DEP0037280DA - Verfahren zur Trennung von Cyanurchlorid aus sublimierenden Eisensalzen - Google Patents
Verfahren zur Trennung von Cyanurchlorid aus sublimierenden EisensalzenInfo
- Publication number
- DEP0037280DA DEP0037280DA DEP0037280DA DE P0037280D A DEP0037280D A DE P0037280DA DE P0037280D A DEP0037280D A DE P0037280DA
- Authority
- DE
- Germany
- Prior art keywords
- cyanuric chloride
- subliming
- separation
- iron salts
- chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 title description 4
- 159000000014 iron salts Chemical class 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 238000000926 separation method Methods 0.000 title 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 239000003054 catalyst Substances 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
Description
EÄ.13736^
Xteutsolie Gold- waä ^über«- Schcideanstalt Tormals
m/U * ueiesfiraitnetraee· 9
Tferfcüura» «f Tyeanujng Tor. Cyanurchlorid aus
Kb i@% Mannt» d&oroytn im Cegeawart von Katalysatoren im Cjaiiiircüloriö tibtamfcftthreae Is ist auch bereite w*g«0@ÄlA
gen aorden, hierbei Metßllchlcride eis Katalysatoren su
*t®m®mi®ii<s Tersuehc? habGii auu ergeben, dass die Polymerisation if<m Chlorcji^n ^u CyAiAUi^cIu-OrId Bit guter Ausbeute
coeriialb 5oo° in GegMieart von
duroiigeführt werden k^mr Bei dieses Terfabxen JEöOht ßioh jedooli die ^u'olis^tionsteaderis tob bei 4ea .-irbeitsteatperat
reu mh® cdcr weniger flüchtigen Eiseus«l£enf insbesondere
stireaä beaerk^r, dass Uas 4\iroh das fIUoJati;?a
Is mn*ä@ nun jge&&4föt dass eine n&ohtragliohQ Heini gtuo^ eines auf ui'jse W@i0e burgee teilten Cyacurchloride nioht
lioh. ist.; 9ms& warn die Reaktioncproöiücte durah b«2 poröse Kohle, inebssondere Äktirkohle, leitet, U"berrasalieiiderweiße 1st sioh dabei geseilt, dass die flüoktigen liisensalae,
insbesondere ^isen- 3-Cblorid,' auch bei höheren '-TeiBperatiireii^ die 0%ertoalb dor SubliiDAtionagrense, sogar oberhalb d«a
Siede punk tee ten Ferrichlorid liegen, von der Kohle se «eitgehcnd adsorbiert werden, dass eise praktißah rollstäadige
von dem Cyanurchlorid möglich ist Obm Cyaniirohlorid
passiert die ^ohle Wi den Arbeitetemperature^ a B 2oo und 45o° liinTerändert und naheau Quantität ir
Claims (1)
- Itie&lsss ff ill smm ^emmmg von C^aaarohlorid uod %·&2oo und °wi« Eisen-Chlorid, inetesoadere %*t d«r voa Cyanurehloriö mm Chloreyen ia GegeatMtrt eisenhaltigen fiataljsatoreii, dadurch gekemiseioluiet, oma Öle ^iapfe, die Cyamirohlorid und die flüohtl^»t€n? durok %mm* über poröae, ktivkohie, leitet,
Family
ID=
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