DE69911186D1 - Verfahren zur reinigung und verwendung von 2-chloro-1,1,1,2,3,3,3-heptafluorpropan und ihre azeotrope mit hf - Google Patents

Verfahren zur reinigung und verwendung von 2-chloro-1,1,1,2,3,3,3-heptafluorpropan und ihre azeotrope mit hf

Info

Publication number
DE69911186D1
DE69911186D1 DE69911186T DE69911186T DE69911186D1 DE 69911186 D1 DE69911186 D1 DE 69911186D1 DE 69911186 T DE69911186 T DE 69911186T DE 69911186 T DE69911186 T DE 69911186T DE 69911186 D1 DE69911186 D1 DE 69911186D1
Authority
DE
Germany
Prior art keywords
heptafluorpropane
azeotrope
chloro
purifying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69911186T
Other languages
English (en)
Other versions
DE69911186T2 (de
Inventor
Newton Miller
N Rao
H Swearingen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Application granted granted Critical
Publication of DE69911186D1 publication Critical patent/DE69911186D1/de
Publication of DE69911186T2 publication Critical patent/DE69911186T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/19Fluorine; Hydrogen fluoride
    • C01B7/191Hydrogen fluoride
    • C01B7/195Separation; Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/23Preparation of halogenated hydrocarbons by dehalogenation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/38Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/08Acyclic saturated compounds containing halogen atoms containing fluorine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/08Acyclic saturated compounds containing halogen atoms containing fluorine
    • C07C19/10Acyclic saturated compounds containing halogen atoms containing fluorine and chlorine
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE69911186T 1998-04-03 1999-04-01 Verfahren zur reinigung und verwendung von 2-chloro-1,1,1,2,3,3,3-heptafluorpropan und ihre azeotrope mit hf Expired - Fee Related DE69911186T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US8070998P 1998-04-03 1998-04-03
US80709P 1998-04-03
PCT/US1999/007225 WO1999051555A1 (en) 1998-04-03 1999-04-01 Processes for the purification and use of 2-chloro-1,1,1,2,3,3,3-heptafluoropropane and azeotropes thereof with hf

Publications (2)

Publication Number Publication Date
DE69911186D1 true DE69911186D1 (de) 2003-10-16
DE69911186T2 DE69911186T2 (de) 2004-07-15

Family

ID=22159113

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69911186T Expired - Fee Related DE69911186T2 (de) 1998-04-03 1999-04-01 Verfahren zur reinigung und verwendung von 2-chloro-1,1,1,2,3,3,3-heptafluorpropan und ihre azeotrope mit hf

Country Status (7)

Country Link
US (1) US6677493B1 (de)
EP (1) EP1066230B1 (de)
JP (1) JP2002510664A (de)
AU (1) AU3377999A (de)
DE (1) DE69911186T2 (de)
ES (1) ES2203107T3 (de)
WO (1) WO1999051555A1 (de)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002510665A (ja) * 1998-04-03 2002-04-09 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー 2,2−ジクロロ−1,1,1,3,3,3−ヘキサフルオロプロパンの精製および使用方法
JP2002544248A (ja) * 1999-05-18 2002-12-24 イネオス フラウアー ホールデイングス リミテッド 1,1,1,2,3,3,3−ヘプタフルオロプロパンの製造
US20050177012A1 (en) * 2001-07-20 2005-08-11 Pcbu Services, Inc. Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
US20030028057A1 (en) * 2001-07-20 2003-02-06 Stephen Owens Methods and materials for the preparation and purification of halogenated hydrocarbons
US7329786B2 (en) * 2001-09-28 2008-02-12 Great Lakes Chemical Corporation Processes for producing CF3CFHCF3
CN1279007C (zh) 2002-08-22 2006-10-11 纳幕尔杜邦公司 制备2-氯-1,1,1,2,3,3,3-七氟丙烷,六氟丙烯和1,1,1,2,3,3,3-七氟丙烷的方法
US20050020863A1 (en) * 2003-07-25 2005-01-27 Honeywell International Inc. Method of making fluorinated propanes
US7423188B2 (en) * 2005-11-01 2008-09-09 E. I. Du Pont De Nemours And Company Azeotrope compositions comprising E-1,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof
US20070106099A1 (en) * 2005-11-10 2007-05-10 Pcbu Services, Inc. Production processes and systems
US8436218B2 (en) 2010-05-27 2013-05-07 Honeywell International Inc. Azeotrope-like composition of hexafluoropropane, hexafluoropropene and hydrogen fluoride
US9309116B2 (en) * 2011-09-26 2016-04-12 Honeywell International Inc. Method for producing high concentration aqueous HF solutions

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4911792A (en) 1988-08-01 1990-03-27 E. I. Du Pont De Nemours And Company Process for the separation of HF via phase separation and distillation
US5364992A (en) 1989-10-10 1994-11-15 E. I. Du Pont De Nemours And Company Halocarbon hydrogenolysis
US5057634A (en) 1989-12-19 1991-10-15 E. I. Du Pont De Nemours And Company Multistep synthesis of hexafluoropropylene
US5068472A (en) 1989-12-19 1991-11-26 E. I. Du Pont De Nemours And Company Multistep synthesis of hexafluoropropylene
US5430206A (en) * 1990-11-20 1995-07-04 E. I. Du Pont De Nemours And Company Method for purifying dichloropentafluoropropanes
EP0665203B1 (de) 1991-04-15 1996-09-11 Daikin Industries, Ltd. Verfahren zur Reinigung von 1,1,1-Trifluoro-2-Chlorethan
JP3175286B2 (ja) * 1991-04-15 2001-06-11 ダイキン工業株式会社 フッ化水素と1,1,1−トリフルオロ−2−クロロエタンの共沸混合物および1,1,1−トリフルオロ−2−クロロエタンの精製方法
FR2675496B1 (fr) 1991-04-17 1993-09-03 Atochem Procede de separation du fluorure d'hydrogene de ses melanges avec le 1,1,1-trifluoro-2-chloroethane.
US5276225A (en) 1991-04-17 1994-01-04 Elf Atochem S.A. Process for separating hydrogen fluoride from its mixtures with 1,1,1-trifluoro-2-chloroethane
SG44743A1 (en) * 1991-11-01 1997-12-19 Solvay Process for the preparation of 1,1,1,2,3,3,3,-heptafluoropropane (R 227)
CA2082844A1 (en) 1991-11-15 1993-05-16 Wolfgang Dukat Process for the separation of a mixture containing hydrogen fluoride and 1-chloro-2,2,2-trifluoroethane
DE69426837T2 (de) * 1993-12-22 2001-07-19 Daikin Ind Ltd Verfahren zur reinigung von 1,1,1,3,3-pentafluoro-2,3-dichloropropan
US5481051A (en) * 1994-12-08 1996-01-02 E. I. Du Pont De Nemours And Company 2,2-dichlorohexafluoropropane hydrogenolysis
US6291729B1 (en) 1994-12-08 2001-09-18 E. I. Du Pont De Nemours And Company Halofluorocarbon hydrogenolysis

Also Published As

Publication number Publication date
DE69911186T2 (de) 2004-07-15
JP2002510664A (ja) 2002-04-09
US6677493B1 (en) 2004-01-13
EP1066230A1 (de) 2001-01-10
EP1066230B1 (de) 2003-09-10
WO1999051555A1 (en) 1999-10-14
AU3377999A (en) 1999-10-25
ES2203107T3 (es) 2004-04-01

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee