DE2656633A1 - Verfahren zur reinigung von gasgemischen - Google Patents
Verfahren zur reinigung von gasgemischenInfo
- Publication number
- DE2656633A1 DE2656633A1 DE19762656633 DE2656633A DE2656633A1 DE 2656633 A1 DE2656633 A1 DE 2656633A1 DE 19762656633 DE19762656633 DE 19762656633 DE 2656633 A DE2656633 A DE 2656633A DE 2656633 A1 DE2656633 A1 DE 2656633A1
- Authority
- DE
- Germany
- Prior art keywords
- zeolite
- composition
- temperature
- adsorption
- sio
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000203 mixture Substances 0.000 title claims description 54
- 238000000034 method Methods 0.000 title claims description 51
- 239000010457 zeolite Substances 0.000 claims description 91
- 229910021536 Zeolite Inorganic materials 0.000 claims description 88
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 88
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 55
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 53
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 48
- 238000001179 sorption measurement Methods 0.000 claims description 42
- 239000007789 gas Substances 0.000 claims description 41
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 24
- 239000001569 carbon dioxide Substances 0.000 claims description 24
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 20
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 18
- 230000008929 regeneration Effects 0.000 claims description 17
- 238000011069 regeneration method Methods 0.000 claims description 17
- 239000001257 hydrogen Substances 0.000 claims description 15
- 229910052739 hydrogen Inorganic materials 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 229910001868 water Inorganic materials 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 13
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 10
- 229910052757 nitrogen Inorganic materials 0.000 claims description 10
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 8
- 229910052786 argon Inorganic materials 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 3
- JYIBXUUINYLWLR-UHFFFAOYSA-N aluminum;calcium;potassium;silicon;sodium;trihydrate Chemical compound O.O.O.[Na].[Al].[Si].[K].[Ca] JYIBXUUINYLWLR-UHFFFAOYSA-N 0.000 claims description 3
- 229910001603 clinoptilolite Inorganic materials 0.000 claims description 3
- DOTMOQHOJINYBL-UHFFFAOYSA-N molecular nitrogen;molecular oxygen Chemical compound N#N.O=O DOTMOQHOJINYBL-UHFFFAOYSA-N 0.000 claims description 3
- ADWQNXMVZMCRRO-UHFFFAOYSA-N methanone;hydrate Chemical compound O.O=[C] ADWQNXMVZMCRRO-UHFFFAOYSA-N 0.000 claims 2
- 238000004140 cleaning Methods 0.000 description 18
- 238000000746 purification Methods 0.000 description 12
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 9
- 239000003463 adsorbent Substances 0.000 description 8
- 239000004215 Carbon black (E152) Substances 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 3
- 239000000446 fuel Substances 0.000 description 3
- 229930195733 hydrocarbon Natural products 0.000 description 3
- 150000002430 hydrocarbons Chemical class 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 101150079116 MT-CO1 gene Proteins 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000004870 electrical engineering Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000011089 mechanical engineering Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/04—Purification or separation of nitrogen
- C01B21/0405—Purification or separation processes
- C01B21/0433—Physical processing only
- C01B21/045—Physical processing only by adsorption in solids
- C01B21/0455—Physical processing only by adsorption in solids characterised by the adsorbent
- C01B21/0466—Zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B23/00—Noble gases; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
