DE2315640C3 - Verfahren zur Herstellung ungesättigter cycloaliphatischer Ketone und dabei gebildete cycloaliphatische Diketone und deren Enolate - Google Patents

Verfahren zur Herstellung ungesättigter cycloaliphatischer Ketone und dabei gebildete cycloaliphatische Diketone und deren Enolate

Info

Publication number
DE2315640C3
DE2315640C3 DE2315640A DE2315640A DE2315640C3 DE 2315640 C3 DE2315640 C3 DE 2315640C3 DE 2315640 A DE2315640 A DE 2315640A DE 2315640 A DE2315640 A DE 2315640A DE 2315640 C3 DE2315640 C3 DE 2315640C3
Authority
DE
Germany
Prior art keywords
spectrum
trimethyl
solution
cyclohex
cycloaliphatic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE2315640A
Other languages
German (de)
English (en)
Other versions
DE2315640A1 (de
DE2315640B2 (de
Inventor
Karl-Heinrich Dr. Onex Schulte-Elte (Schweiz)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Firmenich SA
Original Assignee
Firmenich SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Firmenich SA filed Critical Firmenich SA
Publication of DE2315640A1 publication Critical patent/DE2315640A1/de
Publication of DE2315640B2 publication Critical patent/DE2315640B2/de
Application granted granted Critical
Publication of DE2315640C3 publication Critical patent/DE2315640C3/de
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20—Synthetic spices, flavouring agents or condiments
    • A23L27/203—Alicyclic compounds
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/34—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a carbocyclic ring other than a six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
    • C07C403/18—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/42—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/64—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of functional groups containing oxygen only in singly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/527—Unsaturated compounds containing keto groups bound to rings other than six-membered aromatic rings
    • C07C49/543—Unsaturated compounds containing keto groups bound to rings other than six-membered aromatic rings to a six-membered ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/527—Unsaturated compounds containing keto groups bound to rings other than six-membered aromatic rings
    • C07C49/557—Unsaturated compounds containing keto groups bound to rings other than six-membered aromatic rings having unsaturation outside the rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/527—Unsaturated compounds containing keto groups bound to rings other than six-membered aromatic rings
    • C07C49/573—Unsaturated compounds containing keto groups bound to rings other than six-membered aromatic rings containing hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D261/00—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings
    • C07D261/02—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings
    • C07D261/06—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having two or more double bonds between ring members or between ring members and non-ring members
    • C07D261/08—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having two or more double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Seasonings (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Medicinal Preparation (AREA)
  • Fodder In General (AREA)
  • Confectionery (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
DE2315640A 1972-03-30 1973-03-29 Verfahren zur Herstellung ungesättigter cycloaliphatischer Ketone und dabei gebildete cycloaliphatische Diketone und deren Enolate Expired DE2315640C3 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH477072A CH561676A5 (US20020128544A1-20020912-P00008.png) 1972-03-30 1972-03-30

Publications (3)

Publication Number Publication Date
DE2315640A1 DE2315640A1 (de) 1973-10-11
DE2315640B2 DE2315640B2 (de) 1979-11-15
DE2315640C3 true DE2315640C3 (de) 1980-07-24

Family

ID=4282232

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2315640A Expired DE2315640C3 (de) 1972-03-30 1973-03-29 Verfahren zur Herstellung ungesättigter cycloaliphatischer Ketone und dabei gebildete cycloaliphatische Diketone und deren Enolate

Country Status (7)

