DE191113C - - Google Patents
Info
- Publication number
- DE191113C DE191113C DENDAT191113D DE191113DA DE191113C DE 191113 C DE191113 C DE 191113C DE NDAT191113 D DENDAT191113 D DE NDAT191113D DE 191113D A DE191113D A DE 191113DA DE 191113 C DE191113 C DE 191113C
- Authority
- DE
- Germany
- Prior art keywords
- seeds
- cytoplasm
- saponification
- fats
- fat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L Calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 6
- CSNNHWWHGAXBCP-UHFFFAOYSA-L mgso4 Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 6
- 210000000805 Cytoplasm Anatomy 0.000 claims description 5
- 238000007127 saponification reaction Methods 0.000 claims description 5
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 3
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 3
- 235000004443 Ricinus communis Nutrition 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 1
- 235000014593 oils and fats Nutrition 0.000 claims 1
- 239000003925 fat Substances 0.000 description 7
- 239000002253 acid Substances 0.000 description 3
- 230000001264 neutralization Effects 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 239000000243 solution Substances 0.000 description 2
- 241000189705 Dunedin group Species 0.000 description 1
- 230000003213 activating Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
- C11C1/025—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by saponification and release of fatty acids
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT,PATENT OFFICE,
PATENTSCHRIFTPATENT LETTERING
KLASSE 23 d. GRUPPECLASS 23 d. GROUP
MAURICE NICLOUX in PARIS.MAURICE NICLOUX in PARIS.
Die Verwendung von Rizinuskörnern, welche j auf Fette unter Zusatz von Säure wirken, J ist bereits Gegenstand des Patentes 145413.The use of castor grains, which j act on fats with the addition of acid, J is already the subject of patent 145413.
Es erschien demzufolge sehr wohl begründet, anzunehmen, daß die Verseifung der Fette ohne Unterschied, ob sie sämtlichen Bestandteilen der Körner zusammen oder nur dem in diesen enthaltenen Cytoplasma zuzuschreiben ist, einen Säurezusatz erfordert.It therefore seemed very reasonable to assume that the saponification of the Fats regardless of whether they contain all of the components of the grains together or only to the cytoplasm contained in these, requires the addition of acid.
Nach dieser Richtung hin ausgeführte Versuche ergaben, daß ein Säurezusatz nicht notwendig ist; in dieser Erkenntnis bezieht sich die vorliegende Erfindung auf die Verseifung von Fetten mittels ganzer Samenkörner oder des aus ihnen separierten Cytoplasmas unter Zusatz eines neutralen Mittels.Tests carried out in this direction showed that no acid was added necessary is; in this light, the present invention relates to saponification of fats by means of whole seeds or the cytoplasm separated from them with the addition of a neutral agent.
Es genügt, dem Gemisch der Samenkörner oder des Cytoplasmas mit dem Fett an Stelle angesäuerten Wassers eine gesättigte neutrale Lösung von Kalziumsulfat hinzuzufügen, welche in Lösung eine gewisse Menge neutralen Magnesiumsulfats enthält, und deren verhältnismäßiger Betrag mit der Fettmenge variiert, aber niemals mehr als 5 von 1000 Teilen des Fettes beträgt.It is enough to mix the seeds or the cytoplasm with the fat in place add a saturated neutral solution of calcium sulfate to acidified water, which contains a certain amount of neutral magnesium sulfate in solution, and their proportionate amount varies with the amount of fat, but never more than 5 in 1000 Sharing the fat amounts.
Um z. B. innerhalb 24 bis 28 Stunden von 1000 kg Fett 90 Prozent zu spalten, wird vorteilhaft folgende Zusammensetzung gewählt: To z. B. to split 90 percent of 1000 kg of fat within 24 to 28 hours advantageously the following composition is chosen:
Kalziumsulfat wird in 450 bis 500 kg Wasser aufgelöst. Nach dem Auflösen werden 400 kg der gesättigten Lösung abgegossen und letzterer sodann höchstens 5 kg Magnesiumsulfat zugesetzt.Calcium sulfate is dissolved in 450 to 500 kg of water. After dissolving will be Pour off 400 kg of the saturated solution and then add a maximum of 5 kg of magnesium sulfate to the latter.
Unter den angegebenen Verhältnissen findet nicht nur die Verseifung regelmäßig statt, sondern die Salze zeigen auch eine aktivierende Wirkung; sie bewirken eine Verseifung, welche für eine gleiche Menge von Körnern oder Cytoplasma größer ist, als bei Verwendung von ausgesäuertem Wasser erzielt wird.Under the given conditions, not only does saponification take place regularly, but the salts also show an activating effect; they cause saponification, which is greater for an equal amount of grains or cytoplasm than obtained with the use of acidified water will.
Claims (1)
Publications (1)
Publication Number | Publication Date |
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DE191113C true DE191113C (en) |
Family
ID=454529
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DENDAT191113D Active DE191113C (en) |
Country Status (1)
Country | Link |
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DE (1) | DE191113C (en) |
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0
- DE DENDAT191113D patent/DE191113C/de active Active
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