DE299988C - PROCESS FOR THE MANUFACTURING OF SLIGHTLY SOLUBLE TANNING PREPARATIONS IN COLD WATER - Google Patents
PROCESS FOR THE MANUFACTURING OF SLIGHTLY SOLUBLE TANNING PREPARATIONS IN COLD WATERInfo
- Publication number
- DE299988C DE299988C DE1914299988D DE299988DA DE299988C DE 299988 C DE299988 C DE 299988C DE 1914299988 D DE1914299988 D DE 1914299988D DE 299988D A DE299988D A DE 299988DA DE 299988 C DE299988 C DE 299988C
- Authority
- DE
- Germany
- Prior art keywords
- manufacturing
- cold water
- slightly soluble
- tanning preparations
- tanning
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C14—SKINS; HIDES; PELTS; LEATHER
- C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
- C14C3/00—Tanning; Compositions for tanning
- C14C3/02—Chemical tanning
- C14C3/08—Chemical tanning by organic agents
- C14C3/10—Vegetable tanning
- C14C3/12—Vegetable tanning using purified or modified vegetable tanning agents
-
- C—CHEMISTRY; METALLURGY
- C14—SKINS; HIDES; PELTS; LEATHER
- C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
- C14C3/00—Tanning; Compositions for tanning
- C14C3/02—Chemical tanning
- C14C3/08—Chemical tanning by organic agents
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Treatment And Processing Of Natural Fur Or Leather (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
PATENTSCHRIFTPATENT LETTERING
·■— M 299988 KLASSE 2Qa. GRUPPE· ■ - M 299988 CLASS 2Qa. GROUP
Zusatz zum Patent 284119. ■Addendum to patent 284119. ■
~ ■ Patentiert im Deutschen Reiche vom 30. Januar 1914 ab.~ ■ Patented in the German Empire on January 30, 1914.
Längste Dauer: 16.Oktober 1927.Longest duration: October 16, 1927.
"Im Hauptpatent 284119 ist ein Verfahren zur Herstellung von in kaltem Wasser leicht löslichen Gerbstoffpräparaten aus Gerbstoffextrakten, welche unlösliche bzw. schwerlösliehe Bestandteile enthalten, beschrieben, darin bestehend, daß man die fertigen, eingedickten Gerbstoffextrakte bzw. deren unlösliche oder schwerlösliche Bestandteile, oder die zwecks Herstellung der Extrakte einzudickenden dünnen Brühen mit solchen wasserlöslichen, in ihrem Molekül eine oder mehrere saure salzbildende Gruppen, außer den Hydroxylgruppen enthaltenden Verbindungen, behandelt, wie sie aus aromatischen Oxyverbindungen durch Kondensation mit Formaldehyd oder Formaldehyd entwickelnden oder wie dieser reagierenden Stoffen erhältlich sind, oder mit solchen wasserlöslichen Verbindungen versetzt, wie sie durch Kondensation von Phenolsulfosäuren oder deren Homologen für sich erhalten werden können."In the main patent 284119 is a process for the production of tanning preparations from tannin extracts, which are easily soluble in cold water, which contain insoluble or poorly soluble components, described therein consisting that the finished, thickened tannin extracts or their insoluble or poorly soluble constituents, or the thin ones to be thickened for the purpose of producing the extracts Broths with such water-soluble, in their molecule one or more acidic salt-forming Groups other than the hydroxyl containing compounds treated as they are from aromatic oxy compounds by condensation with formaldehyde or formaldehyde substances that develop or react with them, or with such added to water-soluble compounds, such as those produced by the condensation of phenol sulfonic acids or whose homologues can be obtained for themselves.
In dem Zusatzpatent 299857 wurde dieses Verfahren dahin erweitert, daß man an Stelle der im Hauptpatent beanspruchten Produkte andere synthetische, gerbende Eigenschaften besitzende Verbindungen, insbesondere diejenigen Stoffe, deren Verwendung als Gerbstoffe in den Patenten 281484 und 290965 geschützt ist, benutzen kann.In the additional patent 299857 this process was expanded to include the products claimed in the main patent have other synthetic, tanning properties Possessing compounds, especially those substances whose use as tanning agents is protected in patents 281484 and 290965.
Es wurde nun gefunden, daß man statt der fertigen, eingedickten Gerbstoffextrakte bzw. ihrer 'unlöslichen oder schwerlöslichen Bestandteile, oder der zwecks Herstellung der Extrakte einzudickenden dünnen Brühen auch direkt die gerbende Stoffe enthaltenden Materialien, sei es unmittelbar, sei es nach vorheriger Extraktion mit anderen extrahierenden Mitteln verwenden kann.It has now been found that instead of the finished, thickened tannin extracts or their 'insoluble or sparingly soluble components, or the thin broths to be thickened for the purpose of producing the extracts, also directly the Materials containing tanning substances, either immediately or after previous extraction can use with other extracting agents.
Das für die Herstellung von Gerbbrühen bzw. Gerbextrakten zur Verwendung kommende pflanzliche Gerbstoffmaterial, z. B. Quebrachoholz< wird nach entsprechender Vermahlung in den Extraktionsapparaten, wie üblich,- der Extraktion mit einer heißen etwa 1 ° Be starken wäßrigen Lösung des im Beispiel 2 des Patentes 290965 beschriebenen Produktes unterworfen. Nach Abzug dieser ersten gerbstoffreichen Brühe kann das Material in beliebiger Weise bis zur völligen Erschöpfung weiter extrahiert werdend Die Schlußextraktion kann z. B. auch nach, Beispiel 2 erfolgen.That which is used for the production of tanning liquors or tanning extracts vegetable tanning material, e.g. B. Quebracho wood < is after appropriate grinding in the extraction apparatus, as usual, - the Extraction with a hot about 1 ° Be strong aqueous solution of the example 2 of the patent 290965 product described. After deducting this first rich in tannin Broth, the material can be extracted further in any way until it is completely exhausted. The final extraction can z. B. also according to Example 2.
Beispiel 2. >Example 2.>
Das nach Beispiel 1 vorbehandelte Material oder das wie üblich durch Behandeln mit reinem Wasser oder schwächeren Gerbbrühen oder anderen extrahierenden Mitteln mehr oder weniger erschöpf te Gerbstoff material wird bei 90 bis ioo° C mit einer etwa 1° Be starken Lösung des im Beispiel 1 der Patent-The material pretreated according to Example 1 or as usual by treating with pure water or weaker tanning liquors or other extracting agents or less exhausted tannin material is at 90 to 100 ° C with a about 1 ° Be strong solution of the example 1 of the patent
schrift 26255$ beschriebenen anneutralisierten Produktes kurz behandelt. Zur vollständigen Entfernung des vom Gerbmaterial aus der Exträktiorisbrühe etwa aufgesaugten Produktes wird das7 Material dann noch einer Behandlung mit reinem Wasser in der Siedehitze unterzogen. Die so erhaltenen Brühen können z. B; für sich zu Angerbezwecken oder als Nachdrückbrühen verwendet werden.26255 $ described anneutralized product briefly treated. For complete removal of about sucked from the Exträktiorisbrühe from Gerbmaterial product, the material 7 is then subjected to a treatment with pure water in boiling heat. The broths thus obtained can, for. B; can be used on their own for tanning purposes or as follow-up brews.
In analoger Weise verfährt man bei Extraktion anderer gerbstoffhaltiger Materialien sowie bei Verwendung anderer lösend wirkender Mittel der eingangs gekennzeichneten Art.An analogous procedure is used for the extraction of other materials containing tannin as well when using other dissolving agents of the type identified at the beginning.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE284119T | 1912-10-17 |
Publications (1)
Publication Number | Publication Date |
---|---|
DE299988C true DE299988C (en) | 1917-08-06 |
Family
ID=60410195
Family Applications (4)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1912284119D Expired DE284119C (en) | 1912-10-17 | 1912-10-17 | A PROCESS FOR THE PRODUCTION OF TANNING PREPARATIONS, ELEVY SOLUBLE IN COLD WATER, FROM TANNING MATERIAL EXTRACTS WHICH ARE INSOLUBLE OR CONTAINS LOW COMPONENTS |
DE1913299857D Expired DE299857C (en) | 1912-10-17 | 1913-07-06 | A PROCESS FOR THE PRODUCTION OF ELEVANTLY SOLUBLE TANNING PREPARATIONS IN COLD WATER, UAS TANNING EXTRACTS, WHICH ARE INSOLUBLE OR. CONTAINS LOW COMPONENTS |
DE1914299988D Expired DE299988C (en) | 1912-10-17 | 1914-01-30 | PROCESS FOR THE MANUFACTURING OF SLIGHTLY SOLUBLE TANNING PREPARATIONS IN COLD WATER |
DEB97770D Expired DE393697C (en) | 1912-10-17 | 1921-01-15 | Process for the production of tanning preparations which are easily soluble in cold water |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1912284119D Expired DE284119C (en) | 1912-10-17 | 1912-10-17 | A PROCESS FOR THE PRODUCTION OF TANNING PREPARATIONS, ELEVY SOLUBLE IN COLD WATER, FROM TANNING MATERIAL EXTRACTS WHICH ARE INSOLUBLE OR CONTAINS LOW COMPONENTS |
DE1913299857D Expired DE299857C (en) | 1912-10-17 | 1913-07-06 | A PROCESS FOR THE PRODUCTION OF ELEVANTLY SOLUBLE TANNING PREPARATIONS IN COLD WATER, UAS TANNING EXTRACTS, WHICH ARE INSOLUBLE OR. CONTAINS LOW COMPONENTS |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DEB97770D Expired DE393697C (en) | 1912-10-17 | 1921-01-15 | Process for the production of tanning preparations which are easily soluble in cold water |
Country Status (1)
Country | Link |
---|---|
DE (4) | DE284119C (en) |
-
1912
- 1912-10-17 DE DE1912284119D patent/DE284119C/en not_active Expired
-
1913
- 1913-07-06 DE DE1913299857D patent/DE299857C/en not_active Expired
-
1914
- 1914-01-30 DE DE1914299988D patent/DE299988C/en not_active Expired
-
1921
- 1921-01-15 DE DEB97770D patent/DE393697C/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE299857C (en) | 1917-08-01 |
DE393697C (en) | 1924-04-05 |
DE284119C (en) | 1915-05-04 |
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