DK2049645T3 - Ølklaringshjælpemiddel baseret på siliciumdioxid-xerogel med høj filtrerbarhed - Google Patents

Ølklaringshjælpemiddel baseret på siliciumdioxid-xerogel med høj filtrerbarhed Download PDF

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Publication number
DK2049645T3
DK2049645T3 DK07786398.3T DK07786398T DK2049645T3 DK 2049645 T3 DK2049645 T3 DK 2049645T3 DK 07786398 T DK07786398 T DK 07786398T DK 2049645 T3 DK2049645 T3 DK 2049645T3
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Denmark
Prior art keywords
composition
xerogel
particles
weight
beer
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DK07786398.3T
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English (en)
Inventor
Georg Lüers
Massoud Jalalpoor
Dominik Sedlmayer
Andreas Seewald
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Grace Gmbh & Co Kg
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Publication of DK2049645T3 publication Critical patent/DK2049645T3/da

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    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/04—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material
    • C12H1/0408—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material with the aid of ion-exchange material or inert clarification material, e.g. adsorption material with the aid of inorganic added material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/103—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate comprising silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28047—Gels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28061—Surface area, e.g. B.E.T specific surface area being in the range 100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069—Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06—Precipitation by physical means, e.g. by irradiation, vibrations
    • C12H1/063—Separation by filtration

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • General Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Wood Science & Technology (AREA)
  • General Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Toxicology (AREA)
  • Dispersion Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Silicon Polymers (AREA)

Claims (15)

1. Sammensætning, som er nyttig til behandling af drikkevarer, omfattende xerogel-partikler med et porevolumen på fra 0,2 til 2,0 ml/g, og en middelpartikelstørrelse på fra 5 til 40 pm, hvor sammensætningen omfatter 20 vægt% eller mindre affine partikler.
2. Sammensætning ifølge krav 1, hvor xerogelen omfatter fugt i en mængde på 20 vægt% eller mindre.
3. Sammensætning ifølge krav 1, hvor xerogelen omfatter siliciumdioxid.
4. Sammensætning ifølge krav 1, hvor middelpartikelstørrelsen ligger i området fra 10 til 25 pm.
5. Sammensætning ifølge krav 1, hvor sammensætningen omfatter 18 vægt% eller mindre affine partikler.
6. Sammensætning ifølge krav 1, hvor sammensætningen omfatter 15 vægt% eller mindre affine partikler.
7. Sammensætning ifølge krav 1, hvor middelpartikelstørrelsen ligger i området fra 10 til 25 pm og et overfladeareal på 400 til 800 m2/g.
8. Sammensætning ifølge krav 1, hvor sammensætningen omfatter en filtrerbarhed på i det mindste 40 mDarcy.
9. Fremgangsmåde til fremstilling af en sammensætning, som er nyttig til behandling af drikkevarer, omfattende: fremstilling af en hydrogel; opvarmning af hydrogelen for dannelse af en xerogel; formaling af xerogelen for dannelse af partikler; og fjernelse af fine partikler fra sammensætningen således, at sammensætningen omfatter xerogelpartikler med et porevolumen på fra 0,2 til 2,0 ml/g, og en middelpartikelstørrelse på fra 5 til 40 pm, og sammensætningen omfatter 20 vægt% eller mindre affine partikler.
10. Fremgangsmåde ifølge krav 9, hvor xerogelen omfatter fugtighed i en mængde på 20 vægt% eller mindre.
11. Fremgangsmåde ifølge krav 9, hvor middelpartikelstørrelsen ligger i området fra 10 til 25 pm.
12. Fremgangsmåde til behandling afen drikkevare, omfattende: tilvejebringelse af en xerogelsammensætning; tilvejebringelse af en drikkevare; og filtrering af drikkevaren med xerogelsammensætningen, hvor sammensætningen omfatter xerogelpartikler med et porevolumen på fra 0,2 til 2,0 ml/g, en middelpartikelstørrelse på fra 5 til 40 pm, hvor sammensætningen omfatter 20 vægt% eller mindre affine partikler.
13. Fremgangsmåde ifølge krav 12, hvor drikkevaren omfatter øl, vin, eller frugtjuice.
14. Fremgangsmåde ifølge krav 12, hvor sammensætningen omfatter 18 vægt% eller mindre affine partikler.
15. Fremgangsmåde ifølge krav 12, hvor sammensætningen omfatter 15 vægt% eller mindre affine partikler.
DK07786398.3T 2006-08-07 2007-07-27 Ølklaringshjælpemiddel baseret på siliciumdioxid-xerogel med høj filtrerbarhed DK2049645T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US83609106P 2006-08-07 2006-08-07
PCT/EP2007/006687 WO2008017393A1 (en) 2006-08-07 2007-07-27 Beer clarification aid based on silica xerogel with high filterability

