DE2544363A1 - Verfahren zur behandlung einer dextroseloesung - Google Patents
Verfahren zur behandlung einer dextroseloesungInfo
- Publication number
- DE2544363A1 DE2544363A1 DE19752544363 DE2544363A DE2544363A1 DE 2544363 A1 DE2544363 A1 DE 2544363A1 DE 19752544363 DE19752544363 DE 19752544363 DE 2544363 A DE2544363 A DE 2544363A DE 2544363 A1 DE2544363 A1 DE 2544363A1
- Authority
- DE
- Germany
- Prior art keywords
- dextrose
- solution
- isomerization
- resin
- heavy metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 26
- 238000011282 treatment Methods 0.000 title description 15
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 66
- 238000006317 isomerization reaction Methods 0.000 claims description 64
- 239000008121 dextrose Substances 0.000 claims description 56
- 239000011347 resin Substances 0.000 claims description 38
- 229920005989 resin Polymers 0.000 claims description 38
- 229910001385 heavy metal Inorganic materials 0.000 claims description 36
- 150000002500 ions Chemical class 0.000 claims description 32
- 229920002472 Starch Polymers 0.000 claims description 20
- 235000019698 starch Nutrition 0.000 claims description 20
- 239000008107 starch Substances 0.000 claims description 20
- DSLZVSRJTYRBFB-LLEIAEIESA-N D-glucaric acid Chemical compound OC(=O)[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O DSLZVSRJTYRBFB-LLEIAEIESA-N 0.000 claims description 14
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 14
- 229960002737 fructose Drugs 0.000 claims description 14
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 10
- 239000003729 cation exchange resin Substances 0.000 claims description 8
- 229920001429 chelating resin Polymers 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 8
- 108090000769 Isomerases Proteins 0.000 claims description 5
- 102000004195 Isomerases Human genes 0.000 claims description 5
- 238000005341 cation exchange Methods 0.000 claims description 3
- 230000002255 enzymatic effect Effects 0.000 claims description 3
- 230000005484 gravity Effects 0.000 claims 1
- 239000000758 substrate Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 37
- 239000007788 liquid Substances 0.000 description 29
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 21
- 229940088598 enzyme Drugs 0.000 description 17
- 102000004190 Enzymes Human genes 0.000 description 16
- 108090000790 Enzymes Proteins 0.000 description 16
- 108700040099 Xylose isomerases Proteins 0.000 description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 14
- 150000001768 cations Chemical class 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 239000011521 glass Substances 0.000 description 9
- 239000011701 zinc Substances 0.000 description 9
- 239000011133 lead Substances 0.000 description 8
- 239000003957 anion exchange resin Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- 239000007858 starting material Substances 0.000 description 7
- 229910052725 zinc Inorganic materials 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- 210000004027 cell Anatomy 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 150000003839 salts Chemical group 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 description 4
- 239000003456 ion exchange resin Substances 0.000 description 4
- 229920003303 ion-exchange polymer Polymers 0.000 description 4
- 229910052745 lead Inorganic materials 0.000 description 4
- 230000000813 microbial effect Effects 0.000 description 4
- 239000011707 mineral Substances 0.000 description 4
- 235000010755 mineral Nutrition 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 108090000637 alpha-Amylases Proteins 0.000 description 3
- 102000004139 alpha-Amylases Human genes 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- 239000013522 chelant Substances 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 239000006188 syrup Substances 0.000 description 3
- 235000020357 syrup Nutrition 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- 102100022624 Glucoamylase Human genes 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 description 2
- 229940024171 alpha-amylase Drugs 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 238000003926 complexometric titration Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 238000011069 regeneration method Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- CHRJZRDFSQHIFI-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;styrene Chemical compound C=CC1=CC=CC=C1.C=CC1=CC=CC=C1C=C CHRJZRDFSQHIFI-UHFFFAOYSA-N 0.000 description 1
- FBEHFRAORPEGFH-UHFFFAOYSA-N Allyxycarb Chemical compound CNC(=O)OC1=CC(C)=C(N(CC=C)CC=C)C(C)=C1 FBEHFRAORPEGFH-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229920002261 Corn starch Polymers 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- 102000016943 Muramidase Human genes 0.000 description 1
- 108010014251 Muramidase Proteins 0.000 description 1
- 108010062010 N-Acetylmuramoyl-L-alanine Amidase Proteins 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 241000187134 Streptomyces olivochromogenes Species 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000000274 adsorptive effect Effects 0.000 description 1
- 229910052728 basic metal Inorganic materials 0.000 description 1
- -1 basic metal ions Chemical class 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 229940023913 cation exchange resins Drugs 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 210000004748 cultured cell Anatomy 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 150000004676 glycans Polymers 0.000 description 1
- 239000001963 growth medium Substances 0.000 description 1
- 239000000413 hydrolysate Substances 0.000 description 1
- NBZBKCUXIYYUSX-UHFFFAOYSA-N iminodiacetic acid Chemical compound OC(=O)CNCC(O)=O NBZBKCUXIYYUSX-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000002198 insoluble material Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000006166 lysate Substances 0.000 description 1
- 229960000274 lysozyme Drugs 0.000 description 1
- 239000004325 lysozyme Substances 0.000 description 1
- 235000010335 lysozyme Nutrition 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 150000004804 polysaccharides Polymers 0.000 description 1
- 239000005373 porous glass Substances 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/06—Glucose; Glucose-containing syrups obtained by saccharification of starch or raw materials containing starch
- C13K1/08—Purifying
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Peptides Or Proteins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP49113998A JPS5141450A (en) | 1974-10-04 | 1974-10-04 | Iseikatoyobudotoganjueki no shorihoho |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2544363A1 true DE2544363A1 (de) | 1976-04-15 |
Family
ID=14626488
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752544363 Withdrawn DE2544363A1 (de) | 1974-10-04 | 1975-10-03 | Verfahren zur behandlung einer dextroseloesung |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4100025A (enExample) |
| JP (1) | JPS5141450A (enExample) |
| BE (1) | BE834156A (enExample) |
| CA (1) | CA1060825A (enExample) |
| DE (1) | DE2544363A1 (enExample) |
| ES (1) | ES441495A1 (enExample) |
| FR (1) | FR2286669A1 (enExample) |
| GB (1) | GB1500828A (enExample) |
| IT (1) | IT1043112B (enExample) |
| NL (1) | NL7511690A (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5451847A (en) * | 1977-09-30 | 1979-04-24 | Ricoh Co Ltd | Direct recorder |
| US4288548A (en) * | 1979-11-15 | 1981-09-08 | Standard Brands Incorporated | Process for isomerizing glucose to fructose |
| JPS6049479B2 (ja) * | 1981-03-19 | 1985-11-01 | 東レ株式会社 | グルコ−スイソメラ−ゼ失活防止材およびグルコ−ス異性化反応方法 |
| DE3148603C1 (de) * | 1981-12-09 | 1983-07-21 | Kali-Chemie Ag, 3000 Hannover | Verfahren und Anlage zur Herstellung von Isomerose |
| JPH02139576A (ja) * | 1988-07-26 | 1990-05-29 | Seiko Epson Corp | 湿式記録装置 |
| US5893947A (en) * | 1997-05-09 | 1999-04-13 | Advanced Separation Technologies Incorporated | Process for purifying sugar solutions |
| US20110189342A1 (en) * | 2010-02-01 | 2011-08-04 | Jeong Hea-Seok | High-purity galactooligosaccharides and uses thereof |
| US20130172546A1 (en) * | 2011-12-30 | 2013-07-04 | Renmatix, Inc. | Compositions comprising c5 and c6 oligosaccharides |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2606847A (en) * | 1949-08-06 | 1952-08-12 | Corn Prod Refining Co | Process for the production of dextrose |
| US2994669A (en) * | 1959-08-28 | 1961-08-01 | Wolfen Filmfab Veb | Process for the production of modified phenylene diamine ion exchange resins |
| FR95980E (fr) * | 1967-10-04 | 1972-05-19 | Corn Products Co | Sirop amélioré contenant du dextrose, du lévulose et du maltose, et son procédé de préparation. |
| US3909354A (en) * | 1970-11-09 | 1975-09-30 | Standard Brands Inc | Process for isomerizing glucose to fructose |
| US3755084A (en) * | 1971-06-23 | 1973-08-28 | J Feder | Process for the preparation of apoenzyme |
| JPS5641233B2 (enExample) * | 1972-09-05 | 1981-09-26 | ||
| US3910821A (en) * | 1972-10-04 | 1975-10-07 | Cpc International Inc | Enzymatic isomerization product |
| US3982997A (en) * | 1974-09-18 | 1976-09-28 | Corning Glass Works | Immobilized glucose isomerase |
-
1974
- 1974-10-04 JP JP49113998A patent/JPS5141450A/ja active Granted
-
1975
- 1975-09-30 US US05/618,090 patent/US4100025A/en not_active Expired - Lifetime
- 1975-10-03 IT IT27944/75A patent/IT1043112B/it active
- 1975-10-03 CA CA236,990A patent/CA1060825A/en not_active Expired
- 1975-10-03 DE DE19752544363 patent/DE2544363A1/de not_active Withdrawn
- 1975-10-03 GB GB40678/75A patent/GB1500828A/en not_active Expired
- 1975-10-03 FR FR7530453A patent/FR2286669A1/fr not_active Withdrawn
- 1975-10-03 ES ES441495A patent/ES441495A1/es not_active Expired
- 1975-10-03 NL NL7511690A patent/NL7511690A/xx not_active Application Discontinuation
- 1975-10-03 BE BE2054600A patent/BE834156A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IT1043112B (it) | 1980-02-20 |
| CA1060825A (en) | 1979-08-21 |
| ES441495A1 (es) | 1977-04-01 |
| FR2286669A1 (fr) | 1976-04-30 |
| GB1500828A (en) | 1978-02-15 |
| JPS5141450A (en) | 1976-04-07 |
| NL7511690A (nl) | 1976-04-06 |
| JPS5649118B2 (enExample) | 1981-11-19 |
| BE834156A (fr) | 1976-04-05 |
| US4100025A (en) | 1978-07-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8130 | Withdrawal |