DE253426C - - Google Patents

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Publication number
DE253426C
DE253426C DENDAT253426D DE253426DA DE253426C DE 253426 C DE253426 C DE 253426C DE NDAT253426 D DENDAT253426 D DE NDAT253426D DE 253426D A DE253426D A DE 253426DA DE 253426 C DE253426 C DE 253426C
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DE
Germany
Prior art keywords
petroleum
substances
starchy
water
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
DENDAT253426D
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German (de)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Publication of DE253426C publication Critical patent/DE253426C/de
Priority claimed from US50268A external-priority patent/US1704446A/en
Active legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M175/00Working-up used lubricants to recover useful products ; Cleaning
    • C10M175/0008Working-up used lubricants to recover useful products ; Cleaning with the use of adsorbentia
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L7/00Fuels produced by solidifying fluid fuels
    • C10L7/02Fuels produced by solidifying fluid fuels liquid fuels
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M171/00Lubricating compositions characterised by purely physical criteria, e.g. containing as base-material, thickener or additive, ingredients which are characterised exclusively by their numerically specified physical properties, i.e. containing ingredients which are physically well-defined but for which the chemical nature is either unspecified or only very vaguely indicated
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04Elements
    • C10M2201/041Carbon; Graphite; Carbon black
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04Elements
    • C10M2201/041Carbon; Graphite; Carbon black
    • C10M2201/042Carbon; Graphite; Carbon black halogenated, i.e. graphite fluoride
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06Metal compounds
    • C10M2201/063Peroxides
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10Compounds containing silicon
    • C10M2201/102Silicates
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02Hydroxy compounds
    • C10M2207/021Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/022Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/12Polysaccharides, e.g. cellulose, biopolymers
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00Metal present as such or in compounds
    • C10N2010/04Groups 2 or 12

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Materials Engineering (AREA)
  • Lubricants (AREA)
  • Solid Fuels And Fuel-Associated Substances (AREA)

Description

KAISERLICHESIMPERIAL

PATENTAMT.PATENT OFFICE.

PATENTSCHRIFTPATENT LETTERING

- M 253426 KLASSE 10*. GRUPPE- M 253426 CLASS 10 *. GROUP

CHARLES GERARD in CUREGHEM-BRÜSSELCHARLES GERARD in CUREGHEM BRUSSELS

stärkehaltigen Stoffen.starchy substances.

Patentiert im Deutschen Reiche vom 23. Januar 1912 ab.Patented in the German Empire on January 23, 1912.

Die Erfindung bezweckt, das bekannte Verfahren zu verbessern, nach dem ein künstlicher, für sich zu verwendender oder mit anderen Brennstoffen zu brikettierender Brennstoff aus Petroleum und stärkehaltigen Stoffen erzeugt wird. · The aim of the invention is to improve the known method according to which an artificial fuel, which is to be used by itself or to be briquetted with other fuels, is produced from petroleum and starch-containing substances. ·

Bei dem bekannten Verfahren wird der Kleister kalt bereitet und ganz in der Kälte gearbeitet. Eine bessere Wirkung, besondersIn the known method, the paste is prepared cold and completely in the cold worked. Better effect, especially

ίο hinsichtlich des Stehens des Brennstoffs im Feuer, soll gemäß der Erfindung dadurch erzielt werden, daß die stärkehaltigen Stoffe mit dem Petroleum unter Zulaß heißen Wassers gemischt werden.ίο regarding the standing of the fuel in the Fire, is to be achieved according to the invention in that the starchy substances be mixed with the kerosene with the admission of hot water.

