DE3019625A1 - Verfahren und reaktor zur durchfuehrung exothermer bzw. endothermer katalytischer reaktionen in der gasphase unter hohem druck - Google Patents

Verfahren und reaktor zur durchfuehrung exothermer bzw. endothermer katalytischer reaktionen in der gasphase unter hohem druck

Info

Publication number
DE3019625A1
DE3019625A1 DE19803019625 DE3019625A DE3019625A1 DE 3019625 A1 DE3019625 A1 DE 3019625A1 DE 19803019625 DE19803019625 DE 19803019625 DE 3019625 A DE3019625 A DE 3019625A DE 3019625 A1 DE3019625 A1 DE 3019625A1
Authority
DE
Germany
Prior art keywords
synthesis gas
reactor
reaction
heat exchanger
flow
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE19803019625
Other languages
German (de)
English (en)
Inventor
John Vincent Albano
George Friedman
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lummus Technology LLC
Original Assignee
Lummus Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lummus Co filed Critical Lummus Co
Publication of DE3019625A1 publication Critical patent/DE3019625A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0005—Catalytic processes under superatmospheric pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0403—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
    • B01J8/0407—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds
    • B01J8/0415—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/04—Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • C01C1/0417—Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst characterised by the synthesis reactor, e.g. arrangement of catalyst beds and heat exchangers in the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/02—Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208—Preparation in gaseous phase
    • C01C3/0212—Preparation in gaseous phase from hydrocarbons and ammonia in the presence of oxygen, e.g. the Andrussow-process
    • C01C3/022—Apparatus therefor
    • C01C3/0225—Apparatus therefor characterised by the synthesis reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
    • C07C29/1516—Multisteps
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
    • C07C29/152—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the reactor used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/0007—Pressure measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00088—Flow rate measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/00132—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00194—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Fluid Mechanics (AREA)
  • Toxicology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DE19803019625 1979-05-22 1980-05-22 Verfahren und reaktor zur durchfuehrung exothermer bzw. endothermer katalytischer reaktionen in der gasphase unter hohem druck Withdrawn DE3019625A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/041,378 US4341737A (en) 1979-05-22 1979-05-22 Apparatus for carrying out catalytic exothermic and endothermic high-pressure gas reactions

Publications (1)

Publication Number Publication Date
DE3019625A1 true DE3019625A1 (de) 1980-11-27

Family

ID=21916191

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19803019625 Withdrawn DE3019625A1 (de) 1979-05-22 1980-05-22 Verfahren und reaktor zur durchfuehrung exothermer bzw. endothermer katalytischer reaktionen in der gasphase unter hohem druck

Country Status (10)

Country Link
US (1) US4341737A (enExample)
JP (1) JPS562841A (enExample)
AU (1) AU532977B2 (enExample)
CA (1) CA1121987A (enExample)
DE (1) DE3019625A1 (enExample)
FR (1) FR2457124A1 (enExample)
GB (1) GB2053017B (enExample)
IN (1) IN154372B (enExample)
IT (2) IT1140966B (enExample)
NL (1) NL8002943A (enExample)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3343114A1 (de) * 1983-11-29 1985-06-05 Uhde Gmbh, 4600 Dortmund Vorrichtung zur durchfuehrung exothermer, katalytischer gasreaktionen fuer die ammoniak- oder methanol-synthese
DE3643726A1 (de) * 1986-12-20 1988-06-30 Uhde Gmbh Vorrichtung als nh(pfeil abwaerts)3(pfeil abwaerts)-reaktor
DE3710004A1 (de) * 1987-03-26 1988-10-06 Uhde Gmbh Vorrichtung zur katalytischen behandlung von stickstoff und wasserstoff

