DE3341035A1 - Verfahren zur herstellung von aldehyden - Google Patents
Verfahren zur herstellung von aldehydenInfo
- Publication number
- DE3341035A1 DE3341035A1 DE19833341035 DE3341035A DE3341035A1 DE 3341035 A1 DE3341035 A1 DE 3341035A1 DE 19833341035 DE19833341035 DE 19833341035 DE 3341035 A DE3341035 A DE 3341035A DE 3341035 A1 DE3341035 A1 DE 3341035A1
- Authority
- DE
- Germany
- Prior art keywords
- liquid phase
- phase
- organic
- water
- aqueous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 150000001299 aldehydes Chemical class 0.000 title claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 title description 5
- 239000003054 catalyst Substances 0.000 claims abstract description 30
- 150000001336 alkenes Chemical class 0.000 claims abstract description 27
- 239000007791 liquid phase Substances 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 19
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims abstract description 19
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims abstract description 12
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910002091 carbon monoxide Inorganic materials 0.000 claims abstract description 12
- 239000001257 hydrogen Substances 0.000 claims abstract description 12
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 12
- 238000001816 cooling Methods 0.000 claims abstract description 11
- 239000012074 organic phase Substances 0.000 claims abstract description 11
- 239000012071 phase Substances 0.000 claims abstract description 11
- 239000008346 aqueous phase Substances 0.000 claims abstract description 10
- 150000001875 compounds Chemical class 0.000 claims abstract description 7
- 238000002360 preparation method Methods 0.000 claims abstract 2
- 239000007789 gas Substances 0.000 claims description 32
- 239000007795 chemical reaction product Substances 0.000 claims description 13
- 238000000926 separation method Methods 0.000 claims description 12
- 239000007792 gaseous phase Substances 0.000 claims description 5
- WJIBZZVTNMAURL-UHFFFAOYSA-N phosphane;rhodium Chemical compound P.[Rh] WJIBZZVTNMAURL-UHFFFAOYSA-N 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 abstract description 15
- 238000006243 chemical reaction Methods 0.000 abstract description 12
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 abstract description 8
- 229910052703 rhodium Inorganic materials 0.000 abstract description 7
- 239000010948 rhodium Substances 0.000 abstract description 7
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 abstract description 7
- 229910000073 phosphorus hydride Inorganic materials 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 3
- 239000002912 waste gas Substances 0.000 abstract description 2
- 239000012043 crude product Substances 0.000 description 16
- 238000003786 synthesis reaction Methods 0.000 description 14
- 239000000047 product Substances 0.000 description 12
- 239000000243 solution Substances 0.000 description 7
- 238000004821 distillation Methods 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 238000005191 phase separation Methods 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 4
- 238000007037 hydroformylation reaction Methods 0.000 description 3
- 238000006053 organic reaction Methods 0.000 description 3
- 150000003003 phosphines Chemical class 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- ZTQSAGDEMFDKMZ-UHFFFAOYSA-N Butyraldehyde Chemical compound CCCC=O ZTQSAGDEMFDKMZ-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 150000005840 aryl radicals Chemical class 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 238000005984 hydrogenation reaction Methods 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 125000000542 sulfonic acid group Chemical group 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- AMIMRNSIRUDHCM-UHFFFAOYSA-N Isopropylaldehyde Chemical compound CC(C)C=O AMIMRNSIRUDHCM-UHFFFAOYSA-N 0.000 description 1
