EA201100489A1 - Способ получения спирта - Google Patents
Способ получения спиртаInfo
- Publication number
- EA201100489A1 EA201100489A1 EA201100489A EA201100489A EA201100489A1 EA 201100489 A1 EA201100489 A1 EA 201100489A1 EA 201100489 A EA201100489 A EA 201100489A EA 201100489 A EA201100489 A EA 201100489A EA 201100489 A1 EA201100489 A1 EA 201100489A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- extraction solvent
- solution
- aqueous
- water
- solvent
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
- Saccharide Compounds (AREA)
Abstract
Изобретение относится к способу получения спирта из целлюлозного материала, включающему стадии: (1) осуществления гидролиза указанного целлюлозного материала водной кислотой с получением гидролизата; (2) экстрагирование кислоты и воды из указанного гидролизата с помощью смешиваемого с водой органического экстракционного растворителя с получением (а) первого водного кислого раствора, содержащего указанный экстракционный растворитель, и (б) остатка, содержащего сахара; (3) проведение с указанным остатком реакции расщепления олигосахаридов с получением водного раствора способных к брожению сахаров; (4) осуществление брожения указанных способных к брожению сахаров и отгонку спирта из полученной сброженной смеси; (5) выпаривание указанного экстракционного растворителя из указанного раствора с получением (а) второго водного кислого раствора, содержащего не более 10 мас.%, предпочтительно не более 5 мас.% указанного экстракционного растворителя, и (б) газообразного экстракционного растворителя; (6) осуществление конденсации указанного газообразного экстракционного растворителя для подачи его рециклом, и, при необходимости, (7) концентрирование указанного второго водного кислого раствора для подачи его рециклом, где указанный экстракционный растворитель находится в жидком состоянии при температуре и давлении стадии (2), имеет температуру кипения от 25 до 60°С при давлении от 100 кПа до 800 кПа (от 1 до 8 бар) и является таким, что растворимые в воде олигосахариды осаждаются из раствора путем добавления этого растворителя на стадии (2).
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GBGB0819406.0A GB0819406D0 (en) | 2008-10-22 | 2008-10-22 | Process |
PCT/GB2009/002349 WO2010046619A1 (en) | 2008-10-22 | 2009-10-02 | Process for the production of alcohol |
Publications (2)
Publication Number | Publication Date |
---|---|
EA201100489A1 true EA201100489A1 (ru) | 2011-12-30 |
EA020072B1 EA020072B1 (ru) | 2014-08-29 |
Family
ID=40097873
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EA201100489A EA020072B1 (ru) | 2008-10-22 | 2009-10-02 | Способ получения спирта |
Country Status (11)
Country | Link |
---|---|
US (1) | US8709769B2 (ru) |
EP (1) | EP2356261A1 (ru) |
JP (1) | JP2012506250A (ru) |
CN (1) | CN102203297A (ru) |
AU (1) | AU2009306177A1 (ru) |
BR (1) | BRPI0919856A2 (ru) |
CA (1) | CA2749100C (ru) |
EA (1) | EA020072B1 (ru) |
GB (1) | GB0819406D0 (ru) |
WO (1) | WO2010046619A1 (ru) |
ZA (1) | ZA201102728B (ru) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB0907879D0 (en) * | 2009-05-07 | 2009-06-24 | Weyland As | Process |
ES2862178T3 (es) | 2010-06-26 | 2021-10-07 | Virdia Llc | Métodos de producción de mezclas de azúcares |
IL206678A0 (en) | 2010-06-28 | 2010-12-30 | Hcl Cleantech Ltd | A method for the production of fermentable sugars |
IL207329A0 (en) | 2010-08-01 | 2010-12-30 | Robert Jansen | A method for refining a recycle extractant and for processing a lignocellulosic material and for the production of a carbohydrate composition |
IL207945A0 (en) | 2010-09-02 | 2010-12-30 | Robert Jansen | Method for the production of carbohydrates |
WO2012137201A1 (en) | 2011-04-07 | 2012-10-11 | Hcl Cleantech Ltd. | Lignocellulose conversion processes and products |
US9617608B2 (en) | 2011-10-10 | 2017-04-11 | Virdia, Inc. | Sugar compositions |
