DE1619139A1 - Process for the production of a textile melt - Google Patents

Process for the production of a textile melt

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Publication number
DE1619139A1
DE1619139A1 DE1966P0040527 DEP0040527A DE1619139A1 DE 1619139 A1 DE1619139 A1 DE 1619139A1 DE 1966P0040527 DE1966P0040527 DE 1966P0040527 DE P0040527 A DEP0040527 A DE P0040527A DE 1619139 A1 DE1619139 A1 DE 1619139A1
Authority
DE
Germany
Prior art keywords
carbon atoms
emulsifier
temperature
quaternary ammonium
cationic quaternary
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DE1966P0040527
Other languages
German (de)
Inventor
Lanner Arthur William
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Publication of DE1619139A1 publication Critical patent/DE1619139A1/en
Pending legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/39—Aldehyde resins; Ketone resins; Polyacetals
    • D06M15/423—Amino-aldehyde resins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/372—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing etherified or esterified hydroxy groups ; Polyethers of low molecular weight
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M7/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made of other substances with subsequent freeing of the treated goods from the treating medium, e.g. swelling, e.g. polyolefins
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/02—Water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/26—Amines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/46—Textile oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/015—Dispersions of solid lubricants
    • C10N2050/02—Dispersions of solid lubricants dissolved or suspended in a carrier which subsequently evaporates to leave a lubricant coating
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10—Semi-solids; greasy
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2060/00—Chemical after-treatment of the constituents of the lubricating composition
    • C10N2060/04—Oxidation, e.g. ozonisation
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Paper (AREA)

Description

The Procter & Gamble Company . Cincinnati, Ohio, V.St.A.The Procter & Gamble Company. Cincinnati, Ohio, V.St.A.

Zusatz zur Patentanmeldung P 36 599 Iv"e/8k - unsere jJr.11Addition to patent application P 36 599 Iv "e / 8k - our jJr.11

Verfahren zur Herstellung einer.lextilschmälze Process for the production of an.lextil Schmälze

Die Patentanmeldung P 36 599 I7c/8k betrifft eine Textilschmälze, bestehend aus einer homogenen Wassersuspension eines oxydierten Fischer-Iropsch-Wachses mit einer Kettenlänge von etwa 4G bis etwa 55 Kohlenstoffatomen, einem Schmelzpunkisbereich von etwa 93 bis etwa 104 C,. einer Säurezahl· von etwa 10 bis etwa 35, und einer Durchdringung von etwa 1 bis etwa 6, dieThe patent application P 36 599 I7c / 8k relates to a textile lubricant, consisting of a homogeneous water suspension of an oxidized Fischer-Iropsch wax with one chain length from about 4G to about 55 carbon atoms, a melting point range of from about 93 to about 104 ° C. one Acid number · from about 10 to about 35, and a penetration of about 1 to about 6, the

a) mittels einer kationischen quaternären Ammoniumverbinder formel a) using a cationic quaternary ammonium compound formula

U30)yH.U 3 0) y H.

BAD ORIGINALBATH ORIGINAL

09844/165809844/1658

in welcher JL· eine Älkylgruppe mit 14 bis 20 Kohlenstoffatomen, Rp eine Älkylgruppe mit 1 bis 3 Kohlenstoffatomen, eine Phenyl-, Naphthyl- oder Cj-CU-alkyl-subütituierte Phenylgruppe, iU eine Alkylengruppe mit 2 bis 4 Kohlenstoffatomen, Z~ ein Anion, X plus Y den Wert 1 bis 6 und X den Wert 1 bis 6 bedeutet, oderin which JL an alkyl group with 14 to 20 carbon atoms, Rp is an alkyl group with 1 to 3 carbon atoms, a phenyl, naphthyl or Cj-CU-alkyl-substituted Phenyl group, iU an alkylene group with 2 to 4 carbon atoms, Z ~ is an anion, X plus Y denotes the value 1 to 6 and X denotes the value 1 to 6, or

