EP0280690A4 - Imprägnierungsverfahren und vorrichtung mit vakuumpumpenventilregelungssystem. - Google Patents

Imprägnierungsverfahren und vorrichtung mit vakuumpumpenventilregelungssystem.

Info

Publication number
EP0280690A4
EP0280690A4 EP19870904368 EP87904368A EP0280690A4 EP 0280690 A4 EP0280690 A4 EP 0280690A4 EP 19870904368 EP19870904368 EP 19870904368 EP 87904368 A EP87904368 A EP 87904368A EP 0280690 A4 EP0280690 A4 EP 0280690A4
Authority
EP
European Patent Office
Prior art keywords
chamber
treatment
outlet
main treatment
main
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP19870904368
Other languages
English (en)
French (fr)
Other versions
EP0280690A1 (de
Inventor
Aaltje Elisabeth Maude
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of EP0280690A1 publication Critical patent/EP0280690A1/de
Publication of EP0280690A4 publication Critical patent/EP0280690A4/de
Withdrawn legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/08Impregnating by pressure, e.g. vacuum impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/0207Pretreatment of wood before impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/08Impregnating by pressure, e.g. vacuum impregnation
    • B27K3/10Apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2200/00Wooden materials to be treated
    • B27K2200/10Articles made of particles or fibres consisting of wood or other lignocellulosic material