- CIUQDSCDWFSTQR-UHFFFAOYSA-N [C]1=CC=CC=C1 Chemical compound [C]1=CC=CC=C1 CIUQDSCDWFSTQR-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000012223 aqueous fraction Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000001914 calming effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- -1 naphthyl radical Chemical class 0.000 description 1
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 150000003283 rhodium Chemical class 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C47/00—Compounds having —CHO groups
- C07C47/02—Saturated compounds having —CHO groups bound to acyclic carbon atoms or to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/49—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
- C07C45/50—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (14)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19833341035 DE3341035A1 (de) | 1983-11-12 | 1983-11-12 | Verfahren zur herstellung von aldehyden |
| KR1019840006040A KR870001875B1 (ko) | 1983-11-12 | 1984-09-29 | 알데히드(Aldehdes) 제조방법 |
| DE8484113242T DE3461920D1 (en) | 1983-11-12 | 1984-11-03 | Process for the production of aldehydes |
| EP84113242A EP0144745B1 (de) | 1983-11-12 | 1984-11-03 | Verfahren zur Herstellung von Aldehyden |
| AT84113242T ATE24710T1 (de) | 1983-11-12 | 1984-11-03 | Verfahren zur herstellung von aldehyden. |
| ZA848635A ZA848635B (en) | 1983-11-12 | 1984-11-05 | Process for the preparation of aldehydes |
| JP59231443A JPS60112733A (ja) | 1983-11-12 | 1984-11-05 | アルデヒドの製法 |
| HU844090A HU199383B (en) | 1983-11-12 | 1984-11-05 | Process for producing aldehydes |
| ES537414A ES537414A0 (es) | 1983-11-12 | 1984-11-06 | Mejoras en un procedimiento para la produccion de aldehidos |
| RO84116213A RO90298A (ro) | 1983-11-12 | 1984-11-07 | Procedeu pentru prepararea aldehidelor |
| AU35281/84A AU565580B2 (en) | 1983-11-12 | 1984-11-09 | Preparation of aldehydes |
| BR8405714A BR8405714A (pt) | 1983-11-12 | 1984-11-09 | Processo para a obtencao de aldeidos |
| US06/670,357 US4577043A (en) | 1983-11-12 | 1984-11-09 | Process for the preparation of aldehydes |
| CN85105113.8A CN1006065B (zh) | 1983-11-12 | 1985-07-04 | 醛的制备方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19833341035 DE3341035A1 (de) | 1983-11-12 | 1983-11-12 | Verfahren zur herstellung von aldehyden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3341035A1 true DE3341035A1 (de) | 1985-05-23 |
Family
ID=6214207
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19833341035 Withdrawn DE3341035A1 (de) | 1983-11-12 | 1983-11-12 | Verfahren zur herstellung von aldehyden |
| DE8484113242T Expired DE3461920D1 (en) | 1983-11-12 | 1984-11-03 | Process for the production of aldehydes |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8484113242T Expired DE3461920D1 (en) | 1983-11-12 | 1984-11-03 | Process for the production of aldehydes |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4577043A (https=) |
| EP (1) | EP0144745B1 (https=) |
| JP (1) | JPS60112733A (https=) |
| KR (1) | KR870001875B1 (https=) |
| AT (1) | ATE24710T1 (https=) |
| AU (1) | AU565580B2 (https=) |
| BR (1) | BR8405714A (https=) |
| DE (2) | DE3341035A1 (https=) |
| ES (1) | ES537414A0 (https=) |
| HU (1) | HU199383B (https=) |
| RO (1) | RO90298A (https=) |
| ZA (1) | ZA848635B (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0269011A1 (de) * | 1986-11-27 | 1988-06-01 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von Aldehyden |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4599206A (en) * | 1984-02-17 | 1986-07-08 | Union Carbide Corporation | Transition metal complex catalyzed reactions |
| DE3413427A1 (de) * | 1984-04-10 | 1985-10-17 | Ruhrchemie Ag, 4200 Oberhausen | Verfahren zur herstellung von aldehyden |
| DE3546123A1 (de) * | 1985-12-24 | 1987-06-25 | Ruhrchemie Ag | Verfahren zur herstellung von aldehyden |
| GB2192182B (en) * | 1986-07-01 | 1990-05-23 | Davy Mckee | Process for the production of aldehydes |
| ATE66668T1 (de) * | 1986-07-01 | 1991-09-15 | Davy Mckee London | Verfahren zur herstellung von aldehyden durch hydroformylierung. |
| US4716250A (en) * | 1986-07-10 | 1987-12-29 | Union Carbide Corporation | Hydroformylation using low volatile/organic soluble phosphine ligands |
| DE3625261A1 (de) * | 1986-07-25 | 1988-02-04 | Basf Ag | Verfahren zur kontinuierlichen hydroformylierung olefinisch ungesaettigter verbindungen |
| US4731486A (en) * | 1986-11-18 | 1988-03-15 | Union Carbide Corporation | Hydroformylation using low volatile phosphine ligands |
| DE3726128A1 (de) * | 1987-08-06 | 1989-02-16 | Ruhrchemie Ag | Verfahren zur herstellung von aldehyden |
| US4871878A (en) * | 1987-08-10 | 1989-10-03 | Eastman Kodak Company | Low pressure rhodium catalyzed hydroformylation of olefins |
| US4827043A (en) * | 1988-01-22 | 1989-05-02 | Eastman Kodak Company | Impurity removal from carbon monoxide and/or hydrogen-containing streams |
| US5001274A (en) * | 1989-06-23 | 1991-03-19 | Union Carbide Chemicals And Plastics Company Inc. | Hydroformylation process |
| US5087763A (en) * | 1990-11-09 | 1992-02-11 | Union Carbide Chemicals & Plastics Technology Corporation | Hydroformylation process |
| US5426238A (en) * | 1993-06-10 | 1995-06-20 | Mitsubishi Kasei Corporation | Method for producing an aldehyde |
| ZA96178B (en) * | 1995-01-18 | 1997-06-30 | Exxon Chemical Patents Inc | Organic compounds and processes for their manufacture |
| DE19925384A1 (de) * | 1999-06-02 | 2000-12-07 | Oxeno Olefinchemie Gmbh | Verfahren zur katalytischen Durchführung von Mehrphasenreaktionen, insbesondere Hydroformylierungen |
| JP3864668B2 (ja) * | 2000-05-01 | 2007-01-10 | 三菱化学株式会社 | アルデヒド類の製造方法 |
| DE10201676A1 (de) * | 2002-01-17 | 2003-07-31 | Basf Ag | Verfahren zur Hydroformylierung von Olefinen mit 2 bis 6 Kohlenstoffatomen |
| WO2020242921A1 (en) | 2019-05-24 | 2020-12-03 | Eastman Chemical Company | Recycle content cellulose ester |
| US11365357B2 (en) | 2019-05-24 | 2022-06-21 | Eastman Chemical Company | Cracking C8+ fraction of pyoil |
| EP3976734A4 (en) | 2019-05-24 | 2023-03-15 | Eastman Chemical Company | CRACKING A C4-C7 FRACTION OF PYROLYTIC OIL |
| CN113993977B (zh) | 2019-05-24 | 2024-09-13 | 伊士曼化工公司 | 进入气体裂化器中加工的液体流中混入少量热解油 |
| WO2020247192A1 (en) | 2019-05-24 | 2020-12-10 | Eastman Chemical Company | Recycle content cracked effluent |
| US12534590B2 (en) | 2019-07-29 | 2026-01-27 | Eastman Chemical Company | Recycle content cyclobutane diol polyester |
| US20220281796A1 (en) | 2019-07-29 | 2022-09-08 | Eastman Chemical Company | Recycle content (c4)alkanoic acid |
| US12338211B2 (en) | 2019-07-29 | 2025-06-24 | Eastman Chemical Company | Recycle content (C4)alkanal |
| KR20220041177A (ko) | 2019-07-29 | 2022-03-31 | 이스트만 케미칼 컴파니 | 열분해 및 가메탄올분해로부터의 재활용된 단량체를 갖는 폴리에스테르의 제조 방법 |
| US12528995B2 (en) | 2019-10-31 | 2026-01-20 | ExxonMobil Product Solutions Company | Pyrolysis method and system for recycled waste |
| US11319262B2 (en) | 2019-10-31 | 2022-05-03 | Eastman Chemical Company | Processes and systems for making recycle content hydrocarbons |
| US11945998B2 (en) | 2019-10-31 | 2024-04-02 | Eastman Chemical Company | Processes and systems for making recycle content hydrocarbons |
| WO2021087057A1 (en) | 2019-10-31 | 2021-05-06 | Eastman Chemical Company | Pyrolysis method and system for recycled waste |
| CN118851872A (zh) | 2019-11-07 | 2024-10-29 | 伊士曼化工公司 | 回收成分丙醇 |
| EP4055001A4 (en) | 2019-11-07 | 2024-02-14 | Eastman Chemical Company | MIXED ESTERS AND SOLVENTS WITH RECYCLED CONTENTS |
| EP4054996A4 (en) | 2019-11-07 | 2024-03-27 | Eastman Chemical Company | Recycle content oxo alcohols & oxo plasticizers |
| KR20220093368A (ko) | 2019-11-07 | 2022-07-05 | 이스트만 케미칼 컴파니 | 재활용물 알파 올레핀 및 지방 알코올 |
| GB202012930D0 (en) * | 2020-08-19 | 2020-09-30 | Johnson Matthey Davy Technologies Ltd | Process for hydroformylation with removal of dissolved hydrogen |
| CN113814005B (zh) * | 2021-09-02 | 2024-05-17 | 宁夏百川科技有限公司 | 一种羰基铑催化剂的回收装置及其回收方法 |
| US12195674B2 (en) | 2021-09-21 | 2025-01-14 | Eastman Chemical Company | Using spent caustic solution from pygas treatment to neutralize halogens from liquified waste plastic |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3733362A (en) * | 1968-03-19 | 1973-05-15 | Union Oil Co | Vapor phase carbonylation |
| JPS4840326B1 (https=) * | 1970-12-15 | 1973-11-30 | ||
| US4248802A (en) * | 1975-06-20 | 1981-02-03 | Rhone-Poulenc Industries | Catalytic hydroformylation of olefins |
| US4306084A (en) * | 1978-12-06 | 1981-12-15 | The University Of Texas | Alcohol and aldehyde production using ruthenium carbonyl catalysts |
| DE2965157D1 (en) * | 1979-03-21 | 1983-05-11 | Davy Mckee London | Process for the production of aldehydes by hydroformylation of alkenes |
| US4258215A (en) * | 1979-08-29 | 1981-03-24 | Eastman Kodak Company | Hydroformylation process |
| JPS5645436A (en) * | 1979-09-21 | 1981-04-25 | Mitsubishi Chem Ind Ltd | Hydroformylation of olefin |
| GB2085874B (en) * | 1980-09-04 | 1984-08-08 | Johnson Matthey Plc | Hydroformylation of olefins |
| DE3114147A1 (de) * | 1981-04-08 | 1982-10-28 | Basf Ag, 6700 Ludwigshafen | Verfahren zur gewinnung von aldehyden |
| JPS58157739A (ja) * | 1982-03-12 | 1983-09-19 | Kuraray Co Ltd | １，９−ノナンジア−ルの製造方法 |
| DE3234701A1 (de) * | 1982-09-18 | 1984-04-05 | Ruhrchemie Ag, 4200 Oberhausen | Verfahren zur herstellung von aldehyden |
-
1983
- 1983-11-12 DE DE19833341035 patent/DE3341035A1/de not_active Withdrawn
-
1984
- 1984-09-29 KR KR1019840006040A patent/KR870001875B1/ko not_active Expired
- 1984-11-03 EP EP84113242A patent/EP0144745B1/de not_active Expired
- 1984-11-03 AT AT84113242T patent/ATE24710T1/de not_active IP Right Cessation
- 1984-11-03 DE DE8484113242T patent/DE3461920D1/de not_active Expired
- 1984-11-05 ZA ZA848635A patent/ZA848635B/xx unknown
- 1984-11-05 HU HU844090A patent/HU199383B/hu not_active IP Right Cessation
- 1984-11-05 JP JP59231443A patent/JPS60112733A/ja active Granted
- 1984-11-06 ES ES537414A patent/ES537414A0/es active Granted
- 1984-11-07 RO RO84116213A patent/RO90298A/ro unknown
- 1984-11-09 US US06/670,357 patent/US4577043A/en not_active Expired - Lifetime
- 1984-11-09 AU AU35281/84A patent/AU565580B2/en not_active Ceased
- 1984-11-09 BR BR8405714A patent/BR8405714A/pt not_active IP Right Cessation
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0269011A1 (de) * | 1986-11-27 | 1988-06-01 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von Aldehyden |
| US4801754A (en) * | 1986-11-27 | 1989-01-31 | Ruhrchemie Aktiengesellschaft | Hydroformylation process |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0144745B1 (de) | 1987-01-07 |
| ATE24710T1 (de) | 1987-01-15 |
| AU565580B2 (en) | 1987-09-17 |
| KR870001875B1 (ko) | 1987-10-20 |
| KR850004088A (ko) | 1985-07-01 |
| US4577043A (en) | 1986-03-18 |
| JPS60112733A (ja) | 1985-06-19 |
| AU3528184A (en) | 1985-05-16 |
| ES8601087A1 (es) | 1985-10-16 |
| HUT38088A (en) | 1986-04-28 |
| EP0144745A1 (de) | 1985-06-19 |
| RO90298A (ro) | 1986-10-30 |
| HU199383B (en) | 1990-02-28 |
| JPS6365056B2 (https=) | 1988-12-14 |
| DE3461920D1 (en) | 1987-02-12 |
| ES537414A0 (es) | 1985-10-16 |
| BR8405714A (pt) | 1985-09-10 |
| ZA848635B (en) | 1985-06-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8139 | Disposal/non-payment of the annual fee |