DE59208196D1 - METHOD FOR THE PRODUCTION OF DETERGENTS WITH A HIGH BULK WEIGHT AND IMPROVED SOLUTION SPEED - Google Patents
METHOD FOR THE PRODUCTION OF DETERGENTS WITH A HIGH BULK WEIGHT AND IMPROVED SOLUTION SPEEDInfo
- Publication number
- DE59208196D1 DE59208196D1 DE59208196T DE59208196T DE59208196D1 DE 59208196 D1 DE59208196 D1 DE 59208196D1 DE 59208196 T DE59208196 T DE 59208196T DE 59208196 T DE59208196 T DE 59208196T DE 59208196 D1 DE59208196 D1 DE 59208196D1
- Authority
- DE
- Germany
- Prior art keywords
- liquid
- production
- solid
- poly
- breaker
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
- C11D17/065—High-density particulate detergent compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
Abstract
The invention concerns the production of high-bulk-density solid washing and cleaning agents with improved dissolving speed, produced by mixing solid and liquid washing-agent raw materials and, at the same time or subsequently, modifying the form of the particles in the mixture and, if required, drying it. Anionic surfactants, builders and alkalisation agents are added as the solid components, and non-anionic surfactants as the liquid components. To improve the dissolution behaviour and to facilitate mixing, the liquid non-ionic surfactants are used intimately mixed with a structure breaker in the ratio by wt. of non-ionic surfactant: structure-breaker of 10:1 to 1:2. Preferred structure-breakers are poly(ethylene glycol) or poly(propylene glycol) with a relative molecular weight between 200 and 12,000, addition products produced by reacting about 20 to 80 moles of ethylene oxide with 1 mole of an aliphatic alcohol with substantially 8 to 20 carbon atoms, and mixtures thereof.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE59208196T DE59208196D1 (en) | 1991-07-25 | 1992-07-16 | METHOD FOR THE PRODUCTION OF DETERGENTS WITH A HIGH BULK WEIGHT AND IMPROVED SOLUTION SPEED |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4124701A DE4124701A1 (en) | 1991-07-25 | 1991-07-25 | METHOD FOR THE PRODUCTION OF SOLID DETERGENT AND CLEANING AGENT WITH HIGH SHOCK WEIGHT AND IMPROVED SOLUTION SPEED |
PCT/EP1992/001616 WO1993002176A1 (en) | 1991-07-25 | 1992-07-16 | Method of producing high-bulk-density washing agents with improved dissolving speed |
DE59208196T DE59208196D1 (en) | 1991-07-25 | 1992-07-16 | METHOD FOR THE PRODUCTION OF DETERGENTS WITH A HIGH BULK WEIGHT AND IMPROVED SOLUTION SPEED |
Publications (1)
Publication Number | Publication Date |
---|---|
DE59208196D1 true DE59208196D1 (en) | 1997-04-17 |
Family
ID=6437010
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE4124701A Ceased DE4124701A1 (en) | 1991-07-25 | 1991-07-25 | METHOD FOR THE PRODUCTION OF SOLID DETERGENT AND CLEANING AGENT WITH HIGH SHOCK WEIGHT AND IMPROVED SOLUTION SPEED |
DE59208196T Expired - Fee Related DE59208196D1 (en) | 1991-07-25 | 1992-07-16 | METHOD FOR THE PRODUCTION OF DETERGENTS WITH A HIGH BULK WEIGHT AND IMPROVED SOLUTION SPEED |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE4124701A Ceased DE4124701A1 (en) | 1991-07-25 | 1991-07-25 | METHOD FOR THE PRODUCTION OF SOLID DETERGENT AND CLEANING AGENT WITH HIGH SHOCK WEIGHT AND IMPROVED SOLUTION SPEED |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP0595946B1 (en) |
JP (1) | JPH06509369A (en) |
AT (1) | ATE150084T1 (en) |
DE (2) | DE4124701A1 (en) |
ES (1) | ES2098520T3 (en) |
WO (1) | WO1993002176A1 (en) |
Families Citing this family (47)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0660873B2 (en) † | 1992-09-01 | 2006-05-31 | The Procter & Gamble Company | High density granular detergent composition |
GB9300311D0 (en) * | 1993-01-08 | 1993-03-03 | Unilever Plc | Detergent powders and process for preparing them |
DE4303176C2 (en) * | 1993-02-04 | 1997-07-31 | Henkel Kgaa | Solid washing, rinsing and cleaning agents |
DE4303211C2 (en) * | 1993-02-04 | 1996-05-15 | Henkel Kgaa | Anionic surfactants with improved solubility |
DE4303448A1 (en) * | 1993-02-05 | 1994-08-11 | Henkel Kgaa | Builder for detergents or cleaners |
DE4319666A1 (en) * | 1993-06-14 | 1994-12-15 | Henkel Kgaa | Process for the production of solid washing or cleaning agents with high bulk density and improved rheology |
DE4325500A1 (en) * | 1993-07-29 | 1995-02-02 | Henkel Kgaa | Process for the production of extrudates that are active in washing or cleaning |
US5733862A (en) * | 1993-08-27 | 1998-03-31 | The Procter & Gamble Company | Process for making a high density detergent composition from a sufactant paste containing a non-aqueous binder |
DE4403323A1 (en) * | 1993-09-23 | 1995-08-10 | Henkel Kgaa | Extruded washing or cleaning agents with improved dissolving properties |
WO1995023221A1 (en) | 1994-02-24 | 1995-08-31 | Cognis, Inc. | Improved enzymes and detergents containing them |
ES2364776T3 (en) | 1994-02-24 | 2011-09-14 | HENKEL AG & CO. KGAA | IMPROVED AND DETERGENT ENZYMES THAT CONTAIN THEM. |
DE4415369C1 (en) * | 1994-05-02 | 1995-08-31 | Henkel Kgaa | Heterogeneous surfactant granulate useful in washing powder and detergent |
DE4415362A1 (en) * | 1994-05-02 | 1995-11-09 | Henkel Kgaa | Process for the production of silicate builder granules with increased bulk density |
DE19501269A1 (en) | 1995-01-18 | 1996-07-25 | Henkel Kgaa | Amorphous alkali silicate compound |
DE19525378A1 (en) * | 1995-07-12 | 1997-01-16 | Henkel Kgaa | Amorphous alkali silicate compound |
DE19533790A1 (en) * | 1995-09-13 | 1997-03-20 | Henkel Kgaa | Process for the preparation of an amorphous alkali silicate with impregnation |
DE19620364A1 (en) * | 1996-05-22 | 1997-11-27 | Basf Ag | Use of at least trihydric alcohols and their alkoxylation products to increase the dissolution rate of particulate detergent formulations in water |
DE19624415A1 (en) * | 1996-06-19 | 1998-01-02 | Henkel Kgaa | Process for the production of solid washing or cleaning agents |
DE19624416A1 (en) * | 1996-06-19 | 1998-01-02 | Henkel Kgaa | Process for the production of solid washing or cleaning agents |
DE19638599A1 (en) * | 1996-09-20 | 1998-03-26 | Henkel Kgaa | Process for producing a particulate detergent or cleaning agent |
ES2162337T3 (en) * | 1996-11-18 | 2001-12-16 | Basf Ag | POLIVALENT ALCOHOLS AND THEIR ALCOXYLATE PRODUCTS IN WASHING AGENTS IN THE FORM OF PARTICLES FOR INCREASING THE DISSOLUTION SPEED. |
DE19648014C2 (en) * | 1996-11-20 | 2002-09-19 | Cognis Deutschland Gmbh | Anhydrous surfactant mixtures |
EP1012221B1 (en) * | 1997-09-11 | 2004-06-16 | Henkel Kommanditgesellschaft auf Aktien | Method for producing particulate detergents |
DE19850223A1 (en) | 1998-10-31 | 2000-05-04 | Clariant Gmbh | Detergents and cleaning agents containing alkoxylated fatty acid alkyl esters |
EP1186650A4 (en) | 1999-06-16 | 2004-07-21 | Kao Corp | Article for use in washing in sheet form |
US6610752B1 (en) | 1999-10-09 | 2003-08-26 | Cognis Deutschland Gmbh | Defoamer granules and processes for producing the same |
DE19953792A1 (en) | 1999-11-09 | 2001-05-17 | Cognis Deutschland Gmbh | Detergent tablets |
DE19956802A1 (en) | 1999-11-25 | 2001-06-13 | Cognis Deutschland Gmbh | Detergent tablets |
DE19962883A1 (en) | 1999-12-24 | 2001-07-12 | Cognis Deutschland Gmbh | Detergent tablets |
DE10013763A1 (en) * | 2000-03-20 | 2001-10-18 | Henkel Kgaa | Fragrance alcohol alkoxylates used in laundry and other detergents and cosmetics, have ethoxy and propoxy groups and specified film pressure at critical micelle formation concentration |
DE10031619A1 (en) | 2000-06-29 | 2002-01-10 | Cognis Deutschland Gmbh | Surfactant granules with an improved dissolution rate |
