DE414813C - Process for making clear and durable emulsions - Google Patents
Process for making clear and durable emulsionsInfo
- Publication number
- DE414813C DE414813C DEA40271D DEA0040271D DE414813C DE 414813 C DE414813 C DE 414813C DE A40271 D DEA40271 D DE A40271D DE A0040271 D DEA0040271 D DE A0040271D DE 414813 C DE414813 C DE 414813C
- Authority
- DE
- Germany
- Prior art keywords
- emulsions
- durable
- making clear
- clear
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000839 emulsion Substances 0.000 title claims description 7
- 238000000034 method Methods 0.000 title claims description 4
- -1 alkali metal salts Chemical class 0.000 claims description 3
- 239000003995 emulsifying agent Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 1
- 238000006467 substitution reaction Methods 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000000243 solution Substances 0.000 description 4
- 239000000344 soap Substances 0.000 description 3
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- 150000001447 alkali salts Chemical class 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- LTGPFZWZZNUIIK-LURJTMIESA-N Lysol Chemical compound NCCCC[C@H](N)CO LTGPFZWZZNUIIK-LURJTMIESA-N 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000003710 aryl alkyl group Chemical group 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229930003836 cresol Natural products 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- BVJCFOOIOSGZFW-UHFFFAOYSA-N n-(4-methylphenyl)sulfonylacetamide Chemical compound CC(=O)NS(=O)(=O)C1=CC=C(C)C=C1 BVJCFOOIOSGZFW-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 239000002674 ointment Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/26—Sulfonamides
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Toxicology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Medicinal Preparation (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Description
Verfahren zur Herstellung klarer und haltbarer Emulsionen.Process for making clear and durable emulsions.
Zur Bereitung von Wasser-in-Öl-Emulsionen, z. B. zur Bereitung von Salben, Schmiermitteln u. dgl., ist bereits die Verwendung von A zidylarylsulfonimiden oder ihrer Alkalisalze vorgeschlagen worden. Sollen bei Benutzung der genannten Emulgierungsmittel größere Mengen Wassers emulgiert werden, so ist der Zusatz von Seife unerläßlich, ohne daß dabei eine klare, in jedem Verhältnis mit Wasser mischbare Lösung erhalten wird. For the preparation of water-in-oil emulsions, e.g. B. for the preparation of Ointments, lubricants and the like, is already the use of azidylarylsulfonimides or their alkali salts have been proposed. Should when using the named Emulsifiers larger amounts of water are emulsified, so is the addition of Soap is indispensable, without it being a clear one that is miscible with water in all proportions Solution is obtained.
Es wurde nun gefunden, daß Körper von der Konstitution Aryl-SOI-NH-R, wobei R Wasserstoff, Alkyl, Aralkyl, Aryl oder Azyl bedeuten kann, und Derivate dieser Verbindungen sich in Form ihrer Alkalisalze vorzüglich zur Herstellung klarer und haltbarer öl-in-'LVasser-Emulsionen eignen. Sie übertreffen hierin in mancher Beziehung selbst die als äußerst wirksam bekannten Seifen. So lassen sich mit ihrer Hilfe z. B. von gewissen mit Seife nicht emulgierbaren Phenolen und Halogenphenolen beliebig verdünnbare Emulsionen herstellen. Die nach diesem Verfahren erhältlichen Emulsionen sollen zu Zwecken der Schädlingsbekämpfung, Reinigung, Desinfektion, z. B. als Lysolersatz u. dgl., Verwendung finden. It has now been found that bodies of the constitution Aryl-SOI-NH-R, where R can be hydrogen, alkyl, aralkyl, aryl or aryl, and derivatives these compounds, in the form of their alkali salts, are excellent for the production of clearer and more durable oil-in-water emulsions. They excel in some Relationship even the soaps known to be extremely effective. So can with her Help z. B. of certain phenols and halophenols that cannot be emulsified with soap Produce emulsions that can be diluted as required. Those obtainable by this process Emulsions should be used for the purposes of pest control, cleaning, disinfection, z. B. as a lysol substitute.
Beispiel 1 54,5 Teile I-Methylbenzol-4-sulfamid werden in 35,5 Teilen einer so, 2prozentigen Kalilauge gelöst, worauf IO Teile Aminobenzol zugegeben werden. Es entsteht eine vollkommen klare, sehr haltbare Lösung, die sich beliebig mit Wasser verdünnen läßt. Example 1 54.5 parts of I-methylbenzene-4-sulfamide are used in 35.5 parts a so, 2 percent potassium hydroxide solution, whereupon 10 parts of aminobenzene are added. The result is a completely clear, very durable solution that can be mixed with water can be diluted.
Xhnlich verhalten sich andere Arylsulfamide sowie deren am Kohlenstoff oder Stickstoff substituierten Abkömmlinge. Other aryl sulfamides and those on carbon behave in a similar manner or nitrogen substituted derivatives.
Beispiel 2. Example 2.
45 Teile 1 - Methylbenzol- 4-sulfosäureazetyl amid werden in 34 Teilen einer so, 2prozentigen Isaliumhydroxydlösung gelöst. Hierauf werden 2I Teile Rohkresol (D.A.B. 5) zugegeben. Man erhält eine klare Lösung, die sich auch nach Verdünnen mit beliebigen Mengen Wassers selbst bei längerem Stehen nicht entmischt. 45 parts of 1 - methylbenzene-4-sulfonic acid acetyl amide are in 34 parts a so, 2 percent isalium hydroxide solution dissolved. This is followed by 2I parts of raw cresol (D.A.B. 5) added. A clear solution is obtained, which also changes after dilution not segregated with any amount of water, even when standing for a long time.
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEA40271D DE414813C (en) | 1923-07-05 | 1923-07-05 | Process for making clear and durable emulsions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEA40271D DE414813C (en) | 1923-07-05 | 1923-07-05 | Process for making clear and durable emulsions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE414813C true DE414813C (en) | 1925-06-08 |
Family
ID=6931871
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEA40271D Expired DE414813C (en) | 1923-07-05 | 1923-07-05 | Process for making clear and durable emulsions |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE414813C (en) |
-
1923
- 1923-07-05 DE DEA40271D patent/DE414813C/en not_active Expired
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