Publications (1)

Publication Number Publication Date
DK2049645T3 true DK2049645T3 (da) 2016-06-06

Family

ID=38508779

Family Applications (1)

Application Number Title Priority Date Filing Date
DK07786398.3T DK2049645T3 (da) 2006-08-07 2007-07-27 Ølklaringshjælpemiddel baseret på siliciumdioxid-xerogel med høj filtrerbarhed

Country Status (19)

Country Link
US (1) US10633621B2 (da)
EP (1) EP2049645B1 (da)
JP (1) JP2010500010A (da)
CN (2) CN101541942A (da)
AR (1) AR062237A1 (da)
AU (1) AU2007283125A1 (da)
BR (1) BRPI0715390B1 (da)
CL (1) CL2007002291A1 (da)
DK (1) DK2049645T3 (da)
ES (1) ES2573227T3 (da)
HK (1) HK1222671A1 (da)
HU (1) HUE029242T2 (da)
MX (1) MX2009001405A (da)
PL (1) PL2049645T3 (da)
PT (1) PT2049645T (da)
RU (1) RU2009108297A (da)
SI (1) SI2049645T1 (da)
TW (1) TW200817504A (da)
WO (1) WO2008017393A1 (da)

Families Citing this family (6)

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JP5443058B2 (ja) * 2008-06-11 2014-03-19 富士シリシア化学株式会社 ビール安定化処理用シリカゲル、およびビール安定化処理方法
US8409647B2 (en) * 2008-08-12 2013-04-02 E. I. Du Pont De Nemours And Company Silica microgels for reducing chill haze
DE102008060446A1 (de) * 2008-12-04 2010-06-10 Krones Ag Verfahren zum Ermitteln der Filtrierbarkeit von Bier
CA3138781A1 (en) * 2018-08-01 2020-02-06 Yanee WUTTHINITIKORNKIT Process of improving the flavour and aroma of liquor
JP2020110090A (ja) * 2019-01-11 2020-07-27 アサヒビール株式会社 発酵麦芽飲料の製造方法及び発酵液の濾過方法
CN110156034B (zh) * 2019-07-08 2020-10-23 福建远翔新材料股份有限公司 一种高效啤酒防混浊剂用纳米二氧化硅的生产方法

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Also Published As

Publication number Publication date
MX2009001405A (es) 2009-03-13
TW200817504A (en) 2008-04-16
CN101541942A (zh) 2009-09-23
CL2007002291A1 (es) 2008-05-02
RU2009108297A (ru) 2010-09-20
ES2573227T3 (es) 2016-06-06
PT2049645T (pt) 2016-07-14
BRPI0715390A2 (pt) 2013-06-25
JP2010500010A (ja) 2010-01-07
PL2049645T3 (pl) 2016-09-30
HK1222671A1 (zh) 2017-07-07
HUE029242T2 (en) 2017-02-28
EP2049645A1 (en) 2009-04-22
AU2007283125A1 (en) 2008-02-14
BRPI0715390B1 (pt) 2016-03-22
EP2049645B1 (en) 2016-04-06
SI2049645T1 (sl) 2016-08-31
AR062237A1 (es) 2008-10-22
WO2008017393A1 (en) 2008-02-14
CN105400676A (zh) 2016-03-16
US20100112132A1 (en) 2010-05-06
US10633621B2 (en) 2020-04-28

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