DE69000747T2 - Kryogenisches rektifikationsverfahren zur herstellung von ultrahoch reinem stickstoff. - Google Patents
Kryogenisches rektifikationsverfahren zur herstellung von ultrahoch reinem stickstoff.Info
- Publication number
- DE69000747T2 DE69000747T2 DE9090104908T DE69000747T DE69000747T2 DE 69000747 T2 DE69000747 T2 DE 69000747T2 DE 9090104908 T DE9090104908 T DE 9090104908T DE 69000747 T DE69000747 T DE 69000747T DE 69000747 T2 DE69000747 T2 DE 69000747T2
- Authority
- DE
- Germany
- Prior art keywords
- pure nitrogen
- high pure
- rectification process
- cryogenic rectification
- producing ultra
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
- F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
- F25J3/04084—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of nitrogen
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
- F25J3/0443—A main column system not otherwise provided, e.g. a modified double column flowsheet
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2200/00—Processes or apparatus using separation by rectification
- F25J2200/72—Refluxing the column with at least a part of the totally condensed overhead gas
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2215/00—Processes characterised by the type or other details of the product stream
- F25J2215/42—Nitrogen or special cases, e.g. multiple or low purity N2
- F25J2215/44—Ultra high purity nitrogen, i.e. generally less than 1 ppb impurities
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
- F25J2235/42—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being nitrogen
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2245/00—Processes or apparatus involving steps for recycling of process streams
- F25J2245/42—Processes or apparatus involving steps for recycling of process streams the recycled stream being nitrogen
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2250/00—Details related to the use of reboiler-condensers
- F25J2250/30—External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
- F25J2250/42—One fluid being nitrogen
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2270/00—Refrigeration techniques used
- F25J2270/02—Internal refrigeration with liquid vaporising loop
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/324,444 US4902321A (en) | 1989-03-16 | 1989-03-16 | Cryogenic rectification process for producing ultra high purity nitrogen |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69000747D1 DE69000747D1 (de) | 1993-02-25 |
DE69000747T2 true DE69000747T2 (de) | 1993-05-27 |
Family
ID=23263617
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE9090104908T Expired - Fee Related DE69000747T2 (de) | 1989-03-16 | 1990-03-15 | Kryogenisches rektifikationsverfahren zur herstellung von ultrahoch reinem stickstoff. |
Country Status (7)
Country | Link |
---|---|
US (1) | US4902321A (de) |
EP (1) | EP0387872B1 (de) |
JP (1) | JPH02282684A (de) |
BR (1) | BR9001249A (de) |
CA (1) | CA2012217C (de) |
DE (1) | DE69000747T2 (de) |
ES (1) | ES2041065T3 (de) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5205127A (en) * | 1990-08-06 | 1993-04-27 | Air Products And Chemicals, Inc. | Cryogenic process for producing ultra high purity nitrogen |
US5137559A (en) * | 1990-08-06 | 1992-08-11 | Air Products And Chemicals, Inc. | Production of nitrogen free of light impurities |
US5123947A (en) * | 1991-01-03 | 1992-06-23 | Air Products And Chemicals, Inc. | Cryogenic process for the separation of air to produce ultra high purity nitrogen |
US5170630A (en) * | 1991-06-24 | 1992-12-15 | The Boc Group, Inc. | Process and apparatus for producing nitrogen of ultra-high purity |
JP2983393B2 (ja) * | 1991-10-15 | 1999-11-29 | レール・リキード・ソシエテ・アノニム・プール・レテュード・エ・レクスプロワタシオン・デ・プロセデ・ジョルジュ・クロード | 高純度窒素の製造における極低温蒸留により水素を除去する方法 |
