EA025290B1 - Способ приготовления съедобных эмульсий на основе непрерывной жировой фазы - Google Patents
Способ приготовления съедобных эмульсий на основе непрерывной жировой фазы Download PDFInfo
- Publication number
- EA025290B1 EA025290B1 EA201401260A EA201401260A EA025290B1 EA 025290 B1 EA025290 B1 EA 025290B1 EA 201401260 A EA201401260 A EA 201401260A EA 201401260 A EA201401260 A EA 201401260A EA 025290 B1 EA025290 B1 EA 025290B1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- fat
- unfractionated
- refractory
- oil
- profile
- Prior art date
Links
- 239000000839 emulsion Substances 0.000 title claims abstract description 124
- 238000000034 method Methods 0.000 title claims abstract description 97
- 230000008569 process Effects 0.000 title abstract description 10
- 238000002360 preparation method Methods 0.000 title description 6
- 239000007788 liquid Substances 0.000 claims abstract description 89
- 239000007787 solid Substances 0.000 claims abstract description 53
- 238000002156 mixing Methods 0.000 claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 claims abstract description 17
- 239000007762 w/o emulsion Substances 0.000 claims abstract description 13
- 239000000155 melt Substances 0.000 claims abstract description 4
- 235000019197 fats Nutrition 0.000 claims description 351
- 239000003921 oil Substances 0.000 claims description 71
- 235000019198 oils Nutrition 0.000 claims description 58
- 239000008346 aqueous phase Substances 0.000 claims description 43
- 239000000203 mixture Substances 0.000 claims description 42
- 239000012071 phase Substances 0.000 claims description 28
- 239000013078 crystal Substances 0.000 claims description 14
- 238000005259 measurement Methods 0.000 claims description 9
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims description 8
- 102000003712 Complement factor B Human genes 0.000 claims description 7
- 108090000056 Complement factor B Proteins 0.000 claims description 7
- 239000003346 palm kernel oil Substances 0.000 claims description 7
- 235000019865 palm kernel oil Nutrition 0.000 claims description 7
- 239000003240 coconut oil Substances 0.000 claims description 6
- 235000019864 coconut oil Nutrition 0.000 claims description 6
- 239000011229 interlayer Substances 0.000 claims description 6
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims description 5
- 235000019869 fractionated palm oil Nutrition 0.000 claims description 5
- 239000011630 iodine Substances 0.000 claims description 5
- 229910052740 iodine Inorganic materials 0.000 claims description 5
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- 238000002844 melting Methods 0.000 claims description 4
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- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims 2
- 239000000843 powder Substances 0.000 abstract description 8
- 239000002002 slurry Substances 0.000 abstract 2
- 239000003925 fat Substances 0.000 description 298
- 239000000047 product Substances 0.000 description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 22
- 235000013310 margarine Nutrition 0.000 description 14
- 239000003264 margarine Substances 0.000 description 14
- 239000003995 emulsifying agent Substances 0.000 description 13
- -1 for example Substances 0.000 description 10
- 230000008859 change Effects 0.000 description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
- 239000000523 sample Substances 0.000 description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
- 239000004615 ingredient Substances 0.000 description 8
- 238000009826 distribution Methods 0.000 description 7
- 150000003626 triacylglycerols Chemical class 0.000 description 6
- 235000015112 vegetable and seed oil Nutrition 0.000 description 6
- 239000008158 vegetable oil Substances 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 235000005687 corn oil Nutrition 0.000 description 5
- 235000014113 dietary fatty acids Nutrition 0.000 description 5
- 229930195729 fatty acid Natural products 0.000 description 5
- 239000000194 fatty acid Substances 0.000 description 5
- 239000010410 layer Substances 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 235000019484 Rapeseed oil Nutrition 0.000 description 4
- 235000019486 Sunflower oil Nutrition 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 235000004213 low-fat Nutrition 0.000 description 4
- 239000011780 sodium chloride Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000002600 sunflower oil Substances 0.000 description 4
- 235000013311 vegetables Nutrition 0.000 description 4
- 241001474374 Blennius Species 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
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- 235000018102 proteins Nutrition 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 238000000235 small-angle X-ray scattering Methods 0.000 description 3
