Hughes Incorporated | Rolling sleeve through tubing bridge plug |
US20120227969A1 (en) * | 2009-11-19 | 2012-09-13 | Ian Gray | External Casing Packer |
EP2636843B1 (en) | 2010-12-17 | 2014-10-08 | Welltec A/S | Well completion |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2187480A (en) * | 1938-12-12 | 1940-01-16 | Baker Oil Tools Inc | Well cementing apparatus |
US2943684A (en) * | 1958-02-13 | 1960-07-05 | Smith Ramsey | Selective hydrofracting apparatus |
US3130787A (en) * | 1960-09-12 | 1964-04-28 | James C Mason | Well bridging tool |
US3224267A (en) * | 1962-04-27 | 1965-12-21 | Texaco Inc | Well completion apparatus |
US3542127A (en) * | 1968-05-13 | 1970-11-24 | Lynes Inc | Reinforced inflatable packer with expansible back-up skirts for end portions |
US3578083A (en) * | 1969-11-12 | 1971-05-11 | Schlumberger Technology Corp | Methods and apparatus for plugging well bores with hardenable fluent substances |
FR2395389A1 (fr) * | 1977-06-21 | 1979-01-19 | Mazier Georges | Obturateur dilatable haute pression a flexible arme |
SU740935A1 (ru) * | 1978-07-18 | 1980-06-15 | Московский Ордена Трудового Красного Знамени Геологоразведочный Институт Им.С.Орджоникидзе | Устройство дл цементировани скважин |
US4440226A (en) * | 1982-12-08 | 1984-04-03 | Suman Jr George O | Well completion method |
US4484626A (en) * | 1983-04-15 | 1984-11-27 | K-V Associates, Inc. | Pneumatic packer |
US4655286A (en) * | 1985-02-19 | 1987-04-07 | Ctc Corporation | Method for cementing casing or liners in an oil well |
US4714117A (en) * | 1987-04-20 | 1987-12-22 | Atlantic Richfield Company | Drainhole well completion |
-
1988
- 1988-01-20 FR FR8800595A patent/FR2626040B1/fr not_active Expired - Fee Related
-
1989
- 1989-01-18 CA CA000588483A patent/CA1337043C/fr not_active Expired - Fee Related
- 1989-01-18 US US07/298,659 patent/US4913232A/en not_active Expired - Fee Related
- 1989-01-19 EP EP89400163A patent/EP0325541B1/fr not_active Expired - Lifetime
- 1989-01-19 DE DE8989400163T patent/DE68903642T2/de not_active Expired - Fee Related
- 1989-01-19 ES ES198989400163T patent/ES2010495T3/es not_active Expired - Lifetime
- 1989-01-19 NO NO89890241A patent/NO890241L/no unknown
- 1989-01-19 DE DE198989400163T patent/DE325541T1/de active Pending
Also Published As
Publication number | Publication date |
---|---|
DE68903642T2 (de) | 1993-04-08 |
NO890241D0 (no) | 1989-01-19 |
DE68903642D1 (de) | 1993-01-14 |
NO890241L (no) | 1989-07-21 |
FR2626040A1 (fr) | 1989-07-21 |
EP0325541A1 (fr) | 1989-07-26 |
CA1337043C (fr) | 1995-09-19 |
DE325541T1 (de) | 1989-12-28 |
ES2010495A4 (es) | 1989-11-16 |
FR2626040B1 (fr) | 1993-10-22 |
ES2010495T3 (es) | 1993-05-16 |
US4913232A (en) | 1990-04-03 |
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