DE60034084D1 - Verfahren zur Reinigung eines Gases durch Adsorption - Google Patents

Verfahren zur Reinigung eines Gases durch Adsorption

Info

Publication number
DE60034084D1
DE60034084D1 DE60034084T DE60034084T DE60034084D1 DE 60034084 D1 DE60034084 D1 DE 60034084D1 DE 60034084 T DE60034084 T DE 60034084T DE 60034084 T DE60034084 T DE 60034084T DE 60034084 D1 DE60034084 D1 DE 60034084D1
Authority
DE
Germany
Prior art keywords
gas
adsorber
flow
cycle
depressurisation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60034084T
Other languages
English (en)
Other versions
DE60034084T2 (de
Inventor
Christian Monereau
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA a Directoire et Conseil de Surveillance pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA a Directoire et Conseil de Surveillance pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Publication of DE60034084D1 publication Critical patent/DE60034084D1/de
Application granted granted Critical
Publication of DE60034084T2 publication Critical patent/DE60034084T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40028—Depressurization
    • B01D2259/40032—Depressurization with three sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40043—Purging
    • B01D2259/4005—Nature of purge gas
    • B01D2259/40052—Recycled product or process gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/403—Further details for adsorption processes and devices using three beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/053—Pressure swing adsorption with storage or buffer vessel
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C01B2203/043—Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
DE60034084T 1999-01-29 2000-01-05 Verfahren zur Reinigung eines Gases durch Adsorption Expired - Lifetime DE60034084T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9901035 1999-01-29
FR9901035A FR2788993B1 (fr) 1999-01-29 1999-01-29 Procede d'epuration d'un gaz par adsorption

Publications (2)

Publication Number Publication Date
DE60034084D1 true DE60034084D1 (de) 2007-05-10
DE60034084T2 DE60034084T2 (de) 2007-12-06

Family

ID=9541388

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60034084T Expired - Lifetime DE60034084T2 (de) 1999-01-29 2000-01-05 Verfahren zur Reinigung eines Gases durch Adsorption

Country Status (8)

Country Link
US (1) US6315818B1 (de)
EP (1) EP1023934B1 (de)
AT (1) ATE357961T1 (de)
CA (1) CA2294842C (de)
DE (1) DE60034084T2 (de)
ES (1) ES2284457T3 (de)
FR (1) FR2788993B1 (de)
PT (1) PT1023934E (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110252083A (zh) * 2019-06-27 2019-09-20 天津大沽化工股份有限公司 一种pvc生产中合成尾气变压吸附方法

