DE166358C - - Google Patents
Info
- Publication number
- DE166358C DE166358C DENDAT166358D DE166358DA DE166358C DE 166358 C DE166358 C DE 166358C DE NDAT166358 D DENDAT166358 D DE NDAT166358D DE 166358D A DE166358D A DE 166358DA DE 166358 C DE166358 C DE 166358C
- Authority
- DE
- Germany
- Prior art keywords
- heliotropin
- process protected
- protocatechualdehyde
- cleavage
- solvents
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 2
- IBGBGRVKPALMCQ-UHFFFAOYSA-N 3,4-dihydroxybenzaldehyde Chemical compound OC1=CC=C(C=O)C=C1O IBGBGRVKPALMCQ-UHFFFAOYSA-N 0.000 claims 2
- 238000003776 cleavage reaction Methods 0.000 claims 1
- 229960003371 protocatechualdehyde Drugs 0.000 claims 1
- 230000007017 scission Effects 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical class OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
- C07C45/673—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by change of size of the carbon skeleton
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Micro-Organisms Or Cultivation Processes Thereof (AREA)
Description
2. Ausführungsform des Verfahrens gemäß Anspruch I, dadurch gekennzeichnet, daß man als Lösungsmittel wässerige Lösungen von Bisulfiten verwendet, welche ohne Zusatz von Säuren auf Heliotropin spaltend wirken.2. Embodiment of the method according to claim I, characterized in that the solvent used is aqueous Solutions of bisulfites are used, which are based on heliotropin without the addition of acids have a divisive effect.
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE166358C true DE166358C (en) |
Family
ID=431758
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT166358D Active DE166358C (en) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE166358C (en) |
-
0
- DE DENDAT166358D patent/DE166358C/de active Active
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