Country Link
US (1) US3923896A (US20020128544A1-20020912-P00008.png)
JP (1) JPS5346834B2 (US20020128544A1-20020912-P00008.png)
CH (1) CH561676A5 (US20020128544A1-20020912-P00008.png)
DE (1) DE2315640C3 (US20020128544A1-20020912-P00008.png)
FR (1) FR2178221A1 (US20020128544A1-20020912-P00008.png)
GB (1) GB1391736A (US20020128544A1-20020912-P00008.png)
NL (1) NL7304365A (US20020128544A1-20020912-P00008.png)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4144199A (en) 1974-02-22 1979-03-13 Naarden International, N.V. Safranic acid ester perfume compositions
US4062894A (en) * 1976-08-11 1977-12-13 International Flavors & Fragrances Inc. Derivatives of 1-acetyl-3,3-dimethylcyclohexane
JPS52167819U (US20020128544A1-20020912-P00008.png) * 1976-06-14 1977-12-20
JPS537948A (en) * 1976-07-08 1978-01-24 Oiles Industry Co Ltd Automatic window opening and closing device
US4119576A (en) * 1976-11-11 1978-10-10 International Flavors & Fragrances Inc. Perfume compositions and colognes containing 1-butanoyl-3,3-dimethylcyclohexane
US4157351A (en) * 1978-03-17 1979-06-05 International Flavors & Fragrances Inc. 1-(2,6,6-Trimethyl-1,3-cyclohexadien-1-yl)-1,3-butanedione and organoleptic uses thereof
CA1102816A (en) * 1978-01-27 1981-06-09 Braja D. Mookherjee Cyclohexadien-1-yl-1-butanone derivatives, process for preparing same and organoleptic uses thereof
DE2807584C3 (de) * 1978-02-22 1981-05-07 Dragoco Gerberding & Co Gmbh, 3450 Holzminden Fixateur für Parfümkompositionen
US4271853A (en) * 1978-03-17 1981-06-09 International Flavors & Fragrances Inc. Use for augmenting or enhancing the aroma and taste of smoking tobacco and smoking tobacco articles by adding thereto 1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-1,3-butanedione
US4235247A (en) * 1978-09-15 1980-11-25 International Flavors & Fragrances Inc. Organoleptic uses of 3-hydroxy-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-1-butanone
US4228026A (en) 1979-05-15 1980-10-14 International Flavors & Fragrances Inc. 3-Hydroxy-1-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-1-butanone in detergents
US4301018A (en) * 1979-06-07 1981-11-17 International Flavors & Fragrances Inc. Use of cyclic chemical compounds for augmenting or enhancing the aroma of fabric softener articles
US4284654A (en) * 1979-10-26 1981-08-18 International Flavors & Fragrances Inc. Use of 1-hydroxy-1-ethynyl-2,2,6-trimethyl cyclohexane in augmenting or enhancing the aroma or taste of foodstuffs
JPS58135283A (ja) * 1982-02-06 1983-08-11 植村　厚一 開口部の遮閉防護方法及びその装置
EP0096243B1 (de) * 1982-06-03 1985-08-07 L. GIVAUDAN & CIE Société Anonyme Cyclohex(en)ylmethanole und ihre Ester, mit Riechstoffeigenschaften
US4481372A (en) * 1982-09-30 1984-11-06 International Flavors & Fragrances Inc. Process for preparing allyl alpha and beta ionones and intermediates therefor
US4458093A (en) * 1983-05-20 1984-07-03 International Flavors & Fragrances Inc. Hexadienoyl cyclohexene derivative
US4868339A (en) * 1987-09-23 1989-09-19 Basf K & F Corporation Alkyltetramethylcyclohexane derivatives and their use as perfumes
CN105985258B (zh) * 2015-01-29 2019-08-02 上海彩迩文生化科技有限公司 一种苯甲酰胺化合物的制备方法及其中间体

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2507647A (en) * 1950-05-16 Synthesis of
US2449956A (en) * 1945-07-09 1948-09-21 Shell Dev Dialkylcyclohexyl glycols and certain derivatives thereof
US2742503A (en) * 1951-11-02 1956-04-17 Du Pont Production of imino substituted acetones and their hydrolysis to substituted acetones
US2773099A (en) * 1954-09-03 1956-12-04 Stork Gilbert Method for the preparation of alpha-substituted organic carbonyl compounds
US3268589A (en) * 1963-05-29 1966-08-23 Reynolds Tobacco Co R Process for preparing 4-(2-butenylidene)-3, 5, 5-trimethyl-2-cyclohexene-1-one
US3499938A (en) * 1965-10-11 1970-03-10 Union Oil Co Conversion of ketones to carbinols

Also Published As

Publication number Publication date
JPS5346834B2 (US20020128544A1-20020912-P00008.png) 1978-12-16
DE2315640A1 (de) 1973-10-11
US3923896A (en) 1975-12-02
NL7304365A (US20020128544A1-20020912-P00008.png) 1973-10-02
GB1391736A (en) 1975-04-23
FR2178221A1 (US20020128544A1-20020912-P00008.png) 1973-11-09
DE2315640B2 (de) 1979-11-15
JPS497250A (US20020128544A1-20020912-P00008.png) 1974-01-22
CH561676A5 (US20020128544A1-20020912-P00008.png) 1975-05-15

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Legal Events

Date Code Title Description
C3 Grant after two publication steps (3rd publication)
8339 Ceased/non-payment of the annual fee