DE3610757A1 - Lagerstabile pulverlacke fuer ueberzuege mit matter oberflaeche - Google Patents
Lagerstabile pulverlacke fuer ueberzuege mit matter oberflaecheInfo
- Publication number
- DE3610757A1 DE3610757A1 DE19863610757 DE3610757A DE3610757A1 DE 3610757 A1 DE3610757 A1 DE 3610757A1 DE 19863610757 DE19863610757 DE 19863610757 DE 3610757 A DE3610757 A DE 3610757A DE 3610757 A1 DE3610757 A1 DE 3610757A1
- Authority
- DE
- Germany
- Prior art keywords
- weight
- parts
- powder coatings
- powder coating
- group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000576 coating method Methods 0.000 title claims abstract description 62
- 239000000843 powder Substances 0.000 title claims abstract description 61
- 239000011248 coating agent Substances 0.000 title claims abstract description 36
- 239000000463 material Substances 0.000 title claims abstract 4
- 239000002253 acid Substances 0.000 claims abstract description 22
- -1 epoxide compounds Chemical class 0.000 claims abstract description 19
- 150000008064 anhydrides Chemical class 0.000 claims abstract description 18
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 14
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims abstract description 12
- 150000007513 acids Chemical class 0.000 claims abstract description 10
- 238000002844 melting Methods 0.000 claims abstract description 9
- 230000008018 melting Effects 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 7
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 6
- 239000001257 hydrogen Substances 0.000 claims abstract description 6
- 239000000654 additive Substances 0.000 claims abstract description 5
- 150000001244 carboxylic acid anhydrides Chemical class 0.000 claims abstract description 5
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims abstract description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 3
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims abstract description 3
- 125000003700 epoxy group Chemical group 0.000 claims abstract description 3
- 150000002431 hydrogen Chemical class 0.000 claims abstract description 3
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims abstract description 3
- 239000004848 polyfunctional curative Substances 0.000 claims description 16
- BKCCAYLNRIRKDJ-UHFFFAOYSA-N 2-phenyl-4,5-dihydro-1h-imidazole Chemical compound N1CCN=C1C1=CC=CC=C1 BKCCAYLNRIRKDJ-UHFFFAOYSA-N 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 11
- 239000004593 Epoxy Substances 0.000 claims description 7
- 125000000217 alkyl group Chemical group 0.000 claims description 5
- JJUVAPMVTXLLFR-UHFFFAOYSA-N 5-methyl-2-phenyl-4,5-dihydro-1h-imidazole Chemical compound N1C(C)CN=C1C1=CC=CC=C1 JJUVAPMVTXLLFR-UHFFFAOYSA-N 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- 150000003512 tertiary amines Chemical class 0.000 claims description 2
- GTDPSWPPOUPBNX-UHFFFAOYSA-N ac1mqpva Chemical compound CC12C(=O)OC(=O)C1(C)C1(C)C2(C)C(=O)OC1=O GTDPSWPPOUPBNX-UHFFFAOYSA-N 0.000 claims 2
- 150000008065 acid anhydrides Chemical class 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 1
- 125000006527 (C1-C5) alkyl group Chemical group 0.000 abstract 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000003822 epoxy resin Substances 0.000 description 41
- 229920000647 polyepoxide Polymers 0.000 description 41
- 239000003795 chemical substances by application Substances 0.000 description 35
- 238000000034 method Methods 0.000 description 35
- 239000004594 Masterbatch (MB) Substances 0.000 description 32
- 239000012463 white pigment Substances 0.000 description 31
- 239000004971 Cross linker Substances 0.000 description 30
- 229910010413 TiO 2 Inorganic materials 0.000 description 30
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 30
- 239000012973 diazabicyclooctane Substances 0.000 description 13
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 12
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 description 12
- VLDPXPPHXDGHEW-UHFFFAOYSA-N 1-chloro-2-dichlorophosphoryloxybenzene Chemical compound ClC1=CC=CC=C1OP(Cl)(Cl)=O VLDPXPPHXDGHEW-UHFFFAOYSA-N 0.000 description 9
- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical class OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 description 8
- 101000738322 Homo sapiens Prothymosin alpha Proteins 0.000 description 7
- 102100033632 Tropomyosin alpha-1 chain Human genes 0.000 description 7
- CWMFRHBXRUITQE-UHFFFAOYSA-N trimethylsilylacetylene Chemical compound C[Si](C)(C)C#C CWMFRHBXRUITQE-UHFFFAOYSA-N 0.000 description 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
- 239000003973 paint Substances 0.000 description 6
- 229920005989 resin Polymers 0.000 description 6
- 239000011347 resin Substances 0.000 description 6
- 150000001409 amidines Chemical class 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 2
- 239000004922 lacquer Substances 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- SRPWOOOHEPICQU-UHFFFAOYSA-N trimellitic anhydride Chemical compound OC(=O)C1=CC=C2C(=O)OC(=O)C2=C1 SRPWOOOHEPICQU-UHFFFAOYSA-N 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- NFDXQGNDWIPXQL-UHFFFAOYSA-N 1-cyclooctyldiazocane Chemical compound C1CCCCCCC1N1NCCCCCC1 NFDXQGNDWIPXQL-UHFFFAOYSA-N 0.000 description 1
- VWSLLSXLURJCDF-UHFFFAOYSA-N 2-methyl-4,5-dihydro-1h-imidazole Chemical compound CC1=NCCN1 VWSLLSXLURJCDF-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 1
- 235000009161 Espostoa lanata Nutrition 0.000 description 1
- 240000001624 Espostoa lanata Species 0.000 description 1