- C01B3/506—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification at low temperatures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
- C01B3/56—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
- C01B2203/042—Purification by adsorption on solids
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
- C01B2203/0465—Composition of the impurity
- C01B2203/047—Composition of the impurity the impurity being carbon monoxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
- C01B2203/0465—Composition of the impurity
- C01B2203/0475—Composition of the impurity the impurity being carbon dioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
- C01B2203/0465—Composition of the impurity
- C01B2203/0495—Composition of the impurity the impurity being water
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0043—Impurity removed
- C01B2210/005—Carbon monoxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0043—Impurity removed
- C01B2210/0051—Carbon dioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2210/00—Purification or separation of specific gases
- C01B2210/0043—Impurity removed
- C01B2210/0062—Water
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Combustion & Propulsion (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Separation Of Gases By Adsorption (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Hydrogen, Water And Hydrids (AREA)
- Industrial Gases (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU752197896A SU603414A1 (ru) | 1975-12-15 | 1975-12-15 | Способ очистки газов от окиси углерода, двуокиси углерода и воды |
| SU752197897A SU603415A1 (ru) | 1975-12-15 | 1975-12-15 | Способ очистки газов от окиси углерода, двуокиси углерода и воды |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2656633A1 true DE2656633A1 (de) | 1977-06-23 |
Family
ID=26665570
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19762656633 Withdrawn DE2656633A1 (de) | 1975-12-15 | 1976-12-14 | Verfahren zur reinigung von gasgemischen |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5296975A (enExample) |
| AT (1) | AT366293B (enExample) |
| CH (1) | CH623748A5 (enExample) |
| DD (1) | DD129065A1 (enExample) |
| DE (1) | DE2656633A1 (enExample) |
| FR (1) | FR2335258A1 (enExample) |
| GB (1) | GB1551348A (enExample) |
| IT (1) | IT1074221B (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2506745A1 (fr) * | 1981-05-28 | 1982-12-03 | Toyo Soda Mfg Co Ltd | Article en zeolite modifiee agglomeree |
| EP0078966A3 (en) * | 1981-11-05 | 1983-07-27 | Bayer Ag | Molecular sieve of zeolite for the production of hydrogen by pressure-swing adsorption |
| EP0124737A3 (en) * | 1983-04-11 | 1987-04-29 | Degussa Aktiengesellschaft | Granules of a-type zeolite bonded by magnesium silicates, process for their production and their use |
| EP0124736A3 (en) * | 1983-04-11 | 1987-04-29 | Degussa Aktiengesellschaft | Granules of zeolite bonded by silicates, process for their production and their use |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5922625A (ja) * | 1982-07-27 | 1984-02-04 | Osaka Oxgen Ind Ltd | 一酸化炭素ガス及び窒素ガスを含む混合ガスより窒素ガスを吸着法により除去する方法 |
| US4481018A (en) * | 1982-11-15 | 1984-11-06 | Air Products And Chemicals, Inc. | Polyvalent ion exchanged adsorbent for air separation |
| CA1252451A (en) * | 1984-07-04 | 1989-04-11 | Taisuke Nishida | Method of separating carbon monoxide and carbon monoxide adsorbent used in this method |
| US6248684B1 (en) | 1992-11-19 | 2001-06-19 | Englehard Corporation | Zeolite-containing oxidation catalyst and method of use |
| US5531808A (en) * | 1994-12-23 | 1996-07-02 | The Boc Group, Inc. | Removal of carbon dioxide from gas streams |
| JP3634115B2 (ja) * | 1997-05-23 | 2005-03-30 | 大陽日酸株式会社 | ガス精製方法及び装置 |
| JPH1157371A (ja) * | 1997-08-11 | 1999-03-02 | Taiyo Toyo Sanso Co Ltd | 超清浄空気の製造方法 |
| FR2773499B1 (fr) * | 1998-01-14 | 2000-02-11 | Air Liquide | Procede de purification par adsorption de l'air avant distillation cryogenique |
