DE69707283T2 - Verfahren zur zusammenfügung von werkstoffteilen auf basis von siliciumcarbid mit hilfe einer dicken verbindungsschicht durch feuerfeste hartlötung und so erhaltener verbund - Google Patents

Verfahren zur zusammenfügung von werkstoffteilen auf basis von siliciumcarbid mit hilfe einer dicken verbindungsschicht durch feuerfeste hartlötung und so erhaltener verbund

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Publication number
DE69707283T2
DE69707283T2 DE1997607283 DE69707283T DE69707283T2 DE 69707283 T2 DE69707283 T2 DE 69707283T2 DE 1997607283 DE1997607283 DE 1997607283 DE 69707283 T DE69707283 T DE 69707283T DE 69707283 T2 DE69707283 T2 DE 69707283T2
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Prior art keywords
fire
aid
composite
assembly
solution
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Expired - Lifetime
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DE1997607283
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English (en)
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DE69707283D1 (de
Inventor
Adrien Gasse
Gisele Coing-Boyat
Gerard Bourgeois
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Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
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Commissariat a lEnergie Atomique CEA
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Publication of DE69707283T2 publication Critical patent/DE69707283T2/de
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Expired - Lifetime legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B37/00Joining burned ceramic articles with other burned ceramic articles or other articles by heating
    • C04B37/003Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts
    • C04B37/006Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts consisting of metals or metal salts
    • CCHEMISTRY; METALLURGY
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    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/62645Thermal treatment of powders or mixtures thereof other than sintering
    • C04B35/62665Flame, plasma or melting treatment
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    • C04B37/00Joining burned ceramic articles with other burned ceramic articles or other articles by heating
    • C04B37/003Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts
    • C04B37/005Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts consisting of glass or ceramic material
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52Constituents or additives characterised by their shapes
    • C04B2235/5208Fibers
    • C04B2235/5216Inorganic
    • C04B2235/524Non-oxidic, e.g. borides, carbides, silicides or nitrides
    • C04B2235/5244Silicon carbide
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5436Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
    • CCHEMISTRY; METALLURGY
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6565Cooling rate
    • CCHEMISTRY; METALLURGY
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567Treatment time
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/658Atmosphere during thermal treatment
    • C04B2235/6581Total pressure below 1 atmosphere, e.g. vacuum
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    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/02Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
    • C04B2237/04Ceramic interlayers
    • C04B2237/08Non-oxidic interlayers
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    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/02Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
    • C04B2237/12Metallic interlayers
    • C04B2237/126Metallic interlayers wherein the active component for bonding is not the largest fraction of the interlayer
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    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/02Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
    • C04B2237/16Silicon interlayers
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    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/30Composition of layers of ceramic laminates or of ceramic or metallic articles to be joined by heating, e.g. Si substrates
    • C04B2237/32Ceramic
    • C04B2237/36Non-oxidic
    • C04B2237/365Silicon carbide
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    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/30Composition of layers of ceramic laminates or of ceramic or metallic articles to be joined by heating, e.g. Si substrates
    • C04B2237/32Ceramic
    • C04B2237/38Fiber or whisker reinforced
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    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/50Processing aspects relating to ceramic laminates or to the joining of ceramic articles with other articles by heating
    • C04B2237/52Pre-treatment of the joining surfaces, e.g. cleaning, machining
    • CCHEMISTRY; METALLURGY
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    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/50Processing aspects relating to ceramic laminates or to the joining of ceramic articles with other articles by heating
    • C04B2237/52Pre-treatment of the joining surfaces, e.g. cleaning, machining
    • C04B2237/525Pre-treatment of the joining surfaces, e.g. cleaning, machining by heating
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/12All metal or with adjacent metals
    • Y10T428/12493Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/31504Composite [nonstructural laminate]
    • Y10T428/31678Of metal

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Plasma & Fusion (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Products (AREA)
DE1997607283 1996-06-12 1997-06-11 Verfahren zur zusammenfügung von werkstoffteilen auf basis von siliciumcarbid mit hilfe einer dicken verbindungsschicht durch feuerfeste hartlötung und so erhaltener verbund Expired - Lifetime DE69707283T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9607291A FR2749787B1 (fr) 1996-06-12 1996-06-12 Procede d'assemblage a l'aide d'un joint epais de pieces en materiaux a base de sic par brasage refractaire et joint refractaire et epais ainsi obtenu
PCT/FR1997/001042 WO1997047568A1 (fr) 1996-06-12 1997-06-11 Procede d'assemblage a l'aide d'un joint epais de pieces en materiaux a base de carbure de silicium par brasage refractaire et joint refractaire epais ainsi obtenu

Publications (2)

Publication Number Publication Date
DE69707283D1 DE69707283D1 (de) 2001-11-15
DE69707283T2 true DE69707283T2 (de) 2002-07-11

Family

ID=9492978

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1997607283 Expired - Lifetime DE69707283T2 (de) 1996-06-12 1997-06-11 Verfahren zur zusammenfügung von werkstoffteilen auf basis von siliciumcarbid mit hilfe einer dicken verbindungsschicht durch feuerfeste hartlötung und so erhaltener verbund

Country Status (8)

Country Link
US (2) US5975407A (de)
EP (1) EP0904256B1 (de)
JP (1) JP2000511867A (de)
CA (1) CA2257677C (de)
DE (1) DE69707283T2 (de)
FR (1) FR2749787B1 (de)
TW (1) TW336187B (de)
WO (1) WO1997047568A1 (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102018117738A1 (de) 2018-07-23 2020-01-23 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Reaktionsgefügte keramische Bauteile und Verfahren zu ihrer Herstellung

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DE19959292A1 (de) * 1999-12-09 2001-06-13 Rolls Royce Deutschland Verfahren zum Herstellen einer Brennkammer eines Gasturbinen-Triebwerks
FR2806405B1 (fr) * 2000-03-14 2002-10-11 Commissariat Energie Atomique Procede d'assemblage de pieces en materiaux a base de sic par brasage refractaire non reactif, composition de brasure, et joint et assemblage refractaires obtenus par ce procede
US6974070B2 (en) * 2001-08-07 2005-12-13 University Of Chicago Joining of advanced materials by superplastic deformation
US6774073B2 (en) * 2002-07-29 2004-08-10 Coorstek, Inc. Graphite loaded silicon carbide and methods for making
FR2850649B1 (fr) * 2003-01-30 2005-04-29 Snecma Propulsion Solide Procede pour le traitement de surface d'une piece en materiau composite thermostructural et application au brasage de pieces en materiau composite thermostructural
FR2850742B1 (fr) 2003-01-30 2005-09-23 Snecma Propulsion Solide Panneau de refroidissement actif en materiau composite thermostructural et procede pour sa fabrication
US7022198B2 (en) * 2003-03-07 2006-04-04 The United States Of America As Represented By The Secretary Of The Navy Microwave assisted reactive brazing of ceramic materials
FR2872072B1 (fr) 2004-06-24 2006-09-29 Snecma Propulsion Solide Sa Procede de brasage de pieces en materiau composite thermostructural siliciure
FR2906242B1 (fr) 2006-09-27 2009-01-16 Commissariat Energie Atomique Procede d'assemblage de pieces en ceramique refractaire par frittage a chaud avec champ electrique pulse ("sps")
FR2913145B1 (fr) * 2007-02-22 2009-05-15 Stmicroelectronics Crolles Sas Assemblage de deux parties de circuit electronique integre
FR2935376B1 (fr) * 2008-09-01 2011-06-10 Commissariat Energie Atomique Procede d'assemblage moyennement refractaire de pieces en materiaux a base de sic par brasage non reactif sous atmosphere oxydante, compositions de brasure, et joint et assemblage obtenus par ce procede.
FR2936176B1 (fr) 2008-09-22 2011-06-03 Commissariat Energie Atomique Procede d'assemblage moyennement refractaire de pieces en materiaux a base de sic par brasage non reactif, compositions de brasure, et joint et assemblage obtenus par ce procede
FR2949696B1 (fr) 2009-09-08 2012-01-13 Commissariat Energie Atomique Procede d'assemblage de pieces en materiaux a base de sic par brasage non-reactif, compositions de brasure, et joint et assemblage obtenus par ce procede.
FR2957542B1 (fr) 2010-03-16 2012-05-11 Commissariat Energie Atomique Procede d'assemblage de pieces en materiaux a base de sic par brasage non-reactif, compositions de brasure, et joint et assemblage obtenus par ce procede.
FR2957544B1 (fr) 2010-03-16 2012-05-11 Commissariat Energie Atomique Procede d'assemblage de pieces en materiaux a base de sic par brasage non-reactif avec ajout d'un renfort, compositions de brasure, et joint et assemblage obtenus par ce procede.
FR2957543B1 (fr) 2010-03-16 2012-07-27 Commissariat Energie Atomique Procede d'assemblage de pieces en materiaux a base de sic par brasage non-reactif, compositions de brasure, et joint et assemblage obtenus par ce procede.
FR2984784B1 (fr) 2011-12-22 2014-09-26 Commissariat Energie Atomique Procede d'assemblage de pieces en materiaux a base de sic par brasage non reactif sous atmosphere oxydante. compositions de brasure, et joint et assemblage obtenus par ce procede.
FR2984781B1 (fr) * 2011-12-22 2014-01-24 Commissariat Energie Atomique Procede d'assemblage par brasage d'un substrat comprenant du pyrocarbone avec des pieces comprenant du pyrocarbone.
FR2993495B1 (fr) 2012-07-18 2014-08-22 Herakles Procede de brasage de pieces en materiau composite avec integration d'un pion dans la liaison
FR2993494B1 (fr) 2012-07-18 2014-08-22 Herakles Procede de brasage de pieces en materiau composite avec ancrage du joint de brasure
FR2996478B1 (fr) 2012-10-09 2015-04-24 Commissariat Energie Atomique Procede de brasage de pieces en materiau a base de carbure de silicium avec serrage de maintien
FR2996550B1 (fr) 2012-10-09 2016-01-29 Herakles Procede de traitement local d'une piece en materiau composite poreux
WO2014149094A1 (en) 2013-03-15 2014-09-25 Xu Raymond R Braze materials and method for joining of ceramic matrix composites
US9455053B2 (en) 2013-09-16 2016-09-27 Westinghouse Electric Company Llc SiC matrix fuel cladding tube with spark plasma sintered end plugs
US10364195B2 (en) 2014-07-28 2019-07-30 Rolls-Royce Corporation Braze for ceramic and ceramic matrix composite components
US10335877B2 (en) 2015-01-21 2019-07-02 Rolls-Royce Corporation Multilayer braze tape
US10293424B2 (en) 2015-05-05 2019-05-21 Rolls-Royce Corporation Braze for ceramic and ceramic matrix composite components
JP6750678B2 (ja) * 2016-06-13 2020-09-02 株式会社Ihi セラミックス基複合材料部品及びその製造方法
US10947162B2 (en) 2017-04-13 2021-03-16 Rolls-Royce Corporation Braze alloys for joining or repairing ceramic matrix composite (CMC) components
US11110692B2 (en) 2017-10-03 2021-09-07 Rolls-Royce Corporation Braze material for ceramic matrix composite articles
FR3084077B1 (fr) * 2018-07-20 2021-01-22 Commissariat Energie Atomique Procede d'assemblage hybride de pieces en ceramique ou en composite a matrice ceramique a l'aide d'un materiau d'apport depose puis chauffe sans fusion totale de ce materiau d'apport
US11884597B2 (en) 2022-06-28 2024-01-30 General Electric Company Methods for joining ceramic components to form unitary ceramic components

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US3813759A (en) * 1971-09-09 1974-06-04 English Electric Co Ltd Method of brazing
DE3230320C2 (de) * 1982-08-14 1985-05-30 Dornier System Gmbh, 7990 Friedrichshafen Lot zum Verbinden von Siliziumcarbidwerkstoffen
ATE36131T1 (de) * 1983-09-26 1988-08-15 Gte Prod Corp Duktile niedrigschmelzende hartloetlegierung.
JPH0791610B2 (ja) * 1985-06-17 1995-10-04 日本電装株式会社 非酸化物セラミックヒータ用金属ロー材
FR2707196B1 (fr) * 1993-07-07 1995-08-11 Commissariat Energie Atomique Procédé d'assemblage de molybdène ou de tungstène avec eux-mêmes ou des céramiques contenant du silicium, par brasage.
US5447683A (en) * 1993-11-08 1995-09-05 General Atomics Braze for silicon carbide bodies
US5683028A (en) * 1996-05-03 1997-11-04 Cvd, Incorporated Bonding of silicon carbide components

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102018117738A1 (de) 2018-07-23 2020-01-23 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Reaktionsgefügte keramische Bauteile und Verfahren zu ihrer Herstellung
EP3599229A1 (de) 2018-07-23 2020-01-29 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Reaktionsgefügte keramische bauteile und verfahren zu ihrer herstellung

Also Published As

Publication number Publication date
CA2257677C (fr) 2005-08-09
US6221499B1 (en) 2001-04-24
EP0904256B1 (de) 2001-10-10
FR2749787A1 (fr) 1997-12-19
US5975407A (en) 1999-11-02
TW336187B (en) 1998-07-11
EP0904256A1 (de) 1999-03-31
FR2749787B1 (fr) 1998-07-24
JP2000511867A (ja) 2000-09-12
CA2257677A1 (fr) 1997-12-18
DE69707283D1 (de) 2001-11-15
WO1997047568A1 (fr) 1997-12-18

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