b) mittels eines Gemisches aus dieser Ammoniumverbindung und j einem nichtionischen Emulgator emulgiert ist, der mindestens etwa 8 Mol Äthylenoxyd enthält, wobei der Gehalt an nichtionischem Emulgator etwa 0 bis etwa 7 Teile auf je 3 Teile Ψ kationischem Emulgator, und das Verhältnis des oxydierten fischer-Tropsch-V/achses zu dem Gesamtemulgator etwa 10:1 bis 3s7 beträgt.b) is emulsified by means of a mixture of this ammonium compound and a nonionic emulsifier which contains at least about 8 moles of ethylene oxide, the content of nonionic emulsifier about 0 to about 7 parts per 3 parts of Ψ cationic emulsifier, and the ratio of the oxidized fischer -Tropsch-V / axis to the total emulsifier is about 10: 1 to 3s7.

Die Schmelzpunktbestimmung erfolgt nach dem allgemeinen Verfahren A.8.T.M. D-127-3chmelzuunKt von Petrolatum und mikrokristallinen V/a cha en. Die Säurezahl ist die Anzahl Milligramm an Kaliumhydroxvd, uie durch die in 1 g ;/aohs ι enthaltene freie Säure neutralisiert .verden. Ihre Bestimmung erfolgt dadurch, daß aian die Probe in heißem Toluol titriert, wobei man Phenolphthalein als Indikator verwendet. Die Bestimmung der Hadeldurehdrin^ung erfolgt nach lern allgemeinen Verfahren A.S.T.il. D-1321 für die Hadel-DurcMringung von Petroleumwachsen. Der nach den Vorschriften von-A.S.T.K* D-217 verwendete Penetrometer wird mit einer Gesamtbelastung von 100 g für die liadel und alles Zubehör eingesetzt. The melting point is determined according to the general method A.8.T.M. D-127-3 Melting point of petrolatum and microcrystalline V / a cha en. The acid number is the number of milligrams of potassium hydroxide, uie by that in 1 g; / aohs ι contained free acid neutralizes .verden. Your destiny takes place by titrating the sample in hot toluene, using phenolphthalein as an indicator. The determination of the urge to drag takes place according to general knowledge Procedure A.S.T.il. D-1321 for the needle penetration of petroleum waxes. According to the regulations of A.S.T.K * D-217 used penetrometer comes with a total load of 100 g used for the liadel and all accessories.

Die Patentanmeldung P 36 599 IVc/8k betrifft außerdem ein Verfahren zur Herstellung einer Cextilschniälzzusaaiiaensetzung, das dadurch, gekennzeichnet ist, daß man (a) ein oxydiertes iPischer-Tropsch-r/achs bei et.^a 104 G schmilzt,The patent application P 36 599 IVc / 8k also concerns a Process for the production of a Cextilschniälzzusaaiiaensetzung, which is characterized in that (a) an oxidized iPischer-Tropsch-r / achs at et. ^ a 104 G melts,

(b) zu der Schmelze einen Smulgator ^ibt unci damit vermischt, (c) das Gemisch auf eine 'Xeraper&tur von etwa 121 bis etwa 143°C erwärmt, (d) das arv.-ümite a-e;.,iacii(b) to the melt a smulsifier ^ ibt unci mixed with it, (c) the mixture to a 'Xeraper & ture of heated about 121 to about 143 ° C, (d) das arv.-ümite a-e;., iacii

9 0 984 U /16589 0 984 U / 1658

BAD OfIiGlNALBATHROOM OFFICIAL

zu V/asser von etwa 80 bis etwa 9O,5°C unter ständig em" ; to water from about 80 to about 90.5 ° C. under constant em ";

üiihren zugibt, und (e) die erhaltene Suspension mit einer Geschwindigkeit von aber ö,5°C/i'inute auf eine Temperatur von etwa 32 bis 3ü C abkiüilt.üiihren adds, and (e) the suspension obtained with a Velocity of however Ö.5 ° C / i'inute to one temperature cooled from about 32 to 3 ° C.

Es vrarJe nun geXunäen, daiS" sich aie lextilscnuuilze-Zusammen-« aetzung mit ^uI 0*1 iJl·: en schäften, herst allen ;äfc.st, wenn die letzte iivhiistufe auf eine .Lnd tempera tür von 21-32 C durchgef Jhi't v.ira, /obei das Abkühlen "bei der vorbesohriebenen Greaohv.'iiidijfceit von über Ü,5°C/Hin. stattfindet. ^It now appears that "the lextilsnuuilze-" with ^ uI 0 * 1 iJl ·: en shafts, manufacure all; Äfc.st, if last iivhiistufe on a .Lnd tempera door of 21-32 C carried out Jhi't v.ira, / obei the cooling "at the pre-planed Greaohv.'iiidijfceit of over Ü, 5 ° C / Hin. takes place. ^

Ss wurde .lU-ierie-. .jefunden, daI3 ein Produkt erhalten werden :La:x:i, das eine Vieicosität hat, die im 3ereioii von 200-500 Oentipoise bei Äauaterr^peratur (25 C) liegt, und das deshalb voii. Vcrbrc.a.?iier ohne weiteres aus dem Behälter gegossen weraen kan:. und/oaer ohx-e weiteres weit erver dUimt mit .vasser una iiör«r."iert in V/asaer „eruer. kann, wenn die letzte ^"■...l.ita.iQ 3-ehr ssc-iüiell durchsefüax't .vird. Zu aieseu Zv/eck soll die rJuspsr.^iv-n iileiciiuiäii/: von einer xem^Bx-atur von 3b-90,^°C auf -„ine Abfüllte-acei-utur von 21 -2."20C In einer £titspar.iie von ί-1ϋθ Sek., vorsuvs//eise in 15-30 Sek., abgeicU:*it werden.Ss became .lU-ierie-. It has been found that a product is obtained: La: x: i, which has a viscosity which is in the range of 200-500 oentipoise at external temperature (25 C), and which is therefore voii. Vcrbrc.a.?iier can easily be poured out of the container. and / oaer ohx-e further further dUimt with .vasser una iiör «r." iert in V / asaer "eruer. can, if the last ^" ■ ... l.ita.iQ 3-ehr ssc-iüiell durchsefüax 't .vird. To aieseu Zv / eck should the rJuspsr. ^ Iv-n iileiciiuiäii /: from a xem ^ Bx-atur of 3b-90, ^ ° C to - "ine Bottled-acei-utur of 21-2." 2 0 C In a £ titspar.iie of ί-1ϋθ sec., vorsuvs // eise in 15-30 sec., abicU : * it will be.

Bae sch;,eile A^t'ailen kaun dadurch erreicht werden, daßBae sch;, hurry A ^ t'ailen can be achieved by that

n.'.öise aie 88-9C-, 5 0 v/arae Suspension durch einen us-taaschö*- ^efahrt v/ira oder aber in einen icit einemn. '. öise aie 88-9C-, 50 v / arae suspension by a us-taaschö * - ^ efahrt v / ira or in an icit one

iäantrii UiK1-e.enden 2ank oder durch Zugabe von kaltem Mets&x', oeiöpiels.-eise mit einer Tempera tür von 40C, Eis oäer eine..-, anaeren ICUhImIttel» Die abgekühlte Suspension lässt 3Ϊ3ί: filtrier en und wenn sie die Temperatur von 21-520C err-sioLt iiat, In Behälter verpacken.iäantrii UiK 1 -e.enden 2ank or by adding cold Mets & x ', oeiöpiels.-ice with a temperature door of 4 0 C, ice oäer an ..-, anaer ICUhImIttel »The cooled suspension lets 3Ϊ3ί: filter and when it the temperature of 21-52 0 C err-sioLt iiat, pack in container.

badbath

0 9 8 kU /16 5 80 9 8 kU / 16 5 8

Claims (1)

