DE6097C - Process and apparatus for the digestion of guano and phosphate - Google Patents
Process and apparatus for the digestion of guano and phosphateInfo
- Publication number
- DE6097C DE6097C DENDAT6097D DE6097DA DE6097C DE 6097 C DE6097 C DE 6097C DE NDAT6097 D DENDAT6097 D DE NDAT6097D DE 6097D A DE6097D A DE 6097DA DE 6097 C DE6097 C DE 6097C
- Authority
- DE
- Germany
- Prior art keywords
- phosphate
- acid
- guano
- flour
- container
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000002515 guano Substances 0.000 title claims description 6
- 238000000034 method Methods 0.000 title claims description 4
- 230000029087 digestion Effects 0.000 title claims description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K [O-]P([O-])([O-])=O Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 title description 12
- 239000010452 phosphate Substances 0.000 title description 12
- 235000021317 phosphate Nutrition 0.000 claims 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
- 239000002253 acid Substances 0.000 description 14
- 235000013312 flour Nutrition 0.000 description 11
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000000875 corresponding Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000779 smoke Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- GGZZISOUXJHYOY-UHFFFAOYSA-N 8-amino-4-hydroxynaphthalene-2-sulfonic acid Chemical compound C1=C(S(O)(=O)=O)C=C2C(N)=CC=CC2=C1O GGZZISOUXJHYOY-UHFFFAOYSA-N 0.000 description 1
- 210000000003 Hoof Anatomy 0.000 description 1
- YYRMJZQKEFZXMX-UHFFFAOYSA-N calcium;phosphoric acid Chemical compound [Ca+2].OP(O)(O)=O.OP(O)(O)=O YYRMJZQKEFZXMX-UHFFFAOYSA-N 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000002349 favourable Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000001105 regulatory Effects 0.000 description 1
- 239000002965 rope Substances 0.000 description 1
- 239000002426 superphosphate Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/10—Apparatus for the manufacture of superphosphates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crushing And Pulverization Processes (AREA)
Description
1878.1878.
Klasse 16.Class 16.
AUG. BEHNE in HARBURG λ. d. Elbe. Verfahren und Apparat zur Aufschliersung von Guano und Phosphityy AUG. BEHNE in HARBURG λ. d. Elbe. Method and apparatus for dispersing guano and phosphityy
Patentirt im Deutschen Reiche vom io. December 1878 ab.Patented in the German Empire by the io. December 1878.
In der Zeichnung bedeuten die Buchstaben:In the drawing the letters mean:
A Guano- und Phosphatmehlbehälter, A guano and phosphate flour containers,
B Schwefelsäurebehälter, B sulfuric acid tank,
C Arbeitskufe, C work skids,
D Speisewalze, D feed roller,
E Klappe oder Schott zur Regulirung der Austrittsöffnung für das Phosphatmehl, E flap or bulkhead to regulate the outlet opening for the phosphate meal,
F Abflufshahn für die Säure, F drain cock for the acid,
G Kästen für einen siebartigen Austritt der Säure, G boxes for a sieve-like discharge of the acid,
H Abflufshähne des Säurestrahls, H drain cocks for the acid jet,
J Schwimmer des Phosphatmehlbehälters. J Float in the phosphate flour container.
i Schnur, i cord,
K Schnurscheibe für Schwimmer J1 K rope washer for swimmers J 1
L . . L Schnurscheibe für den Säurebehälter, L. . L washer for the acid tank,
M Säurestandsglas, M acid glass,
N Säurestandszeiger, N acid level indicator,
O Welle/ O wave /
P. . P Schlageisen und Transportirarme, P. P hitting iron and transport arms,
Q Wagen zur Aufnahme des aufgeschlossenen Phosphatmehls, Q trolley for receiving the digested phosphate meal,
Ji Schornstein oder Qualmfang zur Abführung der gesundheitsgefährlichen Dämpfe während des Aufschliefsens, Ji chimney or smoke trap to remove harmful vapors while sleeping,
.S Hebel zur Regulirung der Hahnstellung des Hahnes F, .S Lever for regulating the cock position of cock F,
V Mischraum vor Eintritt in C. V Mixing room before entering C.
Das neue Arbeitsverfahren für den Aufschlufs von Guanophosphaten besteht in dem Zusammenwirken der durch Zeichnung t und Beschreibung dargestellten Apparate in der Weise, dafs ein der Breite der Arbeitskufe durch Schott und Speisewalze zugeflihrtes Band Guano oder Phosphatmehl von einem, dem Mischungsverhältnifs entsprechenden, gleich breiten Strahl Schwefelsäure vor Eintritt in die Arbeitskufe derart getroffen wird, dafs bei der raschen energischen Verbindung beider Substanzen die Verarbeitung dieser gleichmäfsig zugeführten Masse in einem mit entsprechenden Schlageisen und Transportirarmen versehenen Apparat in günstigster Weise geschieht und die Abführung der den Arbeitern gesundheitsschädlichen Dämpfe gleichzeitig bewirkt ist. The new working method for the breakdown of guanophosphates consists in the interaction of the apparatus shown in the drawing and description in such a way that a band of guano or phosphate flour, fed to the width of the working vat through the bulkhead and feed roller, of a stream of sulfuric acid of equal width corresponding to the mixing ratio Before entering the work vat, it is made in such a way that with the rapid energetic combination of the two substances, the processing of this uniformly supplied mass in an apparatus provided with appropriate hammer and transport arms takes place in the most favorable manner and the removal of the vapors harmful to the workers is effected at the same time.