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2527097A1 (fr) * 1982-05-21 1983-11-25 Inst Francais Du Petrole Reacteur longitudinal pour syntheses chimiques en phase gazeuse et en catalyse heterogene
US4518574A (en) * 1983-03-07 1985-05-21 Exxon Research & Engineering Co. Catalytic gas synthesis process
US4637918A (en) * 1983-03-07 1987-01-20 Exxon Research & Engineering Co. Catalytic gas synthesis apparatus
US4789527A (en) * 1983-03-07 1988-12-06 Exxon Research & Engineering Co. Catalytic gas synthesis apparatus
DE3318098A1 (de) * 1983-05-18 1984-11-22 Linde Ag, 6200 Wiesbaden Verfahren und reaktor zur durchfuehrung einer endo- oder exothermen reaktion
BG40018A1 (en) * 1983-07-01 1986-10-15 Nikolov Reactor for carrying out high exothermic and endothermic catalytic processes
TR23236A (tr) * 1984-08-23 1989-07-21 Exxon Research Engineering Co Gelistirilmis katalitik gaz sentezi yoentemi ve cihazi
CH670400A5 (enExample) * 1986-03-13 1989-06-15 Ammonia Casale Sa
GB8609099D0 (en) * 1986-04-15 1986-05-21 British Petroleum Co Plc Production of synthesis gas
GB2193444B (en) * 1986-07-24 1990-10-31 Shell Int Research Process for the chemical conversion of a gaseous feed into an at least partly liquid product
US5192512A (en) * 1987-01-21 1993-03-09 Institut Francais Du Petrole Apparatus for performing chemical reactions under pressure in a multi-stage reaction zone with external intermediary thermal conditioning
DE3708957C2 (de) * 1987-03-19 1996-04-25 Linde Ag Reaktor zur katalytischen Umsetzung von in einem Gasstrom enthaltenem H¶2¶S und SO¶2¶ zu elementarem Schwefel
CN88103614A (zh) * 1987-05-14 1988-12-14 阿莫尼·卡萨尔公司 多相合成反应器的改进
US7066973B1 (en) 1996-08-26 2006-06-27 Nuvera Fuel Cells Integrated reformer and shift reactor
US6012598A (en) * 1997-06-09 2000-01-11 The Columbiana Boiler Company Freight container
DE19754988A1 (de) * 1997-12-11 1999-06-17 Degussa Herstellung von Blausäure nach dem Andrussow-Verfahren
US6620386B1 (en) * 1998-07-09 2003-09-16 Stone & Webster, Inc. Radial flow reactor
US6641625B1 (en) 1999-05-03 2003-11-04 Nuvera Fuel Cells, Inc. Integrated hydrocarbon reforming system and controls
US6986797B1 (en) 1999-05-03 2006-01-17 Nuvera Fuel Cells Inc. Auxiliary reactor for a hydrocarbon reforming system
JP2006502938A (ja) 2002-06-13 2006-01-26 ヌヴェラ フューエル セルズ インコーポレイテッド 優先的酸化反応装置の温度調整
EP1442786A1 (en) * 2003-01-29 2004-08-04 Methanol Casale S.A. Pseudo isothermal radial reactor
US7371361B2 (en) * 2004-11-03 2008-05-13 Kellogg Brown & Root Llc Maximum reaction rate converter system for exothermic reactions
US7510696B2 (en) * 2005-02-07 2009-03-31 Air Products And Chemicals, Inc. Method and apparatus for the production of hydrogen-rich gas
DE102016203753A1 (de) * 2016-03-08 2017-09-14 Thyssenkrupp Ag Verfahren zur Herstellung von Produkten unter wechselnden Lastbedingungen
NZ748600A (en) * 2016-06-21 2023-06-30 Haldor Topsoe As Axial/radial flow converter
WO2018029081A1 (de) * 2016-08-09 2018-02-15 Thyssenkrupp Industrial Solutions Ag Verfahren zur herstellung von ammoniak sowie ammoniaksynthesekonverter
CN115175757A (zh) * 2020-01-24 2022-10-11 碳回收国际公司 负荷跟随反应器系统、相关设备及其操作方法
US12491484B2 (en) 2021-01-15 2025-12-09 CRI, hf Reactor for synthesis of methanol or other products
US11738317B2 (en) 2021-01-15 2023-08-29 CRI, hf Reactor for synthesizing methanol or other products
EP4516740A1 (en) * 2023-09-04 2025-03-05 Topsoe A/S Method for controlling an ammonia plant using renewable energy

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1381826A (fr) * 1964-02-04 1964-12-14 Procédé et dispositif de dérivation de la chaleur de réaction de synthèses à haute pression catalytiques exothermiques de gaz
US3302705A (en) * 1964-09-21 1967-02-07 American Radiator & Standard Heat exchanger
DE1940980A1 (de) * 1964-10-27 1971-02-25 Lentia Gmbh Vorrichtung zur Durchfuehrung exothermer katalytischer Gasreaktionen
FR93022E (fr) * 1964-10-27 1969-01-31 Chemie Linz Ag Procédé et dispositif pour effectuer des réactions catalytiques exothermiques en phase gazeuse.
US3472631A (en) * 1966-04-25 1969-10-14 Robert H Schober Apparatus for carrying out exothermic catalytic gas reactions
US3556738A (en) * 1966-09-12 1971-01-19 Robert Schober Exothermic catalytic gas reactor
DE1914246B1 (de) * 1969-03-20 1970-09-03 Lentia Gmbh Chem Und Pharm Erz Hochdruckreaktor fuer exotherme katalytische Gasreaktionen
BE754531A (fr) * 1969-08-07 1971-02-08 Chemie Linz Ag Procede et dispositif pour le guidage du gaz dans les reacteursde synthese catalytique a haute pression
US3866668A (en) * 1971-01-28 1975-02-18 Du Pont Method of heat exchange using rotary heat exchanger
IT1041778B (it) * 1975-07-15 1980-01-10 Snam Progetti Reattore a flusso radiale per la sintesi dell ammoniaca con produzione di vapore ad alto livello termico
US4152407A (en) * 1977-02-02 1979-05-01 Warren Fuchs Process and apparatus for exothermic reactions
US4230669A (en) * 1978-07-17 1980-10-28 Pullman Incorporated Radial ammonia converter

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3343114A1 (de) * 1983-11-29 1985-06-05 Uhde Gmbh, 4600 Dortmund Vorrichtung zur durchfuehrung exothermer, katalytischer gasreaktionen fuer die ammoniak- oder methanol-synthese
DE3643726A1 (de) * 1986-12-20 1988-06-30 Uhde Gmbh Vorrichtung als nh(pfeil abwaerts)3(pfeil abwaerts)-reaktor
DE3710004A1 (de) * 1987-03-26 1988-10-06 Uhde Gmbh Vorrichtung zur katalytischen behandlung von stickstoff und wasserstoff

Also Published As

Publication number Publication date
CA1121987A (en) 1982-04-20
IN154372B (enExample) 1984-10-20
JPS562841A (en) 1981-01-13
GB2053017A (en) 1981-02-04
IT8022203A0 (it) 1980-05-20
IT8022202A0 (it) 1980-05-20
GB2053017B (en) 1984-03-14
IT1140966B (it) 1986-10-10
AU5861780A (en) 1980-11-27
AU532977B2 (en) 1983-10-20
FR2457124A1 (fr) 1980-12-19
US4341737A (en) 1982-07-27
NL8002943A (nl) 1980-11-25

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Legal Events

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8110 Request for examination paragraph 44
8128 New person/name/address of the agent

Representative=s name: OEDEKOVEN, W., DIPL.-ING., PAT.-ANW., 8000 MUENCHE

8130 Withdrawal