DE69405199D1 - Verfahren und Anlage zur kryogenischen Reinigung von Wasserstoff - Google Patents

Verfahren und Anlage zur kryogenischen Reinigung von Wasserstoff

Info

Publication number
DE69405199D1
DE69405199D1 DE69405199T DE69405199T DE69405199D1 DE 69405199 D1 DE69405199 D1 DE 69405199D1 DE 69405199 T DE69405199 T DE 69405199T DE 69405199 T DE69405199 T DE 69405199T DE 69405199 D1 DE69405199 D1 DE 69405199D1
Authority
DE
Germany
Prior art keywords
plant
hydrogen
cryogenic purification
cryogenic
purification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69405199T
Other languages
English (en)
Other versions
DE69405199T2 (de
Inventor
Catherine Denis
Pierre Gauthier
Jean-Claude Villard
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Publication of DE69405199D1 publication Critical patent/DE69405199D1/de
Application granted granted Critical
Publication of DE69405199T2 publication Critical patent/DE69405199T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
    • F25J3/0695—Start-up or control of the process; Details of the apparatus used
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/506—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification at low temperatures
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
    • F25J3/0605—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the feed stream
    • F25J3/062—Refinery gas, cracking gas, coke oven gas, gaseous mixtures containing aliphatic unsaturated CnHm or gaseous mixtures of undefined nature
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
    • F25J3/063—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream
    • F25J3/0655—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation characterised by the separated product stream separation of hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/046—Purification by cryogenic separation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/048—Composition of the impurity the impurity being an organic compound
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00—Processes or apparatus involving steps for expanding of process streams
    • F25J2240/02—Expansion of a process fluid in a work-extracting turbine (i.e. isentropic expansion), e.g. of the feed stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/04—Internal refrigeration with work-producing gas expansion loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00—Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/42—Modularity, pre-fabrication of modules, assembling and erection, horizontal layout, i.e. plot plan, and vertical arrangement of parts of the cryogenic unit, e.g. of the cold box
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00—Refrigeration
    • Y10S62/902—Apparatus
    • Y10S62/91—Expander
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00—Refrigeration
    • Y10S62/931—Recovery of hydrogen
    • Y10S62/932—From natural gas
DE69405199T 1993-10-26 1994-10-10 Verfahren und Anlage zur kryogenischen Reinigung von Wasserstoff Expired - Fee Related DE69405199T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9312730A FR2711779B1 (fr) 1993-10-26 1993-10-26 Procédé et installation de purification cryogénique d'hydrogène.

Publications (2)

Publication Number Publication Date
DE69405199D1 true DE69405199D1 (de) 1997-10-02
DE69405199T2 DE69405199T2 (de) 1998-01-22

Family

ID=9452202

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69405199T Expired - Fee Related DE69405199T2 (de) 1993-10-26 1994-10-10 Verfahren und Anlage zur kryogenischen Reinigung von Wasserstoff

Country Status (6)

Country Link
US (1) US5511382A (de)
EP (1) EP0655596B1 (de)
CN (1) CN1038494C (de)
CA (1) CA2134173A1 (de)
DE (1) DE69405199T2 (de)
FR (1) FR2711779B1 (de)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2315014C (en) * 1997-12-16 2007-06-19 Lockheed Martin Idaho Technologies Company Apparatus and process for the refrigeration, liquefaction and separation of gases with varying levels of purity
US6668582B2 (en) * 2001-04-20 2003-12-30 American Air Liquide Apparatus and methods for low pressure cryogenic cooling
US20070137246A1 (en) * 2001-05-04 2007-06-21 Battelle Energy Alliance, Llc Systems and methods for delivering hydrogen and separation of hydrogen from a carrier medium
US6581409B2 (en) 2001-05-04 2003-06-24 Bechtel Bwxt Idaho, Llc Apparatus for the liquefaction of natural gas and methods related to same
US7591150B2 (en) * 2001-05-04 2009-09-22 Battelle Energy Alliance, Llc Apparatus for the liquefaction of natural gas and methods relating to same
US7219512B1 (en) 2001-05-04 2007-05-22 Battelle Energy Alliance, Llc Apparatus for the liquefaction of natural gas and methods relating to same
US7637122B2 (en) 2001-05-04 2009-12-29 Battelle Energy Alliance, Llc Apparatus for the liquefaction of a gas and methods relating to same
US7594414B2 (en) * 2001-05-04 2009-09-29 Battelle Energy Alliance, Llc Apparatus for the liquefaction of natural gas and methods relating to same
FR2860576A1 (fr) * 2003-10-01 2005-04-08 Air Liquide Appareil et procede de separation d'un melange gazeux par distillation cryogenique
FR2914990B1 (fr) * 2007-04-13 2010-02-26 Air Liquide Procede de mise en froid d'une ligne d'echange cryogenique.
US7491856B2 (en) 2007-06-27 2009-02-17 H R D Corporation Method of making alkylene glycols
US7749481B2 (en) * 2007-06-27 2010-07-06 H R D Corporation System and process for gas sweetening
US8304584B2 (en) 2007-06-27 2012-11-06 H R D Corporation Method of making alkylene glycols
US9217603B2 (en) 2007-09-13 2015-12-22 Battelle Energy Alliance, Llc Heat exchanger and related methods
US9574713B2 (en) 2007-09-13 2017-02-21 Battelle Energy Alliance, Llc Vaporization chambers and associated methods
US9254448B2 (en) 2007-09-13 2016-02-09 Battelle Energy Alliance, Llc Sublimation systems and associated methods
US8899074B2 (en) 2009-10-22 2014-12-02 Battelle Energy Alliance, Llc Methods of natural gas liquefaction and natural gas liquefaction plants utilizing multiple and varying gas streams
US8061413B2 (en) 2007-09-13 2011-11-22 Battelle Energy Alliance, Llc Heat exchangers comprising at least one porous member positioned within a casing
US8555672B2 (en) * 2009-10-22 2013-10-15 Battelle Energy Alliance, Llc Complete liquefaction methods and apparatus
US20090145167A1 (en) * 2007-12-06 2009-06-11 Battelle Energy Alliance, Llc Methods, apparatuses and systems for processing fluid streams having multiple constituents
US10655911B2 (en) 2012-06-20 2020-05-19 Battelle Energy Alliance, Llc Natural gas liquefaction employing independent refrigerant path
JP6416193B2 (ja) 2013-03-15 2018-10-31 セラニーズ・インターナショナル・コーポレーション カルボニル化法を用いて合成ガスを分離する方法
US9150475B2 (en) 2013-11-08 2015-10-06 Celanese International Corporation Process for producing ethanol by hydrogenation with carbon monoxide controls

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3038318A (en) * 1957-06-07 1962-06-12 Sulzer Ag Expansion turbine and turbocompressor connected therewith in a cold producing plant
US3105631A (en) * 1961-08-15 1963-10-01 Sulzer Ag Expansion turbine having a gas bearing
GB1057020A (en) * 1964-12-17 1967-02-01 Petrocarbon Dev Ltd Recovery of hydrogen from a gas mixture
FR1546283A (fr) * 1966-12-05 1968-11-15 Saia Ag Dispositif de contrôle pour machines travaillant périodiquement
US3553972A (en) * 1968-11-19 1971-01-12 American Messer Corp Cryogenic recovery of hydrogen from ammonia synthesis gas
GB1304568A (de) * 1970-08-13 1973-01-24
US4217759A (en) * 1979-03-28 1980-08-19 Union Carbide Corporation Cryogenic process for separating synthesis gas
FR2546283B1 (fr) * 1983-05-16 1985-09-06 Air Liquide Procede et installation de concentration d'hydrogene
FR2557586B1 (fr) * 1983-12-30 1986-05-02 Air Liquide Procede et installation de recuperation des hydrocarbures les plus lourds d'un melange gazeux
US4619679A (en) * 1984-10-29 1986-10-28 Phillips Petroleum Company Gas processing

Also Published As

Publication number Publication date
DE69405199T2 (de) 1998-01-22
CN1038494C (zh) 1998-05-27
CA2134173A1 (fr) 1995-04-27
US5511382A (en) 1996-04-30
EP0655596B1 (de) 1997-08-27
FR2711779B1 (fr) 1995-12-08
FR2711779A1 (fr) 1995-05-05
CN1107801A (zh) 1995-09-06
EP0655596A1 (de) 1995-05-31

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee