DE813188C - Process for the production of glue powder - Google Patents

Process for the production of glue powder

Info

Publication number
DE813188C
DE813188C DED4554A DED0004554A DE813188C DE 813188 C DE813188 C DE 813188C DE D4554 A DED4554 A DE D4554A DE D0004554 A DED0004554 A DE D0004554A DE 813188 C DE813188 C DE 813188C
Authority
DE
Germany
Prior art keywords
glue
production
glue powder
powder
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DED4554A
Other languages
German (de)
Inventor
Robert Stoebe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HELLMUTH HOLZ DR
Original Assignee
HELLMUTH HOLZ DR
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HELLMUTH HOLZ DR filed Critical HELLMUTH HOLZ DR
Priority to DED4554A priority Critical patent/DE813188C/en
Application granted granted Critical
Publication of DE813188C publication Critical patent/DE813188C/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09HPREPARATION OF GLUE OR GELATINE
    • C09H9/00Drying of glue or gelatine
    • C09H9/04Drying of glue or gelatine in the form of granules, e.g. beads

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Description

Verfahren zur Herstellung von Leimpulver Knochen- oder Hautleimbrühen, die meist 500/0 Wasser enthalten, werden gewöhnlich mittels eines Warmluftstromes bis zu einem Wassergehalt von etwa 12(/o getrocknet, worauf die Masse z, B. in Formen gegossen wird. Zur Gewinnung von Leimpulver muß der Leim dann noch mechanisch zerkleinert werden. Man hat auch schon vorgeschlagen, Leimpulver durch Abschaben der Leimlösung von einer drehenden Trommel unter Vakuum herzustellen; es sind hierfür jedoch teuere und umfangreiche Anlagen notwendig.Process for the production of glue powder, bone or hide glue broth, which usually contain 500/0 water, are usually by means of a stream of warm air to a water content of about 12 (/ o dried, after which the mass, e.g. in molds is poured. To obtain glue powder, the glue then has to be mechanically comminuted will. It has also been suggested to use glue powder by scraping off the glue solution manufacture from a rotating drum under vacuum; however, they are expensive for this and extensive systems are necessary.

Es wurde ein einfaches und wirtschaftliches Verfahren zur Herstellung von hochwertigem, fast farblosem Leimpulver aus wäßrigen Leimlösungen ohne Anwendung mechanischer Zerkleinerungsvorrichtungen gefunden. Das Verfahren besteht im wesentlichen darin, daß die Leimlösung mit organischen Lösungsmitteln, vornehmlich Perchloräthylen, vermischt und unter starkem Rühren so lange destilliert wird, bis praktisch kein Wasser mehr übergeht, worauf das restliche Lösungsmittel entfernt wird, z. B. mittels Vakuum, Warmluft, gespannten Wasserdampfes o. dgl. Überraschenderweise fällt dabei ein mehr oder minder feinkörniges Leimpulver von praktisch weißer Farbe an, welches sich leicht in Wasser löst. Das Pulver kann, da es sehr spröde ist, durch Mahlen noch weiter verfeinert werden.It became a simple and economical method of manufacture of high-quality, almost colorless glue powder from aqueous glue solutions without application mechanical crushers found. The procedure essentially consists that the glue solution with organic solvents, primarily perchlorethylene, mixed and distilled with vigorous stirring until practically none More water passes over, whereupon the remaining solvent is removed, e.g. B. by means of Vacuum, warm air, pressurized steam or the like. Surprisingly, this falls a more or less fine-grained glue powder of practically white color, which easily dissolves in water. The powder can, as it is very brittle, by grinding can be further refined.

Claims (1)

PATENTANSPRÜCHE: t. Verfahren zur Herstellung von Leimpulver aus Leimbrühen, dadurch gekennzeichnet, daß die Leimlösung mit einem organischen Lösungsmittel vermischt und unter starkem Rühren so lange destilliert wird, bis praktisch kein Wasser mehr übergeht, worauf das restliche Lösungsmittel entfernt wird. z. Verfahren nach Anspruch t, dadurch gekennzeichnet, daß man Lösungsmittel verwendet mit einem Siedepunkt über too°. 3. Verfahren nach Anspruch z, dadurch gekennzeichnet, daß man als Lösungsmittel Perchloräthylen verwendet. PATENT CLAIMS: t. Process for the production of glue powder from glue broths, characterized in that the glue solution is mixed with an organic solvent and distilled with vigorous stirring until practically no more water passes over, whereupon the remaining solvent is removed. z. Process according to Claim t, characterized in that solvents with a boiling point above too ° are used. 3. The method according to claim z, characterized in that the solvent used is perchlorethylene.
DED4554A 1950-06-25 1950-06-25 Process for the production of glue powder Expired DE813188C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DED4554A DE813188C (en) 1950-06-25 1950-06-25 Process for the production of glue powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DED4554A DE813188C (en) 1950-06-25 1950-06-25 Process for the production of glue powder

Publications (1)

Publication Number Publication Date
DE813188C true DE813188C (en) 1951-09-10

Family

ID=7031058

Family Applications (1)

Application Number Title Priority Date Filing Date
DED4554A Expired DE813188C (en) 1950-06-25 1950-06-25 Process for the production of glue powder

Country Status (1)

Country Link
DE (1) DE813188C (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0132142A1 (en) * 1983-07-14 1985-01-23 Hitachi Chemical Co., Ltd. Production of gelatin spherical gels
EP0132983A1 (en) * 1983-07-14 1985-02-13 Hitachi Chemical Co., Ltd. Production of gelatin spherical gels and their use

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0132142A1 (en) * 1983-07-14 1985-01-23 Hitachi Chemical Co., Ltd. Production of gelatin spherical gels
EP0132983A1 (en) * 1983-07-14 1985-02-13 Hitachi Chemical Co., Ltd. Production of gelatin spherical gels and their use

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