Wenn man im Augenblicke der Versteifung des Petroleums durch die stärkehaltigen Stoffe eine gewisse Menge heißen, zweckmäßig zum Sieden gebrachten Wassers zuführt, quellen unter der Einwirkung des kochenden Wassers die Stärkekörner auf, so daß diese dadurch befähigt werden, das aufgenommene Wasser und Petroleum festzuhalten. Nach dem Erkalten verdickt sich die Masse, und weder das Wiedererhitzen in dem zur Herstellung der Briketts verwendeten Mischer noch die Hitze des Verbrennungsherdes bewirken eine Wiederverflüssigung des Petroleums, d.h. also seine Austreibung aus den Stärkekörnern, durch welche es eingehüllt ist. Das Petroleum brennt dann vollständig und ohne jedes Auslaufen ab.At the moment when the petroleum is stiffened by the starchy substances add a certain amount of hot water, suitably brought to the boil, swell under the action of the boiling water, the starch grains, so that this thereby be able to hold on to the absorbed water and petroleum. After cooling down the mass thickens, and neither the reheating in which to produce the Briquettes used mixers nor the heat of the combustion stove cause reliquefaction of petroleum, i.e. its expulsion from the starch grains which it is enveloped. The kerosene then burns completely and without any leakage away.

Zur Ausführung des Verfahrens verfährt man zweckmäßig in folgender Weise:To carry out the process, it is advisable to proceed as follows:

Das Rohpetroleum wird in einem mit Dampf geheizten Behälter auf eine geeignete Temperatur, beispielsweise 25 bis 30 ° C, erwärmt..The crude petroleum is heated to a suitable temperature in a steam-heated container. for example 25 to 30 ° C, heated ..

In einem zweiten Behälter wird Wasser auf der Siedetemperatur erhalten.In a second container, water is obtained at the boiling point.

Ein dritter Behälter enthält das als Aufsaugmasse dienende stärkehaltige Gut.A third container contains the starchy material used as an absorbent material.

Aus dem dritten Behälter läßt man eine gewisse Menge der stärkehaltigen Stoffe in einen mit einem Rührer versehenen Mischer. Während der Rührer in Tätigkeit ist, läuft durch Verbindungsrohre aus den beiden anderen Behältern eine gewisse Menge Petroleum und kochendes Wasser zu. Man fügt alsdann nacheinander in geeigneten Mengen stärkehaltige Stoffe, Petroleum und kochendes Wasser hinzu. Wenn die Mischung genügend innig ist, entfernt man sie aus dem Mischer und erhält so ein mehr oder minder dickes Erzeugnis, das sich beim Erkalten verfestigt und entweder unmittelbar als Brennstoff verwendet oder nach einem der bekannten Verfahren mit anderen Stoffen zur Herstellung von Briketts gemischt werden kann. So kann man zur Mischung, wie bereits bekannt, Stearin-, Palmitin-, Ölsäure oder andere Rückstände hinzufügen.A certain amount of the starchy substances is allowed in from the third container a mixer equipped with a stirrer. While the stirrer is in operation, runs a certain amount of petroleum through connecting pipes from the other two containers and boiling water too. Then add starchy products one after the other in suitable quantities Add fabrics, petroleum and boiling water. When the mixture is sufficiently intimate, remove it from the mixer and This gives a more or less thick product that solidifies when it cools and either used directly as fuel or by one of the known methods can be mixed with other substances to make briquettes. So you can, as already known, to the mixture Add stearic, palmitic, oleic acid or other residue.

Nach einem Ausführungsbeispiel der Erfindung kann man zur Herstellung von 100 kg Mischung in folgender Weise verfahren:According to an embodiment of the invention you can proceed as follows to produce 100 kg of mixture:

Man gießt in den Mischer 10 kg Mehl (von Roggen, Weizen, Spelz o. dgl.) oder ein sonstiges stärkehaltiges Gut und setzt das Rühr-Pour 10 kg of flour (from rye, wheat, spelled or the like) or something else into the mixer starchy goods and sets the stirring

werk in Bewegung. Alsdann läßt man auf dieses Mehl kochendes Wasser so lange fließen, bis man eine Masse von der Konsistenz weicher Seife erhält. Man fährt dann mit dem Mischen fort, bis die ganze Masse vollkommen gleichförmig ist. In diesem Augenblick läßt man auf 25 bis 30 ° C. erwärmtes Petroleum in dünnem Strahl in die Masse einfließen, und zwar in einer derartigen Menge, daß es in dem Maße, wie es eintritt, absorbiert wird. Man öffnet dann das Dampfventil des Mischers zwecks Wiedererhitzung des Breies und Aufquellens der Stärkekörner. Von Zeit zu Zeit läßt man noch ein wenig kochendes Wasser hinzu (ungefähr 1J2 1).work in motion. Then boiling water is allowed to run on this flour until a mass of the consistency of soft soap is obtained. Mixing is then continued until the whole mass is perfectly uniform. At this moment petroleum warmed to 25 to 30 ° C. is allowed to flow into the mass in a thin stream, in such an amount that it is absorbed as it occurs. The steam valve of the mixer is then opened to reheat the pulp and swell the starch granules. From time to time a little boiling water is added (about 1 J 2 1).

Dies kann fortgeführt werden, bis die Petroleummenge ihr Maximum erreicht hat. Für die Mischung mit festen Brennstoffen bis zum Verhältnis von 1:3 nimmt man eine Paste aus 10 kg Mehl, 10 bis 15 kg Wasser und 75 kg Petroleum.-,This can continue until the amount of petroleum has reached its maximum. For the mixture with solid fuels up to the ratio of 1: 3 one takes a paste from 10 kg of flour, 10 to 15 kg of water and 75 kg petroleum.

Handelt es sich um eine Mischung, die ohne weiteres als Brennstoff dienen soll, so muß man die oben angegebene Mehlmenge mindestens verdoppeln und bei Beendigung des Mischens ίο bis 15 Prozent Rückstände von Stearin-, öl-, Palmitinsäure usw., d. h. also Stoffen, die beim Erkalten erstarren, sowie 15 bis 20 Prozent Koksstaub hinzufügen.If it is a mixture that is intended to serve as fuel without further ado, then it must you at least double the amount of flour given above and when mixing is complete ίο up to 15 percent residues of stearic, oleic, palmitic acid etc., d. H. so Add substances that solidify when they cool, as well as 15 to 20 percent coke dust.

Die nach dem Verfahren erhaltenen Stoffe sowie die mit den Stoffen hergestellten Briketts sind nicht explosionsgefährlich, da das Petroleum von der Aufsaugmasse vollkommen eingehüllt ist.The substances obtained by the process as well as the briquettes made with the substances are not explosive because the kerosene is completely enveloped by the absorbent material is.

Claims (1)

Patent-An spruch:Patent claim: Verfahren zur Herstellung eines künstlichen, für sich zu verwendenden oder mit anderen Brennstoffen zu brikettierenden Brennstoffs aus Petroleum und stärkehaltigen Stoffen, dadurch gekennzeichnet, daß die stärkehaltigen Stoffe mit dem Petroleum unter Zulaß heißen Wassers verrührt werden.Process for the production of an artificial one, to be used by itself or with other fuels to briquetting petroleum and starchy fuels Substances, characterized in that the starchy substances with the petroleum be stirred while allowing hot water.
DENDAT253426D 1914-04-01 Active DE253426C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB191408279T 1914-04-01
US50268A US1704446A (en) 1925-08-14 1925-08-14 Lubricant and sealing compound

Publications (1)

Publication Number Publication Date
DE253426C true DE253426C (en)

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ID=34379525

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Application Number Title Priority Date Filing Date
DENDAT253426D Active DE253426C (en) 1914-04-01
DENDAT278510D Active DE278510C (en) 1914-04-01

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Application Number Title Priority Date Filing Date
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Country Status (2)

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DE (2) DE278510C (en)
GB (1) GB191408279A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2469438A1 (en) * 1979-11-13 1981-05-22 Ugine Kuhlmann LUBRICANT VARNISH BASED ON GRAPHITE FLUORIDE AND PROCESSES FOR THEIR PREPARATION AND APPLICATION

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GB191408279A (en) 1915-04-01
DE278510C (en)

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