DE968661C - Method for operating filters operating below room temperature, in particular cooled rotary filters - Google Patents

Method for operating filters operating below room temperature, in particular cooled rotary filters

Info

Publication number
DE968661C
DE968661C DEM1193D DEM0001193D DE968661C DE 968661 C DE968661 C DE 968661C DE M1193 D DEM1193 D DE M1193D DE M0001193 D DEM0001193 D DE M0001193D DE 968661 C DE968661 C DE 968661C
Authority
DE
Germany
Prior art keywords
filters
operating
room temperature
below room
trough
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEM1193D
Other languages
German (de)
Inventor
Dipl-Ing Gustav Netzel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Maschf GmbH
Original Assignee
Imperial Maschf GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Maschf GmbH filed Critical Imperial Maschf GmbH
Priority to DEM1193D priority Critical patent/DE968661C/en
Application granted granted Critical
Publication of DE968661C publication Critical patent/DE968661C/en
Expired legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D33/00Filters with filtering elements which move during the filtering operation
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/02Recovery of petroleum waxes from hydrocarbon oils; Dewaxing of hydrocarbon oils
    • C10G73/025Recovery of petroleum waxes from hydrocarbon oils; Dewaxing of hydrocarbon oils by filtration

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Drying Of Solid Materials (AREA)

Description

Verfahren zum Betrieb von unterhalb der Raumtemperatur arbeitenden Filtern, insbesondere gekühlten Drehfiltern Die Erfindung bezieht sich auf ein Verfahren zum Betrieb von unterhalb der Raumtemperatur arbeitenden Filtern, insbesondere gekühlten Drehfiltern.Procedure for operating below room temperature Filters, especially cooled rotary filters The invention relates to a method for the operation of filters that work below room temperature, especially those that are cooled Rotary filters.

Ein solches Filtrieren erfolgt im allgemeinen, um in den zu filtrierenden Stoffen enthaltene störende Beimengungen auszukristallisieren oder zu erhärten und dadurch von der Flüssigkeit zu trennen. Beispielsweise wird ein solches Filtrieren bei der sogenannten Entparaffinierung von Ölen angewendet, um aus ihnen das für den Anwendungszweck schädliche Paraffin abzutrennen und ein Ö1 mit einem niedrigen Stockpunkt zu erhalten. Such filtering is generally carried out in order to be filtered into the To crystallize or harden and disrupt substances contained in thereby separating from the liquid. For example, such filtering is used in the so-called dewaxing of oils used to make them for the intended use to separate harmful paraffin and an oil with a low To get pour point.