AU2013256049B2 (en) | 2012-05-03 | 2017-02-16 | Virdia, Inc. | Methods for treating lignocellulosic materials |
US9493851B2 (en) | 2012-05-03 | 2016-11-15 | Virdia, Inc. | Methods for treating lignocellulosic materials |
US9630894B2 (en) | 2012-09-05 | 2017-04-25 | Dynasep Inc. | Energy efficient method and apparatus for the extraction of biomolecules from dilute aqueous solution |
US9029615B2 (en) | 2012-09-05 | 2015-05-12 | Dynasep Inc. | Energy efficient method and apparatus for the extraction of lower alcohols from dilute aqueous solution |
US9297111B1 (en) | 2013-03-15 | 2016-03-29 | Domtar Paper Company, Llc | Methods for the manufacture of cellulose nanocrystals |
US9850512B2 (en) | 2013-03-15 | 2017-12-26 | The Research Foundation For The State University Of New York | Hydrolysis of cellulosic fines in primary clarified sludge of paper mills and the addition of a surfactant to increase the yield |
US10711319B2 (en) * | 2013-12-24 | 2020-07-14 | Silvanova, Llc | Method for treating cellulosic material |
US9790523B2 (en) | 2014-03-04 | 2017-10-17 | White Dog Labs, Inc. | Energy efficient batch recycle method for the production of biomolecules |
US9951363B2 (en) | 2014-03-14 | 2018-04-24 | The Research Foundation for the State University of New York College of Environmental Science and Forestry | Enzymatic hydrolysis of old corrugated cardboard (OCC) fines from recycled linerboard mill waste rejects |
CN112226466A (zh) | 2015-01-07 | 2021-01-15 | 威尔迪亚公司 | 萃取和转化半纤维素糖的方法 |
CA2985478A1 (en) | 2015-05-27 | 2016-12-01 | Virdia, Inc. | Integrated methods for treating lignocellulosic material |
US10781196B2 (en) | 2016-08-17 | 2020-09-22 | University Of Delaware | Integrated process for direct saccharification and dehydration of intact biomass to furfurals |
Family Cites Families (31)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB376323A (en) * | 1931-03-07 | 1932-07-07 | Henry Dreyfus | Improvements in or relating to the manufacture of dextrins, sugars and other products from cellulosic materials |
GB602833A (en) * | 1944-11-10 | 1948-06-03 | Melle Usines Sa | Improvements in or relating to saccharification of cellulosic materials |
US3212933A (en) | 1963-04-12 | 1965-10-19 | Georgia Pacific Corp | Hydrolysis of lignocellulose materials with solvent extraction of the hydrolysate |
US3398129A (en) | 1963-08-30 | 1968-08-20 | Rexall Drug Chemical | Process for preparing predominantly crystalline alpha-olefin polymers |
US4057486A (en) | 1975-07-14 | 1977-11-08 | Canadian Patents And Development Limited | Separating organic material from tar sands or oil shale |
US4237110A (en) | 1979-04-30 | 1980-12-02 | The Dow Chemical Company | Process for separating and recovering concentrated hydrochloric acid from the crude product obtained from the acid hydrolysis of cellulose |
JPS5653104A (en) | 1979-10-09 | 1981-05-12 | Mitsui Petrochem Ind Ltd | Separation of polymer from polymer solution |
CA1225636A (en) | 1984-07-13 | 1987-08-18 | Robert P. Chang | Method for continuous countercurrent organosolv saccharification of wood and other lignocellulosic materials |
US4645658A (en) | 1985-04-30 | 1987-02-24 | Gaddy James L | Method of recovering hydrochloric acid from a product comprised of sugars and concentrated hydrochloric acid |
US4608245A (en) | 1985-10-17 | 1986-08-26 | Gaddy James L | Method of separation of sugars and concentrated sulfuric acid |
EP0354243B1 (en) | 1987-07-24 | 1994-07-20 | JAPAN as represented by MINISTER OF INTERNATIONAL TRADE AND INDUSTRY | Process for concentrating and purifying alchohol |
DE69128059T2 (de) | 1990-08-17 | 1998-02-26 | Alcell Tech Inc | Verfahren zum Lösungsmittel-Stetigaufschluss |
US5314579A (en) | 1992-01-13 | 1994-05-24 | Quantum Chemical Corporation | Process for removing hydrocarbons from polymer slurries |