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 description 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 125000000320 amidine group Chemical group 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000000010 aprotic solvent Substances 0.000 description 1
- 125000003118 aryl group Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 125000006159 dianhydride group Chemical group 0.000 description 1
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 1
- 150000002118 epoxides Chemical class 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000006224 matting agent Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 229940098458 powder spray Drugs 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetraline Natural products C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 1
- 125000003944 tolyl group Chemical group 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- DIHAURBCYGTGCV-UHFFFAOYSA-N xi-4,5-Dihydro-2,4(5)-dimethyl-1H-imidazole Chemical compound CC1CN=C(C)N1 DIHAURBCYGTGCV-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/44—Amides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/44—Amides
- C08G59/46—Amides together with other curing agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Paints Or Removers (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863610757 DE3610757A1 (de) | 1986-03-29 | 1986-03-29 | Lagerstabile pulverlacke fuer ueberzuege mit matter oberflaeche |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863610757 DE3610757A1 (de) | 1986-03-29 | 1986-03-29 | Lagerstabile pulverlacke fuer ueberzuege mit matter oberflaeche |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3610757A1 true DE3610757A1 (de) | 1987-10-01 |
| DE3610757C2 DE3610757C2 (enrdf_load_stackoverflow) | 1990-09-13 |
Family
ID=6297599
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19863610757 Granted DE3610757A1 (de) | 1986-03-29 | 1986-03-29 | Lagerstabile pulverlacke fuer ueberzuege mit matter oberflaeche |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE3610757A1 (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0493780A3 (en) * | 1990-12-29 | 1993-05-05 | Skw Trostberg Aktiengesellschaft | Hardener for the preparation of mat coatings basing on epoxy resins |
| WO1995033796A1 (fr) * | 1994-06-03 | 1995-12-14 | Elf Atochem S.A. | Compositions pour le revetement de substrats d'aspect mat |
| WO2020180979A1 (en) * | 2019-03-04 | 2020-09-10 | Sabic Global Technologies B.V. | Thermosetting epoxy composition for powder coating |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2630011A1 (de) * | 1976-07-03 | 1978-01-12 | Schering Ag | Verfahren zum herstellen von ueberzuegen mit matter oberflaeche |
-
1986
- 1986-03-29 DE DE19863610757 patent/DE3610757A1/de active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2630011A1 (de) * | 1976-07-03 | 1978-01-12 | Schering Ag | Verfahren zum herstellen von ueberzuegen mit matter oberflaeche |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0493780A3 (en) * | 1990-12-29 | 1993-05-05 | Skw Trostberg Aktiengesellschaft | Hardener for the preparation of mat coatings basing on epoxy resins |
| WO1995033796A1 (fr) * | 1994-06-03 | 1995-12-14 | Elf Atochem S.A. | Compositions pour le revetement de substrats d'aspect mat |
| WO2020180979A1 (en) * | 2019-03-04 | 2020-09-10 | Sabic Global Technologies B.V. | Thermosetting epoxy composition for powder coating |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3610757C2 (enrdf_load_stackoverflow) | 1990-09-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2328012C3 (de) | Pulverfdrmige Überzugsmittel | |
| DE2609361C3 (de) | Schnellhärtende Pulvermischungen | |
| DE1745425A1 (de) | Warmhaertbare Epoxydharzzubereitungen | |
| DE3611158A1 (de) | Epoxidharzueberzugsmasse | |
| DE2738270A1 (de) | Pulverfoermige ueberzugsmittel und deren anwendung | |
| EP0204658B1 (de) | Härtbares Epoxidharz-Stoffgemisch | |
| DE3610757C2 (enrdf_load_stackoverflow) | ||
| DE19549029A1 (de) | Cyclische Amidin- sowie Uretdiongruppen enthaltende Verbindungen, ein Verfahren zu ihrer Herstellung sowie deren Verwendung | |
| EP0176484A2 (de) | Diäthylphenyl-biguanid enthaltende härtbare Gemische und deren Verwendung | |
| DE1906515A1 (de) | Haertbare Mischungen aus Epoxidharzen und cyclischen Harnstoffderivaten | |
| EP0253115B1 (de) | Pulverlacke, deren Herstellung und Verwendung | |
| EP0085913B1 (de) | Reaktive carboxylgruppenhaltige Polymere, Verfahren zu ihrer Herstellung und ihre Verwendung als Bindemittelkomponente für Pulverlacke | |
| DE1494416B2 (de) | Verfahren zur Erzeugung von Lackbzw. Schutzüberzügen | |
| DE3610758C2 (enrdf_load_stackoverflow) | ||
| DE2024395C3 (de) | Härtbare Mischungen aus Epoxidharz und Biguanid | |
| DE4141858A1 (de) | Mit mercaptoverbindungen vorverlaengerte bisphenol a-diglycidylether | |
| EP0663384B1 (de) | Salze der Pyromellitsäure, ein Verfahren zu ihrer Herstellung sowie deren Verwendung | |
| DE19806225A1 (de) | Epoxidharz- und Hybridpulverbeschichtungszusammensetzungen | |
| DE2949401A1 (de) | Produkte aus einem polyepoxid und zweikernigen hydantoinverbindungen | |
| DE2758006C2 (de) | Schnellhärtende Pulvermischungen | |
| DE4400929A1 (de) | Verfahren zur Herstellung von matten Epoxidharzbeschichtungen | |
| EP0253101A2 (de) | Pulverlacke, deren Herstellung und Verwendung | |
| DE2640410A1 (de) | Lagerstabile, pulverfoermige ueberzugsmittel | |
| DE2630011A1 (de) | Verfahren zum herstellen von ueberzuegen mit matter oberflaeche | |
| DE1943696C3 (de) | Härtungsmittel für ein Epoxidharz mit 1,2-Epoxygruppen |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |