DE3025463A1 - Verfahren zur trennung oder reinigung von gemischen mit hilfe eines festen adsorbens - Google Patents
Verfahren zur trennung oder reinigung von gemischen mit hilfe eines festen adsorbensInfo
- Publication number
- DE3025463A1 DE3025463A1 DE19803025463 DE3025463A DE3025463A1 DE 3025463 A1 DE3025463 A1 DE 3025463A1 DE 19803025463 DE19803025463 DE 19803025463 DE 3025463 A DE3025463 A DE 3025463A DE 3025463 A1 DE3025463 A1 DE 3025463A1
- Authority
- DE
- Germany
- Prior art keywords
- adsorbable
- temperature
- adsorbent
- container
- gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 53
- 239000000203 mixture Substances 0.000 title claims description 51
- 239000003463 adsorbent Substances 0.000 title claims description 43
- 239000007787 solid Substances 0.000 title description 11
- 239000007789 gas Substances 0.000 claims description 51
- 238000001179 sorption measurement Methods 0.000 claims description 31
- 230000008569 process Effects 0.000 claims description 21
- 238000000926 separation method Methods 0.000 claims description 19
- 238000003795 desorption Methods 0.000 claims description 17
- 239000000470 constituent Substances 0.000 claims description 15
- 239000000126 substance Substances 0.000 claims description 14
- 238000001816 cooling Methods 0.000 claims description 5
- 230000007423 decrease Effects 0.000 claims description 3
- 229930195733 hydrocarbon Natural products 0.000 claims description 3
- 150000002430 hydrocarbons Chemical class 0.000 claims description 3
- 239000002808 molecular sieve Substances 0.000 claims description 3
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 3
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 2
- 229920001577 copolymer Polymers 0.000 claims description 2
- 229910044991 metal oxide Inorganic materials 0.000 claims description 2
- 150000004706 metal oxides Chemical class 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical class [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical class O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 1
- 230000003247 decreasing effect Effects 0.000 claims 1
- 230000000763 evoking effect Effects 0.000 claims 1
- 235000012239 silicon dioxide Nutrition 0.000 claims 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 17
- 150000001875 compounds Chemical class 0.000 description 16
- 239000003480 eluent Substances 0.000 description 6
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 6
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 6
- 229920006395 saturated elastomer Polymers 0.000 description 6
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 description 5
- 239000002156 adsorbate Substances 0.000 description 4
- 239000012159 carrier gas Substances 0.000 description 3
- 239000001282 iso-butane Substances 0.000 description 3
- 239000008186 active pharmaceutical agent Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 description 2
- 238000010828 elution Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- JFUIHGAGFMFNRD-UHFFFAOYSA-N fica Chemical compound FC1=CC=C2NC(C(=O)NCCS)=CC2=C1 JFUIHGAGFMFNRD-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000002336 sorption--desorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
- B01D53/0462—Temperature swing adsorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2256/00—Main component in the product gas stream after treatment
- B01D2256/24—Hydrocarbons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
- B01D2257/702—Hydrocarbons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/401—Further details for adsorption processes and devices using a single bed
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Separation Of Gases By Adsorption (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Detergent Compositions (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7917624A FR2460703A1 (fr) | 1979-07-06 | 1979-07-06 | Procede de separation ou de purification de melanges a l'aide d'un solide adsorbant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3025463A1 true DE3025463A1 (de) | 1981-01-22 |
Family
ID=9227624
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19803025463 Withdrawn DE3025463A1 (de) | 1979-07-06 | 1980-07-04 | Verfahren zur trennung oder reinigung von gemischen mit hilfe eines festen adsorbens |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4324566A (enExample) |
| BE (1) | BE884185A (enExample) |
| CA (1) | CA1141307A (enExample) |
| DE (1) | DE3025463A1 (enExample) |
| FR (1) | FR2460703A1 (enExample) |
| GB (1) | GB2054403B (enExample) |
| IT (1) | IT1131670B (enExample) |
| NL (1) | NL8003912A (enExample) |
| NO (1) | NO802035L (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3201390A1 (de) * | 1982-01-19 | 1983-07-28 | CEAG Verfahrenstechnik GmbH, 4714 Selm | Verfahren zur rueckgewinnung eines im wesentlichen wasserfreien desorbats sowie vorrichtung zum durchfuehren des verfahrens |
| US4472178A (en) * | 1983-07-05 | 1984-09-18 | Air Products And Chemicals, Inc. | Adsorptive process for the removal of carbon dioxide from a gas |
| US5766311A (en) * | 1996-07-03 | 1998-06-16 | Praxair Technology, Inc. | Multi-thermal pulse PSA system |
| FR2799390B1 (fr) * | 1999-10-08 | 2002-06-07 | Air Liquide | Procede de traitement d'un gaz par adsorption a temperature modulee |
| US20040224422A1 (en) * | 2002-09-27 | 2004-11-11 | Ulrich Bonne | Phased micro analyzer III, IIIA |
| US7000452B2 (en) * | 2002-09-27 | 2006-02-21 | Honeywell International Inc. | Phased micro fluid analyzer |
| US7367216B2 (en) * | 2002-09-27 | 2008-05-06 | Honeywell International Inc. | Phased micro analyzer V, VI |
| US7530257B2 (en) * | 2002-09-27 | 2009-05-12 | Honeywell International Inc. | Phased micro analyzer VIII |
| EP1570261B1 (en) * | 2002-12-10 | 2016-09-07 | Honeywell International Inc. | Phased micro analyzer |
| US7502109B2 (en) * | 2005-05-17 | 2009-03-10 | Honeywell International Inc. | Optical micro-spectrometer |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2889893A (en) * | 1955-03-28 | 1959-06-09 | Texaco Inc | Adsorption separation process |
| US2818137A (en) * | 1955-10-24 | 1957-12-31 | Texas Co | Adsorptive separation process |
| US3043127A (en) * | 1958-12-11 | 1962-07-10 | Phillips Petroleum Co | Thermochromatography heater |
| US3094483A (en) * | 1960-07-12 | 1963-06-18 | Standard Oil Co | Hydrocarbon separation process |
| US3225521A (en) * | 1962-06-04 | 1965-12-28 | Gulf Research Development Co | Serially connected thermochromatographic columns |
| US3323288A (en) * | 1964-05-27 | 1967-06-06 | Union Carbide Corp | Selective adsorption process and apparatus |
| US3369874A (en) * | 1966-02-08 | 1968-02-20 | Research Corp | Mixture separation by cyclic pulsing in a temperature graduated adsorbent bed |
| US3581465A (en) * | 1966-11-25 | 1971-06-01 | Shimazu Seisakusho Ltd | Method and apparatus for concentrating and trapping sample component |
| US3542525A (en) * | 1969-02-24 | 1970-11-24 | Atomic Energy Commission | Cycling zone adsorption process |
| US3653184A (en) * | 1970-06-08 | 1972-04-04 | Mobil Oil Corp | Separation of c{11 {0 aromatics mixture with production chromatography |
| US3660967A (en) * | 1970-09-08 | 1972-05-09 | Union Carbide Corp | Purification of fluid streams by selective adsorption |
| GB1517694A (en) * | 1974-07-03 | 1978-07-12 | Nat Res Dev | Methods and applications of preparative scale chromatography |
-
1979
- 1979-07-06 FR FR7917624A patent/FR2460703A1/fr active Granted
-
1980
- 1980-07-02 US US06/165,243 patent/US4324566A/en not_active Expired - Lifetime
- 1980-07-04 DE DE19803025463 patent/DE3025463A1/de not_active Withdrawn
- 1980-07-04 CA CA000355423A patent/CA1141307A/fr not_active Expired
- 1980-07-04 BE BE0/201305A patent/BE884185A/fr not_active IP Right Cessation
- 1980-07-04 IT IT23229/80A patent/IT1131670B/it active
- 1980-07-04 GB GB8022022A patent/GB2054403B/en not_active Expired
- 1980-07-04 NO NO802035A patent/NO802035L/no unknown
- 1980-07-07 NL NL8003912A patent/NL8003912A/nl not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| FR2460703A1 (fr) | 1981-01-30 |
| GB2054403A (en) | 1981-02-18 |
| IT1131670B (it) | 1986-06-25 |
| NL8003912A (nl) | 1981-01-08 |
| FR2460703B1 (enExample) | 1984-02-10 |
| CA1141307A (fr) | 1983-02-15 |
| BE884185A (fr) | 1980-11-03 |
| GB2054403B (en) | 1983-05-05 |
| IT8023229A0 (it) | 1980-07-04 |
| NO802035L (no) | 1981-01-07 |
| US4324566A (en) | 1982-04-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8139 | Disposal/non-payment of the annual fee |