US5370999A (en) | 1992-12-17 | 1994-12-06 | Colorado State University Research Foundation | Treatment of fibrous lignocellulosic biomass by high shear forces in a turbulent couette flow to make the biomass more susceptible to hydrolysis |
US5723433A (en) | 1993-09-24 | 1998-03-03 | The Chemithon Corporation | Sovent removal process |
US5735916A (en) | 1995-07-13 | 1998-04-07 | Lucas; James Lewis | Process for production of lignin fuel, ethyl alcohol, cellulose, silica/silicates, and cellulose derivatives from plant biomass |
IL121207A (en) | 1997-06-30 | 2000-10-31 | Staley Mfg Co A E | Liquid-liquid extraction for the recovery of lactic acid with an amine solution in the presence of carbon dioxide |
US5868851A (en) | 1997-08-11 | 1999-02-09 | Lightner; Gene E. | Process for production of solid glucose |
WO1999067409A1 (en) | 1998-06-23 | 1999-12-29 | The Regents Of The University Of California | Method of treating biomass material |
US6007636A (en) | 1999-01-04 | 1999-12-28 | Lightner; Gene E. | Method to recycle an aqueous acidic liquor used for depolymerization of cellulose |
WO2001003805A1 (en) | 1999-07-14 | 2001-01-18 | Taylor Tommy G | Innovative incineration system for refuse-derived fuels, coal and petroleum coke, or chlorinated hydrocarbons |
US20020021994A1 (en) | 1999-10-08 | 2002-02-21 | Blue Jerry D. | Sulfur recovery gasification process for spent liquor at high temperature and high pressure |
NO312070B1 (no) | 2000-07-04 | 2002-03-11 | Karl Weydahl | Fremgangsmåte ved en prosess for fremstilling av gj¶rbart sukker fra celluloseholdige råstoffer |
US6423145B1 (en) | 2000-08-09 | 2002-07-23 | Midwest Research Institute | Dilute acid/metal salt hydrolysis of lignocellulosics |
US6441202B1 (en) | 2001-08-20 | 2002-08-27 | Gene E. Lightner | Heterocyclic compounds extracted by a hydrocarbon |
WO2007019505A2 (en) | 2005-08-05 | 2007-02-15 | The Trustees Of Dartmouth College | Method and apparatus for saccharide precipitation from pretreated lignocellulosic materials |
BRPI0505212A (pt) | 2005-11-01 | 2007-08-07 | Dedini Sa Ind De Base | aperfeiçoamentos em processo de hidrólise ácida rápida de material lignocelulósico e em reator de hidrólise |
JP5209597B2 (ja) * | 2006-03-29 | 2013-06-12 | バージニア テック インテレクチュアル プロパティーズ インク | 穏やかな反応条件でのセルロース溶媒に基づくリグノセルロースの分別および試薬の再循環 |
AU2008224486B2 (en) | 2007-03-15 | 2011-10-20 | Hcl Cleantech Ltd. | A process for the recovery of HCl from a dilute solution thereof |
CN101157445A (zh) | 2007-09-18 | 2008-04-09 | 陈培豪 | 植物纤维素原料浓酸水解液中硫酸的回收方法 |
GB0818093D0 (en) | 2008-10-02 | 2008-11-05 | Weyland As | Method |
-
2008
- 2008-10-22 GB GBGB0819406.0A patent/GB0819406D0/en not_active Ceased
-
2009
- 2009-10-02 WO PCT/GB2009/002349 patent/WO2010046619A1/en active Application Filing
- 2009-10-02 EP EP09785188A patent/EP2356261A1/en not_active Withdrawn
- 2009-10-02 AU AU2009306177A patent/AU2009306177A1/en not_active Abandoned
- 2009-10-02 CN CN2009801418642A patent/CN102203297A/zh active Pending
- 2009-10-02 US US13/125,069 patent/US8709769B2/en active Active - Reinstated
- 2009-10-02 BR BRPI0919856A patent/BRPI0919856A2/pt not_active Application Discontinuation
- 2009-10-02 EA EA201100489A patent/EA020072B1/ru not_active IP Right Cessation
- 2009-10-02 CA CA2749100A patent/CA2749100C/en active Active
- 2009-10-02 JP JP2011532703A patent/JP2012506250A/ja active Pending
-
2011
- 2011-04-12 ZA ZA2011/02728A patent/ZA201102728B/en unknown
Also Published As
Publication number | Publication date |
---|---|
GB0819406D0 (en) | 2008-11-26 |
CA2749100C (en) | 2018-02-27 |
ZA201102728B (en) | 2012-07-25 |
EA020072B1 (ru) | 2014-08-29 |
US8709769B2 (en) | 2014-04-29 |
BRPI0919856A2 (pt) | 2019-06-04 |
CN102203297A (zh) | 2011-09-28 |
AU2009306177A1 (en) | 2010-04-29 |
JP2012506250A (ja) | 2012-03-15 |
US20110294181A1 (en) | 2011-12-01 |
CA2749100A1 (en) | 2010-04-29 |
WO2010046619A1 (en) | 2010-04-29 |
EP2356261A1 (en) | 2011-08-17 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): AM AZ BY KZ KG MD TJ TM RU |