DE10044471A1 (en) | 2000-09-08 | 2002-03-21 | Cognis Deutschland Gmbh | Fabric-conditioning detergent composition comprising an anionic surfactant, a nonionic and amphoteric surfactant, a cationic polymer and a phosphate |
DE10044472A1 (en) | 2000-09-08 | 2002-03-21 | Cognis Deutschland Gmbh | laundry detergent |
GB2367830A (en) * | 2000-10-12 | 2002-04-17 | Procter & Gamble | Process for preparing tablets |
GB0030671D0 (en) | 2000-12-15 | 2001-01-31 | Unilever Plc | Detergent compositions |
GB0030669D0 (en) | 2000-12-15 | 2001-01-31 | Unilever Plc | Detergent compositions |
DE10137925A1 (en) | 2001-08-07 | 2003-02-20 | Cognis Deutschland Gmbh | Mixtures for improving hard surface wettability especially in machine dish washing comprise Gemini surfactant and polyethylene glycol |
GB0124307D0 (en) | 2001-10-10 | 2001-11-28 | Unilever Plc | Detergent compositions |
GB0124308D0 (en) | 2001-10-10 | 2001-11-28 | Unilever Plc | Detergent compositions |
DE10242222A1 (en) * | 2002-09-12 | 2004-03-25 | Henkel Kgaa | Mechanically compacted washing or detergent agents containing neutralizable organic polycarboxylic acids are given improved odor values by having specific non-water-soluble builder content and pH |
DE60325504D1 (en) | 2002-11-04 | 2009-02-05 | Unilever Nv | LAUNDRY DETERGENT |
EP1690922A1 (en) * | 2005-02-11 | 2006-08-16 | The Procter & Gamble Company | A solid laundry detergent composition |
DE102006021553A1 (en) * | 2006-02-08 | 2007-08-16 | Henkel Kgaa | fluid reservoir |
JP2009084525A (en) * | 2007-10-03 | 2009-04-23 | Kao Corp | Detergent composition |
US9228157B2 (en) | 2009-04-24 | 2016-01-05 | Conopco, Inc. | Manufacture of high active detergent particles |
DE102015002877A1 (en) | 2015-03-09 | 2016-09-15 | Henkel Ag & Co. Kgaa | Granular detergent or cleaner with improved dissolution rate |
JP7095864B2 (en) * | 2018-04-27 | 2022-07-05 | 株式会社ニイタカ | Manufacturing method of tablet cleaning agent for coffee machines and tablet cleaning agent for coffee machines |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3849327A (en) * | 1971-11-30 | 1974-11-19 | Colgate Palmolive Co | Manufacture of free-flowing particulate heavy duty synthetic detergent composition containing nonionic detergent and anti-redeposition agent |
US3925224A (en) * | 1973-04-17 | 1975-12-09 | Church & Dwight Co Inc | Detergent additive composition |
CA1293421C (en) * | 1985-07-09 | 1991-12-24 | Mark Edward Cushman | Spray-dried granular detergent compositions containing nonionicsurfactant, polyethylene glycol, and polyacrylate |
DE3812530A1 (en) * | 1988-04-15 | 1989-10-26 | Henkel Kgaa | PROCESS FOR INCREASING THE DENSITY OF SPREADY DRY, PHOSPHATE-REDUCED DETERGENT |
CA2017922C (en) * | 1989-06-09 | 1995-07-11 | Frank Joseph Mueller | Formation of discrete, high active detergent granules using a continuous neutralization system |
ATE107352T1 (en) * | 1989-08-09 | 1994-07-15 | Henkel Kgaa | PRODUCTION OF COMPACT GRANULES FOR DETERGENT. |
-
1991
- 1991-07-25 DE DE4124701A patent/DE4124701A1/en not_active Ceased
-
1992
- 1992-07-16 DE DE59208196T patent/DE59208196D1/en not_active Expired - Fee Related
- 1992-07-16 WO PCT/EP1992/001616 patent/WO1993002176A1/en active IP Right Grant
- 1992-07-16 EP EP92916049A patent/EP0595946B1/en not_active Expired - Lifetime
- 1992-07-16 JP JP5502585A patent/JPH06509369A/en active Pending
- 1992-07-16 ES ES92916049T patent/ES2098520T3/en not_active Expired - Lifetime
- 1992-07-16 AT AT92916049T patent/ATE150084T1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE4124701A1 (en) | 1993-01-28 |
WO1993002176A1 (en) | 1993-02-04 |
ATE150084T1 (en) | 1997-03-15 |
EP0595946B1 (en) | 1997-03-12 |
EP0595946A1 (en) | 1994-05-11 |
ES2098520T3 (en) | 1997-05-01 |
JPH06509369A (en) | 1994-10-20 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8363 | Opposition against the patent | ||
8365 | Fully valid after opposition proceedings | ||
8339 | Ceased/non-payment of the annual fee |