| US6074973A (en) * | 1998-03-20 | 2000-06-13 | Engelhard Corporation | Catalyzed hydrocarbon trap material and method of making the same |
| US6302943B1 (en) * | 1999-11-02 | 2001-10-16 | Air Products And Chemicals, Inc. | Optimum adsorbents for H2 recovery by pressure and vacuum swing absorption |
| EP1142622B1 (en) * | 2000-04-04 | 2006-06-21 | Tosoh Corporation | Method of adsorptive separation of carbon dioxide |
| FR2832141B1 (fr) * | 2001-11-14 | 2004-10-01 | Ceca Sa | Procede de purification de gaz de synthese |
| EP2628521A1 (fr) | 2012-02-14 | 2013-08-21 | Air Liquide Medical G.m.b.H. | Installation de production sur site de gaz médical utilisant une électrovanne 3-voies reliée à une ligne de purge |
| EP2628523A1 (fr) | 2012-02-14 | 2013-08-21 | Air Liquide Medical G.m.b.H. | Installation de production sur site de gaz médical et procédé de pilotage associé |
| EP2628522A1 (fr) | 2012-02-14 | 2013-08-21 | Air Liquide Medical G.m.b.H. | Installation de production sur site de gaz médical à plusieurs capacités en série et ligne de purge |
| EP2628524B1 (fr) | 2012-02-14 | 2019-05-29 | Air Liquide Medical G.m.b.H. | Installation de production sur site de gaz médical |
| CA2829065A1 (en) | 2013-09-27 | 2015-03-27 | Vitalaire Canada Inc. | On-site medical gas production plant and associated operating method |
| CA2829060C (en) | 2013-09-27 | 2015-02-03 | Vitalaire Canada Inc. | On-site medical gas production plant and associated operating method |
| CA2863543C (en) | 2014-09-11 | 2015-11-03 | Vitalaire Canada Inc. | On-site medical gas production plant and associated operating method |
| EP3858477A4 (en) * | 2018-09-25 | 2022-06-29 | Sekisui Chemical Co., Ltd. | Method for reusing zeolite adsorbent, and regenerated adsorbent |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4830686A (enExample) * | 1971-08-24 | 1973-04-23 | ||
| US3885927A (en) * | 1974-02-05 | 1975-05-27 | Union Carbide Corp | Process for removing carbon dioxide from gas streams |
-
1976
- 1976-11-24 CH CH1478776A patent/CH623748A5/de not_active IP Right Cessation
- 1976-12-14 FR FR7637639A patent/FR2335258A1/fr active Granted
- 1976-12-14 DE DE19762656633 patent/DE2656633A1/de not_active Withdrawn
- 1976-12-14 GB GB5206276A patent/GB1551348A/en not_active Expired
- 1976-12-15 AT AT0927376A patent/AT366293B/de not_active IP Right Cessation
- 1976-12-15 DD DD19637976A patent/DD129065A1/xx unknown
- 1976-12-15 IT IT5262776A patent/IT1074221B/it active
- 1976-12-15 JP JP15066876A patent/JPS5296975A/ja active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2506745A1 (fr) * | 1981-05-28 | 1982-12-03 | Toyo Soda Mfg Co Ltd | Article en zeolite modifiee agglomeree |
| EP0078966A3 (en) * | 1981-11-05 | 1983-07-27 | Bayer Ag | Molecular sieve of zeolite for the production of hydrogen by pressure-swing adsorption |
| US4477267A (en) * | 1981-11-05 | 1984-10-16 | Bayer Aktiengesellschaft | Molecular sieve zeolite for producing hydrogen by pressure variation adsorption technique |
| EP0124737A3 (en) * | 1983-04-11 | 1987-04-29 | Degussa Aktiengesellschaft | Granules of a-type zeolite bonded by magnesium silicates, process for their production and their use |
| EP0124736A3 (en) * | 1983-04-11 | 1987-04-29 | Degussa Aktiengesellschaft | Granules of zeolite bonded by silicates, process for their production and their use |
Also Published As
| Publication number | Publication date |
|---|---|
| DD129065A1 (de) | 1977-12-28 |
| IT1074221B (it) | 1985-04-17 |
| FR2335258A1 (fr) | 1977-07-15 |
| GB1551348A (en) | 1979-08-30 |
| ATA927376A (de) | 1981-08-15 |
| FR2335258B1 (enExample) | 1980-03-28 |
| AT366293B (de) | 1982-03-25 |
| CH623748A5 (en) | 1981-06-30 |
| JPS5296975A (en) | 1977-08-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| 8139 | Disposal/non-payment of the annual fee |