Definitions

  • the present invention relates to a material impregnation system particularly useful in the treatment of cellulose, e.g. wood or wood composites. in this respect it is well known to impregnate wood with fire retardants and/or preservatives thereby improving the natural properties of the material.
  • cellulose e.g. wood or wood composites.
  • CCA copper chrome arsenic
  • CCA. is widely used as a preservative.
  • Water soluble phosphates and microbiocides are also known to impart corrosion and mould resistance.
  • apparatus for vacuum-pressure impregnating material comprising:
  • sensing means located in an upper portion of the main treatment chamber to sense when treatment chemical has filled the main treatment chamber to a predetermined level and provide an output signal
  • evacuation means responsive to the output signal to evacuate air remaining in the main treatment chamber whereafter the pump means urges treatment chemical into the main treatment chamber until the main treatment chamber is full and the upper chamber is filled to a predetermined level
  • pressure means to apply pressure to the main treatment chamber thereby impregnating the material with treatment chemical
  • the main treatment chamber is generally . -. spherical with hemispherical ends and the upper chamber is an open based cone or a frusto-cone. These chambers are sealingly connected about an opening in the main treatment chamber.
  • Characteristic of the invention is the speed which 0 the treatment chemical is introduced to and from the main treatment chamber. In one preferred form this is achieved by the withdrawal means including means to open an outlet in the main treatment chamber and air imput means to introduce air into the main treatment chamber to force treatment chemical through the outlet. 5
  • the most preferred form of air imput is a vacuum pump which may carry out the dual role of evacuation as well.
  • the difficulty presented with vacuum pumps is how to control their operation in a reliable yet simple manner.
  • control system comprises a 5 control system for a vacuum pump comprising: (a) a first chamber to be positively pressurized comprising an inlet and a first and second outlet; (b) a second chamber to be negatively pressurized comprising a first and second inlet and an outlet;
  • a first valve means associated with the first c b outlet of the first chamber and the first inlet of the second chamber, to close either the first outlet or first inlet and open the other;
  • a second valve means to open or close the
  • control means to operate the valve means to (i) (a) open the first outlet of the first chamber;
  • each chamber in either its positively or negatively pressurized condition notwithstanding that it is only being actuated to either evacuate or pressurize a remote chamber. Further, this means that the vacuum pump may be easily and readily change from either condition.
  • one of the chambers on top of the other and the valve arrangement located internally of the chambers.
  • the valve means may be butterfly valves or other means capable of opening or closing the inlet or outlet.
  • these valves may be controlled by the use of levers which may be interconnected by appropriate linkage. The linkage and valves will be actuated remotely in response to the desired state of the autoclave. Pistons connected to the levers has been found to be a particularly simple and effective method of actuating the valve means.
  • This arrangement also lends itself to compact manufacture thereby avoiding the bulky nature of conventional control systems.
  • the material to be impregnated is immersed in treatment chemical and it is desirable for most if not all of it to be covered. This enables the bulk of the treatment chemical to occupy most of the main treatment chamber and minimizes the time taken to achieve the subsequent evacuation and filling steps.
  • the autoclave is usually pressurized by use of a pump applied to the treatment chemical.
  • pressure impregnation is carried out at between 1200 and 1500 kpa, more preferably about 1380 kpa, for periods of two to three hours.
  • the removal of treatment chemical after impregnation can be accelerated by maintaining the pressure upon the autoclave and opening an outlet in the main treatment chamber.
  • the main treatment chamber is then again evacuated of air which withdraws excess treatment chemical from the material.
  • the main treatment chamber can be pressurized before and/or after this subsequent evacuation to remove remaining amounts of treatment chemical from the chamber.
  • control system is particularly suited to use in this method as it can be easily changed from the evacuation mode to the pressurized mode to remove t - the remainder of the treatment chemical from the main treatment chamber.
  • Figure 1 is a control system for a vacuum pump in an evacuation position.
  • Figure 2 is a control system for a vacuum pump in a pressurized position.
  • Figure 3 is a chemical dosing chart.
  • Figure 4 is a partial flow diagram of the impregnation system according to one aspect of the invention.
  • Figure 5 is a further partial flow diagram of the impregnation system used in Figure 4.
  • _ n Figure 6 is a partial flow diagram of the chemical supply used in Figure 4.
  • Figure 7 is a sequential illustration of the method according to the invention.
  • control system __ comprises a housing 10, including three chambers being silencer chamber 11, positive chamber 12 and negative chamber 13.
  • the positive chamber is provided with an inspection hatch which allows easy checking and maintenance of the valve system discussed below.
  • Pipe 14 extends externally of the housing 10 to a source of negative pressure - and extends through the silencer chamber 11 and positive chamber 12 into negative chamber 13.
  • Pipe 15 extends from outside housing 10 into the silencer chamber 11.
  • Pipe 16 is connected externally of
  • Pipe 17 is externally connected to a chamber (not shown) which is to be evacuated or alternately positively pressurized. It extends through the silencer chamber 11 into the positive chamber 12 and is sealingly connected to a valve 20.
  • Pipe 18 extends from the silencer chamber 11 into the positive chamber 12 and is sealingly connected to a valve 22 which valve 22 is also sealingly connected to valve 20.
  • Pipe 28 extends from negative chamber 13 into the positive chamber 12 and also connects with valve 20.
  • Pipe 19 extends between silencer chamber 11 and negative chamber 13. Interposed in pipe 19 is valve 21.
  • Valve 20, 21 and 22 are each provided with arms 24, 26 and 25 respectively.
  • Linkage 27 connects arms 24, 26 and 25. Arm 25 extends either side of valve 22 and is connected at one end to an accuation piston 23, that end being distant and on the opposite side of the valve 22 to the connection between linkage 27 and arm 25.
  • Positive chamber 12 has a drain pipe 31 which extends from the positive chamber 12 through negative chamber 13 and vents externally of housing 10.
  • Figure 1 depicts the flow of air from a evacuation chamber (not shown).
  • pipe 14 is connected externally of housing 10 to a source of negative pressure, it draws air from negative chamber 13.
  • the drop in pressure in negative chamber 13 causes suction upon pipes 28 and 27.
  • Valve 21 is closed preventing air to be drawn from the silencer chamber 11.
  • Valve 20 is open allowing air to be drawn from pipe 17 through valve 20 into pipe 28.
  • Valve 22 is in the closed position preventing air to be drawn through valve 22 either from the positive chamber 12 or pipe 18. Accordingly, air is drawn from the evacuation chamber (not shown) through pipe 17 via valve 20 into pipe 28.
  • Pipe 28 channels the air into negative chamber 13 and the air is subsequently removed from negative chamber 13 via pipe 14 to the source of negative pressure
  • the source of positive pressure + is not discontinued during the evacuation operation. Air is forced under pressure through pipe 16 and expelled into the positive chamber 12. Whilst valve 22 is closed to prevent air being sucked from the positive chamber 12 into valve 20, it nevertheless permits air from the positive chamber 12 to
  • valve 22 enter valve 22 and pass into pipe 18.
  • the air in pipe 18 is b expelled into the silencer chamber 11 and vented to the atmosphere via pipe 15.
  • valve 22 in pipe 19 is closed thus preventing air passing therethrough into the negative chamber 13.
  • Figure 2 depicts the control system effecting 0 pressurization to the evacuation chamber (not shown).
  • Pressurized air + enters pipe 16 and is discharged into positive chamber 12.
  • Valve 22 is open permitting air to flow into valve 20 which is also open to divert the air into pipe 17.
  • Valve 22 prevents air entering pipe 18.
  • Valve 20 5 prevents air entering pipe 28.
  • the pressurized air in pipe 17 expels into the evacuation chamber (not shown) .
  • valves 20, 21 and 22 are achieved by actuating piston 23 which moves the valves via 5 arms 24, 25 and 26 and linkage 27.
  • control system described herein enables the vacuum pump to be alternatively operated in a simple manner.
  • the system is very compact whilst still maintaining ease of c service and low capital outlay compared with conventional systems.
  • FIGs 4, 5 and 6 are partial flow diagrams which together illustrate the apparatus according to one aspect of the invention. 0 When utilizing this apparatus it is necessary to carry out an initial moisture content test upon the wood to be treated.
  • a dosing chart is reproduced from which the concentration of chemical may be selected. The chart plots percentage moisture against concentration of treatment chemical (litres per cubic meter of material) and type of wood. In this respect:
  • autoclave 32 comprises a treatment chamber 33 and an upper chamber 34.
  • Treatment chemical 35 is fed to treatment 33 from supply tanks A, B and C
  • Supply tank A is a work tank into which recycled used chemical 36 is passed after engaging a treatment filter 43.
  • Tank B is a bulk concentrated chemical supply whilst tank C is a bulk water supply.
  • the outlet of tanks A, B and C are set to ensure correct formulation.
  • the amount of concentrated chemical released into conduit 37 is closely controlled by sensor 55 located in conduit 37 which regulates control valve 38 in dependence up monitoring of treatment chemical formulation by sensor 55.
  • Swing check valves 40 and 41 are associated with tanks A and C respectively to prevent back flow of chemical.
  • conduit 37 Interposed in conduit 37 is a pneumatic valve 42 which can selectively close the conduit. Similarly check valves 44 and 45 are located in conduits 46 and 37 to allow recycling of used chemical 36. Sensor 47 senses the presence of treatment chemical.
  • upper chamber 34 is sealingly attached to treatment chamber 33.
  • a level sensor 50 is situated in treatment chamber 33 at a level above the upper level of the material to be treated (not shown) .
  • conduits 48 and 47 Connected to upper chamber 34 are conduits 48 and 47.
  • Conduit 48 can selectively pressurize upper chamber 34 and treatment chamber 33. This pressurization is achieved by the use of vacuum pump apparatus 51.
  • Conduit 49 can selectively evacuate upper chamber 34 and treatment chamber 33 again using vacuum pump apparatus 51. As noise is generated in generating the vacuum or pressure silencers and filters 52 are utilized.
  • a pressure relief valve 53 is incorporated between conduit 48 and the vacuum pump 51 for safety reasons.
  • Pressure pump 54 is located in conduit 37 and is operable to pressurize the treatment chemical 35 flowing into treatment chamber 33 and pressurize the autoclave 32.
  • the autoclave 32 is initially in the empty condition AA. Wood 55 is tested for moisture and an appropriate amount of concentrated chemical is selected. Wood 55 is then placed into the treatment chamber 33 and sealed therein (condition BB). Sensor 55 regulates control valve 38 to allow and maintain the predetermined amount of concentrated chemical to enter conduit 37 in combination with amounts from tanks A and C Treatment chemical 35 is pumped into treatment chamber 33 and prevented from flowing into conduit 46 by check valve 44.
  • the treatment chemical 35 fills treatment chamber 33 until level sensor 50 senses it at which time valve 42 is closed (condition CC).
  • Conduit 48 is closed and conduit 49 evacuates the air from the autoclave (condition DD).
  • Valve 42 is reopened which floods the autoclave up ' to the level of conduit 48 (condition EE).
  • c Pressure pump 54 is operated to pressurize the autoclave 32 for a predetermined period (condition FF.) Pump 54 ceases operation, valve 45 closes conduit 37 and used treatment chemical 36 is blown from the treatment chamber (condition GG) into conduit 46 for treatment in 0 filter 43 and recirculation to tank A.
  • Conduit 48 is closed and conduit 49 opened to apply a vacuum and withdraw excess treatment chemical from the face of the material which accumulates in the lower portion of the main treatment chamber 33 (condition HH).
  • Conduit 49 is closed and conduit 48 opened to apply air into and pressurize upper chamber 34 and treatment chamber 33 (condition HH) .
  • Valve 42 is open to permit residual used treatment chemical 36 to be blown from the treatment chamber 33 (condition II) .
  • the system and apparatus of the invention permit operation of the impregnation plant at close to ideal conditions.
  • the modified autoclave gives an effective evacuation of the main chamber allowing an improved impregnation of the material. Accordingly the invention achieves greater impregnation with short treatment times than previously known. Treatment costs are therefore reduced.
  • the system also monitors the strength of the treating solution to an accuracy of + or - 0.1%. This far exceeds current specific gravity meters, thus enabling more accurate retention of treatment chemical at a large saving in cost, as the chemical solution is sampled condtinuously and automatically. As it enters the autoclave, flow control valves vary the solution strength to maintain this accuracy, thus eliminating hand mixing and adjusting AFTER the chemical has entered the autoclave.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)
EP19870904368 1986-07-01 1987-07-01 Imprägnierungsverfahren und vorrichtung mit vakuumpumpenventilregelungssystem. Withdrawn EP0280690A4 (de)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
AU6673/86 1986-07-01
AUPH667386 1986-07-01
AUPI161587 1987-04-28
AU1615/87 1987-04-28

