DE60031245D1 - Membran auf basis von silizium selektiert gegenüber wasserstoff - Google Patents

Membran auf basis von silizium selektiert gegenüber wasserstoff

Info

Publication number
DE60031245D1
DE60031245D1 DE60031245T DE60031245T DE60031245D1 DE 60031245 D1 DE60031245 D1 DE 60031245D1 DE 60031245 T DE60031245 T DE 60031245T DE 60031245 T DE60031245 T DE 60031245T DE 60031245 D1 DE60031245 D1 DE 60031245D1
Authority
DE
Germany
Prior art keywords
membrane
vycor
modified
diaphragnetically
silicon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60031245T
Other languages
English (en)
Inventor
Ted Oyama
K Prabhu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Virginia Tech Intellectual Properties Inc
Original Assignee
Virginia Tech Intellectual Properties Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Virginia Tech Intellectual Properties Inc filed Critical Virginia Tech Intellectual Properties Inc
Application granted granted Critical
Publication of DE60031245D1 publication Critical patent/DE60031245D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D67/00Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039Inorganic membrane manufacture
    • B01D67/0072Inorganic membrane manufacture by deposition from the gaseous phase, e.g. sputtering, CVD, PVD
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • B01D53/228Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion characterised by specific membranes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D67/00Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039Inorganic membrane manufacture
    • B01D67/0044Inorganic membrane manufacture by chemical reaction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D71/00Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02Inorganic material
    • B01D71/024Oxides
    • B01D71/027Silicium oxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/501Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by diffusion
    • C01B3/503Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by diffusion characterised by the membrane
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2323/00Details relating to membrane preparation
    • B01D2323/08Specific temperatures applied
    • B01D2323/081Heating
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0405Purification by membrane separation
    • C01B2203/041In-situ membrane purification during hydrogen production
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/047Composition of the impurity the impurity being carbon monoxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0475Composition of the impurity the impurity being carbon dioxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/048Composition of the impurity the impurity being an organic compound
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0495Composition of the impurity the impurity being water
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02CCAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00Capture or disposal of greenhouse gases
    • Y02C20/20Capture or disposal of greenhouse gases of methane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Combustion & Propulsion (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Silicon Compounds (AREA)
DE60031245T 1999-02-02 2000-01-31 Membran auf basis von silizium selektiert gegenüber wasserstoff Expired - Lifetime DE60031245D1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11843399P 1999-02-02 1999-02-02
PCT/US2000/002075 WO2000045940A1 (en) 1999-02-02 2000-01-31 Hydrogen-selective silica based membrane

Publications (1)

Publication Number Publication Date
DE60031245D1 true DE60031245D1 (de) 2006-11-23

Family

ID=22378555

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60031245T Expired - Lifetime DE60031245D1 (de) 1999-02-02 2000-01-31 Membran auf basis von silizium selektiert gegenüber wasserstoff

Country Status (7)