Der Gang des Arbeitsverfahrens ist folgender:The course of the working procedure is as follows:
Man füllt den Behälter A vollständig mit Guano oder Phosphatmehl, dessen Gewicht genau bestimmt wurde; ebenso füllt man Behälter B mit der Quantität Schwefelsäure, die •zum Aufschliefsen jenes Phosphatmehls erforderlich ist.The container A is completely filled with guano or phosphate flour, the weight of which has been precisely determined; in the same way, container B is filled with the quantity of sulfuric acid that is required to break up that phosphate flour.
Beim Austritt beider Substanzen (Mehl und Säure) findet die Mischung im Räume V in der Weise statt, dafs das austretende Mehlband in seiner ganzen Breite von einem gleich breiten Säureband getroffen wird.When both substances emerge (flour and acid), the mixture in space V takes place in such a way that the whole width of the emerging ribbon of flour is hit by an acid ribbon of equal width.
Damit aber das Mischungsverhältnifs zwischen beiden Materialien in jeder Zeitdauer des Austritts ein richtiges ist, mufs die Entleerung des Säurebehälters B proportional dem Austritt des Phosphatmehls sein, so dafs bei vollständiger Entleerung des Phosphatbehälters A die vollständige Entleerung des Säurebehälters B eingetreten ist. Dieser Anforderung genügt man dadurch, dafs man den AbHufs bezw. den Zutritt der Säure zum austretenden Mehle durch ein entsprechendes Oeffncn oder Schliefsen des Abflufshahnes F in der Weise bewirkt, dafs das Sinken des Säurestandes im Glase M dem Gange des Zeigers N entspricht.However, so that the mixing ratio between the two materials is correct in every period of time of the discharge, the emptying of the acid container B must be proportional to the discharge of the phosphate flour, so that when the phosphate container A is completely emptied, the acid container B has been completely emptied. This requirement is satisfied by the fact that the hoof or the access of the acid to the emerging flour is effected by opening or closing the drain cock F in such a way that the drop in the acid level in the glass M corresponds to the movement of the pointer N.
Damit aber der Gang des Zeigers N proportional dem Mehlgange ist, ertheilt eine durch Schwimmer J und Schnur / mit dem Phosphatbehälter A in Verbindung gebrachte Scheibe A', deren Abwicklung (Peripherie) gleich der Füllungshöhe des Behälters A ist, einer der Füllungshöhe des Säurebehälters B in ihrer Abwickelung gleiche Scheibe L durch ihre gemeinschaftliche Welle O eine Drehung, welche mittelst Schnur auf jenen Zeiger übertragen, den proportionalen Entleerungsgrad beider Behälter in jedem Stadium richtig anzeigt.But so that the rate of the pointer N is proportional to the flour course, a disk A 'connected to the phosphate container A by a float J and string /, the development (periphery) of which is equal to the filling height of the container A , gives one of the filling height of the acid container B. In its development, the same disk L, through its common shaft O, has a rotation which, by means of a cord, is transmitted to the pointer and correctly indicates the proportional degree of emptying of both containers at every stage.
Für die verschiedenen Füllungsgrade des Säurebehälters sind diesen entsprechende Schnurscheiben von verschiedenen Durchmessern angeordnet. For the various degrees of filling of the acid container, these are corresponding cord washers arranged of different diameters.
Das so durch richtigen Säurezufliifs zum rationellen Aufschlufs vorbereitete Phosphatmehl tritt nun unter gleichmäfsiger Zuführung in die Arbeitskufe C, wird hier durch Schlageisen undThe phosphate flour, prepared in this way by the correct addition of acid to the rational digestion, now enters the working vat C, which is fed in evenly, and is here by means of iron and
Transportirarme /'. . Γ energisch gemischt und vollständig aufgeschlossen dem Wagen Q zugeführt, welcher das gewonnene Superphosphat zum Transport nach dem Lagerräume aufnimmt. Die sich während des Aufschliefsens entwickelnden gesundheitsschädlichen Dämpfe werden durch den Schornstein bezw. Qualmfang R fortgeführt.Transportirearms / '. . Γ energetically mixed and completely unlocked, fed to the wagon Q , which picks up the superphosphate obtained for transport to the storage rooms. The harmful vapors that develop during the opening process are released through the chimney and / or. Smoke trap R continued.
Claims (1)
Das durch Zeichnung und Beschreibung dargestellte Arbeitsverfahren des Aufschliefsens von Guano und Phosphaten, unter Anwendung des hierfür beschriebenen, in seinem Zusammenhange neu und eigentümlichen Gesammtapparates. Patent claim: & t / *, f ~
The working process of the digestion of guano and phosphates, represented by drawing and description, using the overall apparatus described for this purpose, which is new and peculiar in its context.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE6097C true DE6097C (en) |
Family
ID=284347
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT6097D Active DE6097C (en) | Process and apparatus for the digestion of guano and phosphate |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE6097C (en) |
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0
- DE DENDAT6097D patent/DE6097C/en active Active
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