Publications (2)

Publication Number Publication Date
EP0280690A1 EP0280690A1 (de) 1988-09-07
EP0280690A4 true EP0280690A4 (de) 1989-03-09

Family

ID=25643116

Family Applications (1)

Application Number Title Priority Date Filing Date
EP19870904368 Withdrawn EP0280690A4 (de) 1986-07-01 1987-07-01 Imprägnierungsverfahren und vorrichtung mit vakuumpumpenventilregelungssystem.

Country Status (3)

Country Link
EP (1) EP0280690A4 (de)
JP (1) JPH01500503A (de)
WO (1) WO1988000114A1 (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6576174B1 (en) * 2000-01-27 2003-06-10 Industrial Thermo Polymers Limited Residual gas extraction process
US6696102B2 (en) * 2001-01-19 2004-02-24 Premier Wood Treating, L.L.C. Cellulose preservative method and apparatus
US6586109B2 (en) 2001-09-21 2003-07-01 Premier Wood Treating, Llc Fire retardant cellulose preservative treatment process
GB0906146D0 (en) 2009-04-09 2009-05-20 Kebony Asa Apparatus and operating systems for manufacturing impregnated wood
GB0906989D0 (en) 2009-04-23 2009-06-03 Kebony Asa Decking

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2432008A (en) * 1942-02-07 1947-12-02 Bolidens Gruv Ab Process and device for full-cell treatment of timber and similar material
GB1424809A (en) * 1972-10-17 1976-02-11 Richardson Starling Ltd Double vacuum treatment of timber and other porous materials
US3968276A (en) * 1972-10-25 1976-07-06 Diversified Wood Products, Inc. Process for the preservation of wood
US4581243A (en) * 1984-11-19 1986-04-08 Permawood Treating Co. Wood treating method and apparatus

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1399833A (en) * 1971-04-19 1975-07-02 Protim & Gallwey Ltd Treatment of timber
GB1405754A (en) * 1971-08-23 1975-09-10 Protim Ltd Treatment of timber
NO781826L (no) * 1977-05-31 1978-12-01 Forest Prod Util Lab Fremgangsmaate til trykkimpregnering av tre
NZ211005A (en) * 1984-02-02 1988-03-30 Terje Rosenlund Impregnating wood

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2432008A (en) * 1942-02-07 1947-12-02 Bolidens Gruv Ab Process and device for full-cell treatment of timber and similar material
GB1424809A (en) * 1972-10-17 1976-02-11 Richardson Starling Ltd Double vacuum treatment of timber and other porous materials
US3968276A (en) * 1972-10-25 1976-07-06 Diversified Wood Products, Inc. Process for the preservation of wood
US4581243A (en) * 1984-11-19 1986-04-08 Permawood Treating Co. Wood treating method and apparatus

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of WO8800114A1 *

Also Published As

Publication number Publication date
EP0280690A1 (de) 1988-09-07
WO1988000114A1 (en) 1988-01-14
JPH01500503A (ja) 1989-02-23

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