US5218825A (en) * | 1991-11-15 | 1993-06-15 | Air Products And Chemicals, Inc. | Coproduction of a normal purity and ultra high purity volatile component from a multi-component stream |
US5289688A (en) * | 1991-11-15 | 1994-03-01 | Air Products And Chemicals, Inc. | Inter-column heat integration for multi-column distillation system |
US5195324A (en) * | 1992-03-19 | 1993-03-23 | Prazair Technology, Inc. | Cryogenic rectification system for producing nitrogen and ultra high purity oxygen |
FR2694383B1 (fr) * | 1992-07-29 | 1994-09-16 | Air Liquide | Production et installation de production d'azote gazeux à plusieurs puretés différentes. |
US5419137A (en) * | 1993-08-16 | 1995-05-30 | The Boc Group, Inc. | Air separation process and apparatus for the production of high purity nitrogen |
US5385024A (en) * | 1993-09-29 | 1995-01-31 | Praxair Technology, Inc. | Cryogenic rectification system with improved recovery |
US5511380A (en) | 1994-09-12 | 1996-04-30 | Liquid Air Engineering Corporation | High purity nitrogen production and installation |
US5983667A (en) * | 1997-10-31 | 1999-11-16 | Praxair Technology, Inc. | Cryogenic system for producing ultra-high purity nitrogen |
US5918482A (en) * | 1998-02-17 | 1999-07-06 | Praxair Technology, Inc. | Cryogenic rectification system for producing ultra-high purity nitrogen and ultra-high purity oxygen |
US5906113A (en) * | 1998-04-08 | 1999-05-25 | Praxair Technology, Inc. | Serial column cryogenic rectification system for producing high purity nitrogen |
US7981195B2 (en) * | 2007-11-09 | 2011-07-19 | Praxair Technology, Inc. | System for preventing contaminants from reaching a gas purifier |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3210947A (en) * | 1961-04-03 | 1965-10-12 | Union Carbide Corp | Process for purifying gaseous streams by rectification |
JPS5241754A (en) * | 1975-09-29 | 1977-03-31 | Aisin Seiki Co Ltd | Clutch construction |
JPS5644577A (en) * | 1979-09-19 | 1981-04-23 | Hitachi Ltd | Method of sampling pressurized nitrogen for air separator |
US4416677A (en) * | 1982-05-25 | 1983-11-22 | Union Carbide Corporation | Split shelf vapor air separation process |
US4566887A (en) * | 1982-09-15 | 1986-01-28 | Costain Petrocarbon Limited | Production of pure nitrogen |
GB2129115B (en) * | 1982-10-27 | 1986-03-12 | Air Prod & Chem | Producing gaseous nitrogen |
EP0279500B2 (de) * | 1983-03-08 | 1998-11-04 | Daido Hoxan Inc. | Sehr reiner Stickstoffgaserzeugungsapparat |
DE3476114D1 (en) * | 1983-03-08 | 1989-02-16 | Daido Oxygen | Apparatus for producing high-purity nitrogen gas |
JPS61110872A (ja) * | 1984-11-02 | 1986-05-29 | 日本酸素株式会社 | 窒素製造方法 |
US4594085A (en) * | 1984-11-15 | 1986-06-10 | Union Carbide Corporation | Hybrid nitrogen generator with auxiliary reboiler drive |
JPH0627621B2 (ja) * | 1986-11-19 | 1994-04-13 | 株式会社日立製作所 | 高純度窒素ガス製造装置 |
US4755202A (en) * | 1987-07-28 | 1988-07-05 | Union Carbide Corporation | Process and apparatus to produce ultra high purity oxygen from a gaseous feed |
-
1989
- 1989-03-16 US US07/324,444 patent/US4902321A/en not_active Expired - Fee Related
-
1990
- 1990-03-15 ES ES199090104908T patent/ES2041065T3/es not_active Expired - Lifetime
- 1990-03-15 BR BR909001249A patent/BR9001249A/pt not_active IP Right Cessation
- 1990-03-15 DE DE9090104908T patent/DE69000747T2/de not_active Expired - Fee Related
- 1990-03-15 CA CA002012217A patent/CA2012217C/en not_active Expired - Fee Related
- 1990-03-15 JP JP2062862A patent/JPH02282684A/ja active Pending
- 1990-03-15 EP EP90104908A patent/EP0387872B1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP0387872A2 (de) | 1990-09-19 |
CA2012217C (en) | 1993-12-14 |
ES2041065T3 (es) | 1993-11-01 |
EP0387872A3 (en) | 1990-11-07 |
JPH02282684A (ja) | 1990-11-20 |
BR9001249A (pt) | 1991-03-26 |
DE69000747D1 (de) | 1993-02-25 |
EP0387872B1 (de) | 1993-01-13 |
CA2012217A1 (en) | 1990-09-16 |
US4902321A (en) | 1990-02-20 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |