DK3801892T3 - Fremgangsmåde til fremstilling af en zeolit af høj renhed med en struktur af typen afx med et organisk, nitrogenholdigt struktureringsmiddel - Google Patents

Fremgangsmåde til fremstilling af en zeolit af høj renhed med en struktur af typen afx med et organisk, nitrogenholdigt struktureringsmiddel Download PDF

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Publication number
DK3801892T3
DK3801892T3 DK19723802.5T DK19723802T DK3801892T3 DK 3801892 T3 DK3801892 T3 DK 3801892T3 DK 19723802 T DK19723802 T DK 19723802T DK 3801892 T3 DK3801892 T3 DK 3801892T3
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Denmark
Prior art keywords
zeolith
procedure
preparation
high purity
nitrogen containing
Prior art date
Application number
DK19723802.5T
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English (en)
Inventor
Franco Raquel Martinez
Eric Llido
David Berthout
Bogdan Harbuzaru
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Ifp Energies Now
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Application filed by Ifp Energies Now filed Critical Ifp Energies Now
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Publication of DK3801892T3 publication Critical patent/DK3801892T3/da

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16Alumino-silicates
    • B01J20/18Synthetic zeolitic molecular sieves
    • B01J20/186Chemical treatments in view of modifying the properties of the sieve, e.g. increasing the stability or the activity, also decreasing the activity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/305Addition of material, later completely removed, e.g. as result of heat treatment, leaching or washing, e.g. for forming pores
    • B01J20/3057Use of a templating or imprinting material ; filling pores of a substrate or matrix followed by the removal of the substrate or matrix
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3071Washing or leaching
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3078Thermal treatment, e.g. calcining or pyrolizing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04Mixing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06Washing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08Heat treatment
    • B01J37/10Heat treatment in the presence of water, e.g. steam
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
DK19723802.5T 2018-05-24 2019-05-16 Fremgangsmåde til fremstilling af en zeolit af høj renhed med en struktur af typen afx med et organisk, nitrogenholdigt struktureringsmiddel DK3801892T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1854383A FR3081347B1 (fr) 2018-05-24 2018-05-24 Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
PCT/EP2019/062556 WO2019224084A1 (fr) 2018-05-24 2019-05-16 Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote

Publications (1)

Publication Number Publication Date
DK3801892T3 true DK3801892T3 (da) 2024-07-15

Family

ID=63896256

Family Applications (1)

Application Number Title Priority Date Filing Date
DK19723802.5T DK3801892T3 (da) 2018-05-24 2019-05-16 Fremgangsmåde til fremstilling af en zeolit af høj renhed med en struktur af typen afx med et organisk, nitrogenholdigt struktureringsmiddel

Country Status (8)

Country Link
US (1) US11643332B2 (da)
EP (1) EP3801892B1 (da)
JP (1) JP7355762B2 (da)
KR (1) KR20210011385A (da)
CN (1) CN112188927A (da)
DK (1) DK3801892T3 (da)
FR (1) FR3081347B1 (da)
WO (1) WO2019224084A1 (da)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3081347B1 (fr) 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote
FR3095199B1 (fr) * 2019-04-19 2021-10-29 Ifp Energies Now Procédé de synthèse rapide d'une zeolithe de type structural AFX avec une source de faujasite

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4508837A (en) 1982-09-28 1985-04-02 Chevron Research Company Zeolite SSZ-16
US5194235A (en) 1992-08-27 1993-03-16 Chevron Research And Technology Company Synthesis of SSZ-16 zeolite catalyst
FR2936790B1 (fr) * 2008-10-07 2010-09-24 Inst Francais Du Petrole Procede de preparation d'une zeolithe de type structural mtw
WO2010118377A2 (en) * 2009-04-09 2010-10-14 California Institute Of Technology Molecular sieves and related methods and structure directing agents
RU2637021C2 (ru) * 2012-10-18 2017-11-29 Басф Се Последующая обработка цеолитного материала
RU2732126C2 (ru) * 2014-11-14 2020-09-11 Джонсон Мэтти Паблик Лимитед Компани Afx цеолит
US10046316B2 (en) * 2015-02-05 2018-08-14 Tosoh Corporation Zeolite
JP6430303B2 (ja) 2015-03-16 2018-11-28 国立大学法人横浜国立大学 Afx型ゼオライトの製法
EP3377194A1 (en) * 2015-11-16 2018-09-26 Exxonmobil Upstream Research Company Adsorbent materials and methods of adsorbing carbon dioxide
US9868643B2 (en) 2016-05-20 2018-01-16 Chevron U.S.A. Inc. Synthesis of zeolite SSZ-16
BR112018070992A2 (pt) * 2016-05-24 2019-01-29 Exxonmobil Chemical Patents Inc zeólita sintética compreendendo um metal catalítico
US9908108B2 (en) * 2016-06-07 2018-03-06 Chevron U.S.A. Inc. High-silica AFX framework type zeolites
EP3464180B1 (en) 2016-06-07 2021-09-29 Chevron U.S.A. Inc. High-silica afx framework type zeolites
WO2018064318A1 (en) 2016-09-30 2018-04-05 Johnson Matthey Public Limited Company A novel zeolite synthesis with alkaline earth metal
US10414665B2 (en) 2016-09-30 2019-09-17 Johnson Matthey Public Limited Company Synthesis of AFX zeolite
FR3064261B1 (fr) 2017-03-24 2019-03-22 IFP Energies Nouvelles Procede de synthese de la zeolithe izm-2 en presence d'un structurant dihydroxyde de 1,6-bis(methylpiperidinium)hexane
FR3064262B1 (fr) 2017-03-24 2019-03-22 IFP Energies Nouvelles Procede de synthese de la zeolithe izm-2 en presence d'un structurant dibromure de 1,6-bis(methylpiperidinium)hexane
US10053368B1 (en) 2017-09-07 2018-08-21 Chevron U.S.A. Inc. Synthesis of AFX framework type molecular sieves
FR3081345B1 (fr) 2018-05-24 2023-11-10 Ifp Energies Now Procede de synthese d'une zeolithe de type structural afx de tres haute purete en presence d'un structurant organique azote
FR3081348B1 (fr) 2018-05-24 2023-11-10 Ifp Energies Now Catalyseur comprenant une zeolithe de type structural afx de tres haute purete et au moins un metal de transition pour la reduction selective de nox
FR3081347B1 (fr) 2018-05-24 2023-07-28 Ifp Energies Now Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote

Also Published As

Publication number Publication date
US20210206650A1 (en) 2021-07-08
JP2021524432A (ja) 2021-09-13
FR3081347B1 (fr) 2023-07-28
EP3801892B1 (fr) 2024-04-17
FR3081347A1 (fr) 2019-11-29
US11643332B2 (en) 2023-05-09
KR20210011385A (ko) 2021-02-01
WO2019224084A1 (fr) 2019-11-28
EP3801892A1 (fr) 2021-04-14
CN112188927A (zh) 2021-01-05
JP7355762B2 (ja) 2023-10-03

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