Country Link
US (1) US6527833B1 (de)
EP (1) EP1154836B1 (de)
AT (1) ATE342119T1 (de)
AU (1) AU766490B2 (de)
CA (1) CA2361504A1 (de)
DE (1) DE60031245D1 (de)
WO (1) WO2000045940A1 (de)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6488838B1 (en) 1999-08-17 2002-12-03 Battelle Memorial Institute Chemical reactor and method for gas phase reactant catalytic reactions
GB0106478D0 (en) * 2001-03-16 2001-05-02 Univ Robert Gordon Apparatus and method
US6508862B1 (en) 2001-04-30 2003-01-21 Battelle Memorial Institute Apparatus and methods for separation/purification utilizing rapidly cycled thermal swing sorption
US6630012B2 (en) 2001-04-30 2003-10-07 Battelle Memorial Institute Method for thermal swing adsorption and thermally-enhanced pressure swing adsorption
US6503298B1 (en) 2001-04-30 2003-01-07 Battelle Memorial Institute Apparatus and methods for hydrogen separation/purification utilizing rapidly cycled thermal swing sorption
DE60231134D1 (de) * 2001-09-17 2009-03-26 Ngk Insulators Ltd Verfahren zur herstellung von zeolith-folie deca-dodecasil 3r, zeolith-folie deca-dodecasil 3r und verbund-zeolith-folie deca-dodecasil 3r sowie herstellungsverfahren dafür
US6854602B2 (en) * 2002-06-04 2005-02-15 Conocophillips Company Hydrogen-selective silica-based membrane
FR2850588B1 (fr) * 2003-01-31 2007-08-03 Inst Francais Du Petrole Membrane inorganique poreuse contenant du carbone, son procede de preparation et son utilisation
EP2527046A1 (de) * 2003-07-29 2012-11-28 Intelligent Energy, Inc. Dünne Wasserstofftrennmembranen und zugehörige Verwendungen
US7179325B2 (en) * 2004-02-10 2007-02-20 Virginia Tech Intellectual Properties, Inc. Hydrogen-selective silica-based membrane
US20060013759A1 (en) * 2004-07-13 2006-01-19 Conocophillips Company Systems and methods for hydrogen production
US7494533B2 (en) * 2005-12-29 2009-02-24 American Air Liquide, Inc. Systems for purifying gases having organic impurities using granulated porous glass
US7524359B2 (en) * 2005-12-29 2009-04-28 American Air Liquide, Inc. Methods for purifying gases having organic impurities using granulated porous glass
US7585356B2 (en) * 2006-05-01 2009-09-08 Virginia Tech Intellectual Properties, Inc. Hydrothermally-stable silica-based composite membranes for hydrogen separation
US7497110B2 (en) * 2007-02-28 2009-03-03 Varian, Inc. Methods and apparatus for test gas leak detection
US20080202210A1 (en) * 2007-02-28 2008-08-28 Varian, Inc. Test gas leak detection using a composite membrane
US20080256913A1 (en) * 2007-04-17 2008-10-23 Giacobbe Frederick W Systems for purifying a gas mixture comprising two gases using granulated porous glass
US20080257152A1 (en) * 2007-04-17 2008-10-23 Giacobbe Frederick W Methods of purifying a gas mixture comprising two gases using granulated porous glass
US7938894B2 (en) * 2008-02-14 2011-05-10 Conocophillips Company Hybrid organic-inorganic gas separation membranes
EP2103586A1 (de) 2008-03-20 2009-09-23 Bp Oil International Limited Verfahren zur Umwandlung von Methan in Ethan in einem Reaktor mit Membran
GR20080100438A (el) 2008-06-27 2010-01-27 Μεθοδος χημικης διεισδυσης ατμων χαμηλης θερμοκρασιας, για την τροποποιηση του μεγεθους των πορων και την επιδιορθωση ατελειων σε μικροπορωδεις και νανοπορωδεις μεμβρανες
US8273152B2 (en) * 2008-11-14 2012-09-25 Praxair Technology, Inc. Separation method and apparatus
DE102009026869A1 (de) 2009-06-09 2011-02-03 Schott Ag Membran aus porösem Glas, Verfahren zu deren Herstellung und Verwendung derselben
US9126151B2 (en) * 2009-12-11 2015-09-08 Sumitomo Electric Industries, Ltd. Silica-based hydrogen separation material and manufacturing method therefor, as well as hydrogen separation module and hydrogen production apparatus having the same
US8900344B2 (en) * 2010-03-22 2014-12-02 T3 Scientific Llc Hydrogen selective protective coating, coated article and method
US20160222511A1 (en) * 2015-01-29 2016-08-04 Flosfia Inc. Apparatus and method for forming film
JP6478103B2 (ja) * 2015-01-29 2019-03-06 株式会社Flosfia 成膜装置および成膜方法
JP2018159699A (ja) * 2017-03-23 2018-10-11 株式会社住化分析センター 水素ガス中の不純物の濃縮キット、水素ガス中の不純物の濃縮方法、及び水素ガスの品質管理方法
CN108187507B (zh) * 2017-12-22 2021-05-28 中国矿业大学(北京) 一种表面改性的反应性电化学膜及其制备方法
DE102018101446A1 (de) 2018-01-23 2018-03-08 Agilent Technologies Inc. Helium-selektive Membran, Verfahren zu deren Herstellung und diese enthaltender Helium-Sensor und Helium-Leck-Detektor

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4482360A (en) * 1982-05-29 1984-11-13 Nippon Steel Corporation Porous materials for concentration and separation of hydrogen or helium, and process therewith for the separation of the gas
US4689150A (en) * 1985-03-07 1987-08-25 Ngk Insulators, Ltd. Separation membrane and process for manufacturing the same
JPS61238303A (ja) * 1985-04-15 1986-10-23 Mitsubishi Heavy Ind Ltd 微細多孔質膜の製造方法
US4902307A (en) * 1988-11-18 1990-02-20 California Institute Of Technology Synthesis of SiO2 membrane on porous support and method of use of same
US5453298A (en) * 1990-11-08 1995-09-26 California Institute Of Technology Method for forming H2-permselective oxide membranes
DE4117284A1 (de) * 1991-05-27 1992-12-03 Studiengesellschaft Kohle Mbh Verfahren zur herstellung von mikroporoesen keramikmembranen fuer die trennung von gas- und fluessigkeitsgemischen
US5487774A (en) * 1993-11-08 1996-01-30 Wisconsin Alumni Research Foundation Gas phase fractionation method using porous ceramic membrane
US5415891A (en) * 1994-01-10 1995-05-16 Media And Process Technology Inc. Method for forming metal-oxide-modified porous ceramic membranes
JP3373057B2 (ja) * 1994-07-29 2003-02-04 エヌオーケー株式会社 水素分離膜の製造法
US5772735A (en) * 1995-11-02 1998-06-30 University Of New Mexico Supported inorganic membranes
US5789024A (en) * 1996-05-15 1998-08-04 New Jersey Institute Of Technology Subnanoscale composite, N2-permselective membrane for the separation of volatile organic compounds
US6152986A (en) * 1999-07-07 2000-11-28 Ppg Industries Ohio, Inc. Method of enriching chlorine gas

Also Published As

Publication number Publication date
CA2361504A1 (en) 2000-08-10
ATE342119T1 (de) 2006-11-15
AU766490B2 (en) 2003-10-16
WO2000045940A1 (en) 2000-08-10
EP1154836A1 (de) 2001-11-21
EP1154836A4 (de) 2002-08-28
EP1154836B1 (de) 2006-10-11
US6527833B1 (en) 2003-03-04
AU3474300A (en) 2000-08-25

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8332 No legal effect for de