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2825291A1 (fr) * 2001-06-01 2002-12-06 Air Liquide Procede de traitement d'un gaz par adsortion et installation de mise en oeuvre du procede
FR2833183B1 (fr) * 2001-12-12 2004-01-23 Air Liquide Procede de traitement par adsorption d'un melange gazeux, et installation de production de monoxyde de carbone comportant une unite de traitement de mise en oeuvre d'un tel procede
FR2835932B1 (fr) * 2002-02-13 2004-03-19 Air Liquide Procede de commande d'une installation de traitement d'un gaz par adsorption et installation de traitement correspondante
FR2836062A1 (fr) * 2002-02-15 2003-08-22 Air Liquide Procede de production d'hydrogene a partir d'un gaz de charge riche en hydrogene et unite de mise en oeuvre de ce procede
FR2836060B1 (fr) * 2002-02-15 2004-11-19 Air Liquide Procede et unite de production d'hydrogene a partir d'un gaz de charge riche en hydrogene
FR2841152B1 (fr) * 2002-06-19 2005-02-11 Air Liquide Procede de traitement d'au moins un gaz de charge par adsorption a modulation de pression
FR2841153B1 (fr) * 2002-06-21 2004-07-23 Air Liquide Procede de regulation d'une unite de traitement, par adsorption a modulation de pression, d'au moins un gaz de charge
JP2004066125A (ja) * 2002-08-07 2004-03-04 Sumitomo Seika Chem Co Ltd 目的ガスの分離方法
US6887301B2 (en) * 2003-06-04 2005-05-03 H2Gen Innovations, Inc. Flow control in pressure swing adsorption systems
US7179324B2 (en) * 2004-05-19 2007-02-20 Praxair Technology, Inc. Continuous feed three-bed pressure swing adsorption system
FR2889459B1 (fr) 2005-08-08 2007-09-14 Air Liquide Procede de separation dans une unite psa d'au moins un melange gazeux
FR2892322A1 (fr) * 2005-10-24 2007-04-27 Air Liquide Procede psa h2 avec elution additionnelle
US7651549B2 (en) * 2006-06-13 2010-01-26 Air Products And Chemicals, Inc. Pressure swing adsorption process with improved recovery of high-purity product
FR2909570A1 (fr) * 2006-12-08 2008-06-13 Air Liquide Procede de production d'hydrogene a partir d'un gaz riche en hydrogene
US7862645B2 (en) 2008-02-01 2011-01-04 Air Products And Chemicals, Inc. Removal of gaseous contaminants from argon
FR2933313B1 (fr) 2008-07-03 2011-07-22 Air Liquide Traitement de gaz humide contenant des poussieres
FR2937258B1 (fr) 2008-10-21 2011-05-20 Air Liquide Repressurisation d'un vsa traitant un melange gazeux comprenant un combustible
FR2952553B1 (fr) * 2009-11-19 2012-06-01 Air Liquide Procede de purification d'un flux gazeux mettant en oeuvre un contacteur a passages paralleles presentant une conservation de ses performances
FR2967083A1 (fr) * 2010-11-04 2012-05-11 Air Liquide Procede de purification d'un flux gazeux mettant en œuvre un contacteur a passages paralleles dans un cycle psa super-rapide
US8496733B2 (en) 2011-01-11 2013-07-30 Praxair Technology, Inc. Large scale pressure swing adsorption systems having process cycles operating in normal and turndown modes
US8491704B2 (en) 2011-01-11 2013-07-23 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8551217B2 (en) 2011-01-11 2013-10-08 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8435328B2 (en) 2011-01-11 2013-05-07 Praxair Technology, Inc. Ten bed pressure swing adsorption process operating in normal and turndown modes
RU2486943C1 (ru) * 2011-12-30 2013-07-10 Виталий Леонидович Бондаренко Способ обогащения неоногелиевой смеси и установка для его реализации
NL2010072C2 (en) * 2012-12-28 2014-07-03 Green Vision Holding B V Method and device for separating a gas mixture by means of pressure swing adsorption.
US9216364B2 (en) * 2013-03-15 2015-12-22 Air Products And Chemicals, Inc. Onsite ultra high purity chemicals or gas purification
FR3013605B1 (fr) 2013-11-28 2017-05-26 Air Liquide Procede psa avec une etape active par temps de phase
CN103787285B (zh) * 2014-01-16 2015-10-28 新疆独山子天利高新技术股份有限公司 五塔变压吸附制氮装置
FR3046550B1 (fr) * 2016-01-13 2020-02-21 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Psa h2 avec modification du flux gazeux d'alimentation
CN111545014A (zh) * 2020-05-13 2020-08-18 北京中科富海低温科技有限公司杭州分公司 一种变压吸附脱除氢气中氩的方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3703068A (en) * 1971-03-26 1972-11-21 Union Carbide Corp Control system for selective adsorption process
FR2363362A1 (fr) * 1976-09-07 1978-03-31 Air Liquide Procede de traitement, par adsorption, d'un melange gazeux
DE2923325A1 (de) * 1979-06-08 1980-12-11 Linde Ag Zyklisches adsorptionsverfahren zum zerlegen eines gasgemisches
JPS6261616A (ja) * 1985-09-11 1987-03-18 Nippon Steel Corp 混合ガスから高純度ガスを分離する方法
US4693730A (en) * 1986-07-24 1987-09-15 Union Carbide Corporation Pressure swing adsorption product purity control method and apparatus
US4705541A (en) * 1987-02-12 1987-11-10 Air Products And Chemicals, Inc. Production of mixed gases of controlled composition by pressure swing adsorption
US4761165A (en) * 1987-09-01 1988-08-02 Union Carbide Corporation Pressure swing adsorption control method and apparatus
US4915711A (en) * 1989-05-18 1990-04-10 Air Products And Chemicals, Inc. Adsorptive process for producing two gas streams from a gas mixture
FR2682611B1 (fr) * 1991-10-17 1993-12-03 Air Liquide Procede et installation d'epuration d'un gaz par adsorption.
US5232473A (en) * 1992-05-07 1993-08-03 The Boc Group, Inc. Pressure swing adsorption with countercurrent feed pressurization
US5354346A (en) * 1992-10-01 1994-10-11 Air Products And Chemicals, Inc. Purge effluent repressurized adsorption process
US5248322A (en) * 1992-10-01 1993-09-28 Air Products And Chemicals, Inc. Depressurization effluent repressurized adsorption process
US5542966A (en) * 1994-10-21 1996-08-06 Nitrotec Corporation Helium recovery
US5536300A (en) * 1994-10-21 1996-07-16 Nitrotec Corporation Natural gas enrichment process
US5529607A (en) * 1995-03-15 1996-06-25 The Boc Group, Inc. PSA process with dynamic purge control
FR2761616B1 (fr) * 1997-04-02 1999-05-07 Air Liquide Procede et installation de separation d'un melange gazeux par adsorption
FR2765810B1 (fr) * 1997-07-09 1999-08-13 Air Liquide Procede de separation d'un melange gazeux par adsorption a variation de pression

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110252083A (zh) * 2019-06-27 2019-09-20 天津大沽化工股份有限公司 一种pvc生产中合成尾气变压吸附方法
CN110252083B (zh) * 2019-06-27 2022-05-20 天津大沽化工股份有限公司 一种pvc生产中合成尾气变压吸附方法

Also Published As

Publication number Publication date
PT1023934E (pt) 2007-06-29
EP1023934B1 (de) 2007-03-28
ATE357961T1 (de) 2007-04-15
US6315818B1 (en) 2001-11-13
CA2294842A1 (fr) 2000-07-29
FR2788993B1 (fr) 2001-02-23
EP1023934A1 (de) 2000-08-02
FR2788993A1 (fr) 2000-08-04
ES2284457T3 (es) 2007-11-16
DE60034084T2 (de) 2007-12-06
CA2294842C (fr) 2008-03-25

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