EP0045201A1 - A method of rendering material aseptic - Google Patents
A method of rendering material aseptic Download PDFInfo
- Publication number
- EP0045201A1 EP0045201A1 EP81303417A EP81303417A EP0045201A1 EP 0045201 A1 EP0045201 A1 EP 0045201A1 EP 81303417 A EP81303417 A EP 81303417A EP 81303417 A EP81303417 A EP 81303417A EP 0045201 A1 EP0045201 A1 EP 0045201A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- substance
- radiation
- aseptic
- layer
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims abstract description 15
- 238000009877 rendering Methods 0.000 title claims abstract description 9
- 239000000463 material Substances 0.000 title claims description 27
- 230000005855 radiation Effects 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 230000001954 sterilising effect Effects 0.000 claims abstract description 5
- 230000002195 synergetic effect Effects 0.000 claims abstract description 4
- 239000000126 substance Substances 0.000 claims description 20
- 231100000331 toxic Toxicity 0.000 claims description 4
- 230000002588 toxic effect Effects 0.000 claims description 4
- 239000004698 Polyethylene Substances 0.000 abstract description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052782 aluminium Inorganic materials 0.000 abstract description 3
- 239000004411 aluminium Substances 0.000 abstract description 3
- 239000011087 paperboard Substances 0.000 abstract description 3
- -1 polyethylene Polymers 0.000 abstract description 3
- 229920000573 polyethylene Polymers 0.000 abstract description 3
- 238000004806 packaging method and process Methods 0.000 abstract description 2
- 230000001678 irradiating effect Effects 0.000 abstract 1
- 238000005507 spraying Methods 0.000 abstract 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 8
- 230000000844 anti-bacterial effect Effects 0.000 description 6
- 239000003899 bactericide agent Substances 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 210000004666 bacterial spore Anatomy 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 230000001665 lethal effect Effects 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 238000012371 Aseptic Filling Methods 0.000 description 1
- 244000063299 Bacillus subtilis Species 0.000 description 1
- 235000014469 Bacillus subtilis Nutrition 0.000 description 1
- 241000282414 Homo sapiens Species 0.000 description 1
- 238000009455 aseptic packaging Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000002301 combined effect Effects 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- QOSATHPSBFQAML-UHFFFAOYSA-N hydrogen peroxide;hydrate Chemical compound O.OO QOSATHPSBFQAML-UHFFFAOYSA-N 0.000 description 1
- 238000011081 inoculation Methods 0.000 description 1
- 239000002054 inoculum Substances 0.000 description 1
- 231100000518 lethal Toxicity 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920006327 polystyrene foam Polymers 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000009291 secondary effect Effects 0.000 description 1
- 210000004215 spore Anatomy 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/02—Sterilising, e.g. of complete packages
- B65B55/04—Sterilising wrappers or receptacles prior to, or during, packaging
Definitions
- This invention relates to a method of rendering material aseptic.
- United States Patent 3,566,575 discloses an aseptic packaging machine for forming, aseptically treating, filling and sealing containers while protecting them with a clear air atmosphere after they have been aseptically treated by a bactericide.
- the aseptic treatment is accomplished by a fogging system to provide for total contact by the bactericide with the internal sufaces of the container and includes a drying station for removal of the residual bactericide after the treatment.
- the suggested bactericide is 35% hydrogen peroxide solution (H 2 0 2 ).
- H 2 0 2 35% hydrogen peroxide solution
- the H 2 0 2 is removed by drying, which is done by jetting hot air down through the open top of the container. Complete removal is desirable since it has been alleged that, even in small residual quantities, H 2 0 2 has a toxic effect on human beings.
- the relatively large amount of H 2 0 2 required is very difficult to dry away completely, especially since the drying is least effective at the bottom of the container, so that again a relatively long time is required. The total time delays involved therefore seriously jeopardize the commercial of the machine.
- the radiation source is directed with Its window inside the carton to cover all internal surfaces.
- the carton is designed so as to avoid any shadows on its inside.
- the radiation source is a gas discharge lamp with a power unit and emits ultraviolet rays cf 200-280 nm (esp. 254 nm) when a lifter has raised a carton around the quartz tube of the lamp.
- Addition UV lamps can be arranged in the chamber. If an electron beam is used instead of the UV lamps, lead screens are required to protect the personnel against X-rays, produced as a secondary effect.
- a preferred material for the cartons is polystyrene foam, strengthened by a surface coating of a homogeneous plastic.
- a method of rendering material aseptic in which the material is contacted with a substance, and the material and the substance are irradiated with ultraviolet radiation, the substance and the radiation having a synergistic sterilizing effect, characterized in that said substance is not toxic in residual quantities,
- Such substance can be water, for example.
- a method of rendering material aseptic in which the material is provided with a layer of a substance and the material and the substance are irradiated with ultravioler. radiation the substance and the radiation having a synergistie.sterilizing effect, characyterized in that said layer is relatively thin and the irradiation is relatively intensive.
- the substance can be hydrogen peroxide solution or water, for example.
- the layer consists of droplets of H 2 0 2 or water.
- the layer is less than 0.1 mm thick, for example about 2u thick. we believe that such a relatively thin layer has the advantage that the droplets do not shelter to a substantial extent from the ultraviolet radiation the organisms to be killed.
- the dosage of the irradiation is advantageously at least 5 mW sec./cm 2 over every part of the material desired to be rendered aseptic, so giving a relatively high dosage.
- a method of rendering material aseptic in which the material is irradiated with ultraviolet radiation, characterized in that substantially no radiation the wavelength of which has been substantially changed by the material is reflected by the material.
- Ultraviolet radiation was provided by a hign intensity W-C germicidal lamp (UVC-13-70) produced by Brown, Boveri & Cie of Baden.
- the lamp was so situated relative to the carton that the lowest dosage of any part of the interior surface of the carton was 5 mW-sec./cm 2 with a 10 second exposure of the interior surface.
- H z 0 2 solution was used into the cartons at ambient temperature.
- 0.1 ml of H 2 O 2 in 1% w/v solution was sprayed for 0.6 sec., to give an H 2 0 2 layer thickness of about 2 ⁇ .
- Water was also sprayed into the cartons in a similar manner.
- the present invention is particularly usable in the machine of our Patent Application No. 7 9302970.3
- H 2 0 2 The desired lethal effect'on bacteria of the combined use of H 2 0 2 and UV has been found to be consistently achieved even at very low H 2 0 2 concentrations e.g. down to 0.05% H 2 0 2 solution.
- residual H 2 0 2 can in any case be made very low, without any serious detriment to the bactericidal effect.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB8024780 | 1980-07-29 | ||
GB8024780 | 1980-07-29 |
Publications (1)
Publication Number | Publication Date |
---|---|
EP0045201A1 true EP0045201A1 (en) | 1982-02-03 |
Family
ID=10515115
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP81303417A Withdrawn EP0045201A1 (en) | 1980-07-29 | 1981-07-24 | A method of rendering material aseptic |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP0045201A1 (enrdf_load_stackoverflow) |
JP (1) | JPS57110252A (enrdf_load_stackoverflow) |
AU (1) | AU7352581A (enrdf_load_stackoverflow) |
DK (1) | DK338481A (enrdf_load_stackoverflow) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001091809A3 (en) * | 2000-05-29 | 2002-04-04 | Fine Hygienic Paper Fze | Sterilization process for hygienic products |
WO2003015834A1 (fr) * | 2001-08-20 | 2003-02-27 | Menicon Co., Ltd. | Procede de desinfection |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH07112489B2 (ja) * | 1989-06-26 | 1995-12-06 | エフ エム シー コーポレーション | 過酸化水素、過酸及びu.v.照射による容器の殺菌法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3566575A (en) * | 1968-02-26 | 1971-03-02 | Ex Cell O Corp | Aseptic packaging machine |
CH578457A5 (enrdf_load_stackoverflow) * | 1974-11-08 | 1976-08-13 | Bbc Brown Boveri & Cie | |
CH595248A5 (en) * | 1974-12-10 | 1978-02-15 | Anders Ruben Rausing | Sterilised cartons for long-life liquids |
US4175140A (en) * | 1974-04-10 | 1979-11-20 | Aluminiumwerke Ag. Rorschach | Method for automatic low-bacteria to aseptic filling and packing of foodstuffs employing ultraviolet radiation |
WO1980001457A1 (en) * | 1979-01-11 | 1980-07-24 | J Peel | Method of sterilisation |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2735550A1 (de) * | 1977-08-06 | 1979-02-08 | Guenther O Prof Dr Schenck | Mehrkammer-photoreaktor |
JPS5491437A (en) * | 1977-12-22 | 1979-07-19 | Matsushita Electric Ind Co Ltd | Pasteurizing method for culture solution in solution cultivation |
-
1981
- 1981-07-24 EP EP81303417A patent/EP0045201A1/en not_active Withdrawn
- 1981-07-29 AU AU73525/81A patent/AU7352581A/en not_active Abandoned
- 1981-07-29 JP JP56117886A patent/JPS57110252A/ja active Granted
- 1981-07-29 DK DK338481A patent/DK338481A/da not_active Application Discontinuation
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3566575A (en) * | 1968-02-26 | 1971-03-02 | Ex Cell O Corp | Aseptic packaging machine |
US4175140A (en) * | 1974-04-10 | 1979-11-20 | Aluminiumwerke Ag. Rorschach | Method for automatic low-bacteria to aseptic filling and packing of foodstuffs employing ultraviolet radiation |
CH578457A5 (enrdf_load_stackoverflow) * | 1974-11-08 | 1976-08-13 | Bbc Brown Boveri & Cie | |
CH595248A5 (en) * | 1974-12-10 | 1978-02-15 | Anders Ruben Rausing | Sterilised cartons for long-life liquids |
WO1980001457A1 (en) * | 1979-01-11 | 1980-07-24 | J Peel | Method of sterilisation |
Non-Patent Citations (1)
Title |
---|
THE JOURNAL OF APPLIED BACTERIOLOGY, vol. 47, no. 2, October 1979, London, New York, San Francisco C.E. BAYLISS AND W.M. WAITES " The Combined Effect of Hydrogen Peroxide and Ultraviolet Irradiation on Bacterial Spores " pages 263-269 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001091809A3 (en) * | 2000-05-29 | 2002-04-04 | Fine Hygienic Paper Fze | Sterilization process for hygienic products |
WO2003015834A1 (fr) * | 2001-08-20 | 2003-02-27 | Menicon Co., Ltd. | Procede de desinfection |
Also Published As
Publication number | Publication date |
---|---|
JPS644468B2 (enrdf_load_stackoverflow) | 1989-01-25 |
JPS57110252A (en) | 1982-07-09 |
AU7352581A (en) | 1982-06-10 |
DK338481A (da) | 1982-01-30 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
AK | Designated contracting states |
Designated state(s): AT BE CH DE FR GB IT LI NL SE |
|
17P | Request for examination filed |
Effective date: 19820723 |
|
RAP1 | Party data changed (applicant data changed or rights of an application transferred) |
Owner name: LIQUIPAK INTERNATIONAL B.V. |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN |
|
18D | Application deemed to be withdrawn |
Effective date: 19840406 |
|
RIN1 | Information on inventor provided before grant (corrected) |
Inventor name: STANNARD, CATHERINE JANE Inventor name: WOOD, JOHN MATHEW |