- 235000012424 soybean oil Nutrition 0.000 description 3
- 239000003549 soybean oil Substances 0.000 description 3
- 235000014698 Brassica juncea var multisecta Nutrition 0.000 description 2
- 235000006008 Brassica napus var napus Nutrition 0.000 description 2
- 235000006618 Brassica rapa subsp oleifera Nutrition 0.000 description 2
- 244000188595 Brassica sinapistrum Species 0.000 description 2
- 235000004977 Brassica sinapistrum Nutrition 0.000 description 2
- DPUOLQHDNGRHBS-UHFFFAOYSA-N Brassidinsaeure Natural products CCCCCCCCC=CCCCCCCCCCCCC(O)=O DPUOLQHDNGRHBS-UHFFFAOYSA-N 0.000 description 2
- 239000004278 EU approved seasoning Substances 0.000 description 2
- URXZXNYJPAJJOQ-UHFFFAOYSA-N Erucic acid Natural products CCCCCCC=CCCCCCCCCCCCC(O)=O URXZXNYJPAJJOQ-UHFFFAOYSA-N 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- 235000019482 Palm oil Nutrition 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 239000003637 basic solution Substances 0.000 description 2
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- DPUOLQHDNGRHBS-KTKRTIGZSA-N erucic acid Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(O)=O DPUOLQHDNGRHBS-KTKRTIGZSA-N 0.000 description 2
- 235000013861 fat-free Nutrition 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 235000011194 food seasoning agent Nutrition 0.000 description 2
- 235000019866 hydrogenated palm kernel oil Nutrition 0.000 description 2
- 239000000944 linseed oil Substances 0.000 description 2
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- 239000002960 lipid emulsion Substances 0.000 description 2
- 235000021243 milk fat Nutrition 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 235000014593 oils and fats Nutrition 0.000 description 2
- 239000004006 olive oil Substances 0.000 description 2
- 235000008390 olive oil Nutrition 0.000 description 2
- 239000002540 palm oil Substances 0.000 description 2
- 230000004044 response Effects 0.000 description 2
- 235000014102 seafood Nutrition 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 230000005469 synchrotron radiation Effects 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 1
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 241000273930 Brevoortia tyrannus Species 0.000 description 1
- 241000195493 Cryptophyta Species 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 102000014171 Milk Proteins Human genes 0.000 description 1
- 108010011756 Milk Proteins Proteins 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 235000018936 Vitellaria paradoxa Nutrition 0.000 description 1
- 241001135917 Vitellaria paradoxa Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000002535 acidifier Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical compound [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 235000019868 cocoa butter Nutrition 0.000 description 1
- 229940110456 cocoa butter Drugs 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 239000002385 cottonseed oil Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 235000013367 dietary fats Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 230000009969 flowable effect Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 239000003349 gelling agent Substances 0.000 description 1
- 239000010520 ghee Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000007407 health benefit Effects 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 235000021239 milk protein Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000007764 o/w emulsion Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920000223 polyglycerol Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000010491 poppyseed oil Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 229940057910 shea butter Drugs 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 239000003784 tall oil Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000000844 transformation Methods 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 238000011179 visual inspection Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/001—Spread compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
- A23D9/04—Working-up
- A23D9/05—Forming free-flowing pieces
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Edible Oils And Fats (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12168344 | 2012-05-16 | ||
| PCT/EP2013/058248 WO2013171027A1 (en) | 2012-05-16 | 2013-04-22 | Process for the preparation of edible fat-continuous emulsions |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EA201401260A1 EA201401260A1 (ru) | 2015-04-30 |
| EA025290B1 true EA025290B1 (ru) | 2016-12-30 |
Family
ID=48224803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EA201401260A EA025290B1 (ru) | 2012-05-16 | 2013-04-22 | Способ приготовления съедобных эмульсий на основе непрерывной жировой фазы |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US11350644B2 (https=) |
| EP (1) | EP2849573B1 (https=) |
| AU (1) | AU2013261968B2 (https=) |
| BR (1) | BR112014028059B1 (https=) |
| CA (1) | CA2872903C (https=) |
| EA (1) | EA025290B1 (https=) |
| HU (1) | HUE030241T2 (https=) |
| IN (1) | IN2014MN02279A (https=) |
| MX (1) | MX344433B (https=) |
| PL (1) | PL2849573T3 (https=) |
| WO (1) | WO2013171027A1 (https=) |
| ZA (1) | ZA201408341B (https=) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11412751B2 (en) | 2013-03-15 | 2022-08-16 | Upfield Europe B.V. | Edible aerated water-in-oil emulsions |
| CA2984060C (en) * | 2015-05-28 | 2023-01-24 | Unilever Bcs Limited | Process for preparing fat slurries and a process for preparing emulsions of such slurries |
| PL3393265T3 (pl) * | 2015-12-21 | 2019-08-30 | Upfield Europe B.V. | Sposób otrzymywania zawiesiny tłuszczowej zawierającej olej z oliwek i otrzymywania tłuszczu do smarowania zawierającego wspomnianą zawiesinę |
| EP3648612B1 (en) * | 2017-06-07 | 2021-06-09 | Upfield Europe B.V. | Process for making edible oil-continuous emulsions |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001041586A1 (en) * | 1999-12-10 | 2001-06-14 | Unilever N.V. | Heat treated, whippable oil in water emulsion |
| WO2005074722A1 (en) * | 2004-01-28 | 2005-08-18 | Unilever N.V. | Savoury food composition comprising low-trans triglyceride fat composition |
| WO2011160921A1 (en) * | 2010-06-22 | 2011-12-29 | Unilever Nv | Edible fat powders |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU604259B2 (en) * | 1986-09-26 | 1990-12-13 | Unilever Plc | Process for preparing an edible dispersion containing a continuous fat phase and an aqueous phase |
| US5139803A (en) | 1989-02-09 | 1992-08-18 | Nabisco, Inc. | Method and liposome composition for the stabilization of oxidizable substances |
| US7563748B2 (en) | 2003-06-23 | 2009-07-21 | Cognis Ip Management Gmbh | Alcohol alkoxylate carriers for pesticide active ingredients |
| ATE509692T1 (de) | 2003-07-17 | 2011-06-15 | Unilever Nv | Verfahren zur herstellung einer öl und strukturierungsmittel enthaltenden essbaren dispersion |
| WO2010000020A1 (en) | 2008-06-30 | 2010-01-07 | Cathrx Ltd | A catheter |
| CA2745973A1 (en) | 2008-12-19 | 2010-06-24 | Unilever Plc | Edible fat powders |
| PL2367437T3 (pl) | 2008-12-19 | 2014-08-29 | Unilever Bcs Europe Bv | Sposób wytwarzania jadalnego środka do smarowania z ciągłą fazą tłuszczową |
| PL2367440T3 (pl) * | 2008-12-19 | 2013-11-29 | Unilever Bcs Europe Bv | Sposób wytwarzania jadalnego środka do smarowania z ciągłą fazą tłuszczową |
| WO2011000020A1 (en) | 2009-06-12 | 2011-01-06 | Sbc Research Pty Ltd | Enhanced method of detection |
-
2013
- 2013-04-22 MX MX2014013787A patent/MX344433B/es active IP Right Grant
- 2013-04-22 EP EP13719287.8A patent/EP2849573B1/en active Active
- 2013-04-22 HU HUE13719287A patent/HUE030241T2/en unknown
- 2013-04-22 CA CA2872903A patent/CA2872903C/en active Active
- 2013-04-22 EA EA201401260A patent/EA025290B1/ru not_active IP Right Cessation
- 2013-04-22 IN IN2279MUN2014 patent/IN2014MN02279A/en unknown
- 2013-04-22 WO PCT/EP2013/058248 patent/WO2013171027A1/en not_active Ceased
- 2013-04-22 AU AU2013261968A patent/AU2013261968B2/en active Active
- 2013-04-22 BR BR112014028059-2A patent/BR112014028059B1/pt active IP Right Grant
- 2013-04-22 US US14/400,173 patent/US11350644B2/en active Active
- 2013-04-22 PL PL13719287T patent/PL2849573T3/pl unknown
-
2014
- 2014-11-13 ZA ZA2014/08341A patent/ZA201408341B/en unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001041586A1 (en) * | 1999-12-10 | 2001-06-14 | Unilever N.V. | Heat treated, whippable oil in water emulsion |
| WO2005074722A1 (en) * | 2004-01-28 | 2005-08-18 | Unilever N.V. | Savoury food composition comprising low-trans triglyceride fat composition |
| WO2011160921A1 (en) * | 2010-06-22 | 2011-12-29 | Unilever Nv | Edible fat powders |
Also Published As
| Publication number | Publication date |
|---|---|
| US20150140197A1 (en) | 2015-05-21 |
| AU2013261968A1 (en) | 2014-11-27 |
| HUE030241T2 (en) | 2017-04-28 |
| ZA201408341B (en) | 2016-09-28 |
| MX344433B (es) | 2016-12-15 |
| CA2872903C (en) | 2020-04-14 |
| IN2014MN02279A (https=) | 2015-08-07 |
| BR112014028059B1 (pt) | 2020-11-17 |
| EA201401260A1 (ru) | 2015-04-30 |
| PL2849573T3 (pl) | 2017-01-31 |
| CA2872903A1 (en) | 2013-11-21 |
| EP2849573A1 (en) | 2015-03-25 |
| EP2849573B1 (en) | 2016-07-27 |
| BR112014028059A2 (pt) | 2017-06-27 |
| AU2013261968B2 (en) | 2015-04-09 |
| WO2013171027A1 (en) | 2013-11-21 |
| MX2014013787A (es) | 2015-01-26 |
| US11350644B2 (en) | 2022-06-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s) |
Designated state(s): AM AZ BY KZ KG TJ TM |
|
| PC4A | Registration of transfer of a eurasian patent by assignment |