Zur Durchführung einer solchen Filterung wird entweder der zu filternde Stoff entsprechend tief gekühlt dem Trog zugeführt oder im bzw. am Trog eine von einem geeigneten Kühlmittel durchflossene Kühlanlage vorgesehen. Unter Umständen werden beide Maßnahmen gleichzeitig getroffen. Im Großbetrieb werden vorzugsweise gekapselte Drehfilter eingesetzt, bei denen in dem Kapselgehäuse oberhalb des Filtertroges das Trocknen des Kuchens durch Saug- oder Druckluft und vielfach auch noch das Waschen des Kuchens erfolgt. Wenn die den Trog abdeckende Haube auch indirekt vom Trog her gekühlt wird, so herrscht in ihrem Innern, selbst bei Abdämmung nach außen, durch den Wärmeleitverlust eine nicht unwesentlich höhere Temperatur als im Trog. Infolgedessen lösen sich die imTrog in den festen Zustand übergeführten, im Kuchen befindlichen Stoffe teilweise bei Überführung des Kuchens aus dem Trog zur Trockenzone und zur Waschzone wieder auf. Die wieder gelösten Stoffe gelangen dann doch noch in das Filtrat, von dem sie bereits getrennt waren. In dem Filtertuch verbleiben Reste der wieder verflüssigten Stoffe. Diese kristallisieren aus bzw. erhärten, wenn das Filtertuch wieder in die kalte Trogfiüssigkeit eintaucht, und führen zu Verstopfungen des Tuches. Die wieder verflüssigten Stoffe beeinträchtigen auch den Waschvorgang, da sie beim Aufbringen der Waschflüssigkeit erstarren und dabei die Teilchen des Kuchens zusammenbacken, wodurch die Durchlässigkeit des Kuchens für die Waschflüssigkeit herabgesetzt wird. To carry out such a filtering, either the The substance is fed to the trough cooled down accordingly or one of the troughs in or on the trough a suitable coolant through which a cooling system is provided. In certain circumstances both measures are taken at the same time. In large operations are preferred encapsulated rotary filter used, in which in the capsule housing above the filter trough drying the cake with suction or compressed air and, in many cases, washing it of the cake. If the hood covering the trough also indirectly from the trough is cooled, so prevails inside, even with damming to the outside the heat conduction loss a not insignificantly higher temperature than in the trough. Consequently dissolve in the trough in the solid state transferred, in the cake some of the substances found when transferring the cake from the trough to the drying zone and back up to the washing zone. The substances that have been dissolved again still get there into the filtrate from which they were already separated. Remain in the filter cloth Remnants of the re-liquefied substances. These crystallize or harden, when the filter cloth is immersed again in the cold trough liquid and feed Clogging of the cloth. The re-liquefied substances also affect the Washing process, as they solidify when the washing liquid is applied and thereby the Particles of the cake bake together, which increases the permeability of the cake the washing liquid is reduced.

Diese Nachteile hat man durch Einleiten von gekühltem Inertgas unter die Haube oder durch Verwendung eines besonders tief gekühlten Waschmittels, das während des Versprühens durch Verdampfungswärme die Umgebung kühlt, zu beheben versucht. In beiden Fällen ist eine dauernde, viel Aufmerksamkeit erfordernde Kontrolle sowohl der Temperatur des Troginhaltes als auch der Temperatur unter der Haube erforderlich, um gleiche Wärmeverhältnisse in beiden Räumen einzuhalten. These disadvantages are overcome by introducing cooled inert gas the hood or by using a particularly deeply refrigerated detergent that trying to remedy the environment cools during the spraying by heat of vaporization. In both cases there is a constant, careful inspection both the temperature of the trough contents as well as the temperature under the hood required, in order to maintain the same heat conditions in both rooms.

Bei automatischer Temperaturregelung müssen für den Trog und die Haube besondere Temperaturfühler und für das Kühlmittel des Troges sowie das Kühlmittel der Haube besondere Regelvorrichtungen vorgesehen werden.With automatic temperature control, the trough and the hood special temperature sensors and for the coolant of the trough and the coolant special control devices are provided for the hood.

Gemäß der Erfindung wird eine wesentliche Vereinfachung dadurch erzielt, daß die Kühlung des über der Filterfläche befindlichen Raumes durch Rohrleitungen erfolgt, die von der zu filtrierenden tiefgekühlten Rohflüssigkeit durchflossen werden, welche hierauf dem Filtertrog zugeführt wird. Bei der erfindungsgemäßen Einrichtung braucht lediglich eine einzige Temperatur, nämlich die der gemeinsam zur Kühlung des Raumes unter der Haube und zur Kühlung des Troges dienenden Rohflüssig-Iieit beobachtet und geregelt zu werden. Bei automatischer Temperaturregelung benötigt man nur einen einzigen Wärmefühler und eine einzige Regelvorrichtung Beim Betrieb anderer Filter, in denen zunächst kein Gasraum vorhanden ist, z. B. Kerzenfilter, Filterpressen u. dgl., kann der Erfindungsgegenstand auch in entsprechend abgeänderter Form zur Anwendung gelangen. Da meistens mehrere Filter dieser Art aufgestellt werden, wird die als wärmeaufnehmendes Mittel dienende Rohflüssigkeit zunächst den Filtern zugeleitet, auf denen ein Trockenvorgang stattfindet, und anschließend solchen, in denen diese filtriert wird. Hierdurch wird vermieden, daß der Drück-, Wasch- und Trocltensaugvorgang bei einer höheren als der Filtertemperatur vor sich geht. According to the invention, a significant simplification is achieved by that the cooling of the space located above the filter surface by pipelines takes place through which the deep-frozen raw liquid to be filtered flows which is then fed to the filter trough. In the inventive The device only needs a single temperature, namely that of the common for cooling the space under the hood and for cooling the trough serving raw liquid to be observed and regulated. Required for automatic temperature control you only have a single heat sensor and a single control device during operation other filters in which there is initially no gas space, e.g. B. candle filter, Filter presses and the like, the subject matter of the invention can also be modified accordingly Form to apply. Since several filters of this type are usually set up, the raw liquid, which serves as a heat-absorbing agent, is first fed to the filters on which a drying process takes place, and then those on which a drying process takes place in which this is filtered. This avoids that the pressure, washing and dry suction takes place at a higher than the filter temperature.

Claims (1)

PATENTANSPRUCH: Verfahren zum Betrieb von unterhalb der Raumtemperatur arbeitenden Filtern, insbesondere gekühlten Drehfiltern, bei denen die Temperatur im Filter während des Waschens und Trockensaugvorganges möglichst gleich der Temperatur des Filtervorganges sein soll, dadurch gekennzeichnet, daß die Kühlung des über der Filterfläche befindlichen Raumes durch Rohrleitungen erfolgt, die von der zu filtrierenden gekühlten Rohflüssigkeit durchflossen werden, welche hierauf dem Filtertrog zugeführt wird. PATENT CLAIM: Process for operation from below room temperature working filters, especially cooled rotary filters, in which the temperature the same temperature as possible in the filter during washing and dry vacuuming of the filtering process should be, characterized in that the cooling of the over The space located on the filter surface is carried out by pipes leading from the to filtered, cooled raw liquid are flowed through, which then the filter trough is fed. In Betracht gezogene Druckschriften: Britische Patentschrift Nr. 455 272; USA.-Patentschrift Nr. I994485; französische Patentschrift Nr. 790 634. Documents considered: British Patent No. 455 272; U.S. Patent No. I994485; French patent specification No. 790 634.
DEM1193D 1943-06-06 1943-06-06 Method for operating filters operating below room temperature, in particular cooled rotary filters Expired DE968661C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEM1193D DE968661C (en) 1943-06-06 1943-06-06 Method for operating filters operating below room temperature, in particular cooled rotary filters

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEM1193D DE968661C (en) 1943-06-06 1943-06-06 Method for operating filters operating below room temperature, in particular cooled rotary filters

Publications (1)

Publication Number Publication Date
DE968661C true DE968661C (en) 1958-03-20

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
DEM1193D Expired DE968661C (en) 1943-06-06 1943-06-06 Method for operating filters operating below room temperature, in particular cooled rotary filters

Country Status (1)

Country Link
DE (1) DE968661C (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1994485A (en) * 1931-06-20 1935-03-19 Atlantic Refining Co Treatment of oil-wax mixtures
FR790634A (en) * 1934-06-29 1935-11-25 Alco Products Improved process for dewaxing hydrocarbon oils
GB455272A (en) * 1934-03-31 1936-10-12 Texaco Development Corp Improvements in separation of wax from mineral oil by filtration

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1994485A (en) * 1931-06-20 1935-03-19 Atlantic Refining Co Treatment of oil-wax mixtures
GB455272A (en) * 1934-03-31 1936-10-12 Texaco Development Corp Improvements in separation of wax from mineral oil by filtration
FR790634A (en) * 1934-06-29 1935-11-25 Alco Products Improved process for dewaxing hydrocarbon oils

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