PatentanspruchesClaim 1. Verfahren zur Herstellung einer Textilschmälae, bei dem1. Process for the production of a Textilschmälae, in which (1) ein Fincher-Tropsch-Wachs mit einer Kettenlänge von etwa 40 bis etwa bi? Kohlenstoffatomen, einem SchmelzpunktBuereich von etwa 93 tis etwa 1Q4°C, einer Säurezahl von etwa 10 bis etwa 35, und einer Durchdringung von etwa 1 bis etwa 6, bei 104 G geschmolzen wird,(1) a Fincher-Tropsch wax with a chain length of about 40 to about bi? Carbon atoms, a melting point range from about 93 to about 104 ° C, an acid number from about 10 to about 35, and a penetration of about 1 to about 6, is melted at 104 G, (2) die Schmalze gleichmäßig mit einem Emulgator |;eiüischt wird, der entweder(2) Mix the lard evenly with an emulsifier will that either (a) eine kationiache quaternäre Ammoniumverbindung der Formel(a) a cationic quaternary ammonium compound of the formula B1-H-(E3O)xHB 1 -H- (E 3 O) x H (H1O) H(H 1 O) H in welcher R^ eine Alky!gruppe mit 14 bis 20 Kohlenstoffatomen, Ro eine Alkylgruppe mit 1 bis 3 Kohlenstoffatomen, eine Phenyl-, Naphthyl- oder Cj-Chalky 1-aubstituierte Phenylgruppe, die beiden R», die gleich oder verschieden sein können, eine Alkylengruppe mit 2 bis 4 Kohlenstoffatomen, Z~ ein Anion, X plus Y den Wert 1 bis 6 und X den Wert 1 bis 6 bedeuten, oderin which R ^ is an alkyl group with 14 to 20 carbon atoms, Ro is an alkyl group with 1 to 3 carbon atoms, a phenyl, naphthyl or Cj-chalky 1-substituted phenyl group, the two R », which can be the same or different, an alkylene group with 2 to 4 carbon atoms, Z ~ Anion, X plus Y denote the value 1 to 6 and X denote the value 1 to 6, or (b) ein G-emisoh dieser kationischen quaternären Ammonium verbindung mit einem nichtionischen Emulgator, der mindestens 8 Äthylenoxydeinheiten (O2H.O) enthält, wobei das Gewxohtaverhäitnis des niohtionischen Emulgators zur kationischen quaternären Ammoniumverbindung 7*3 nicht übersteigt und das Gewichtsverhältnis des oxidierten Fischer-Iropsch-Waohaes zur Gesamtmenge des Emulgators 10j 1 bis 3s7 beträgt, ist,(b) a G-emisoh of this cationic quaternary ammonium combination with a non-ionic emulsifier containing at least 8 ethylene oxide units (O2H.O), wherein the weight ratio of the nonionic emulsifier to the cationic quaternary ammonium compound 7 * 3 and does not exceed the weight ratio of the oxidized Fischer-Iropsch-Waohaes to the total amount of the emulsifier 10j is 1 to 3s7, is, 909844/1658909844/1658 (3) das Gemisch auf 121 bis 143°C erwärmt wird und(3) the mixture is heated to 121 to 143 ° C and (4) unter ständigem ülihren zu ./asaer mit einer Temperatur von 88 bis 90,5 C gegeben wird, dadurch gekennzeichnet, daß die entstandene Suspension mit einer Geschwindigkeit von über O,5°C/Min. auf eine Temperatur von 21 bis unter 320C abgekühlt wird.(4) is added with constant ülihren to ./asaer at a temperature of 88 to 90.5 C, characterized in that the resulting suspension at a rate of about 0.5 ° C / min. to a temperature of 21 to below 32 0 C is cooled. Verfahren nach Anspruch 1, dadurch gekenn se lehnet, da/3 zur jSrzielung einer Viscositüt von 200-500 Ceritipoise bei 250C die entstandene Suspension während einer Zeitspanne von 5-100 Sekunden, vorzugsweise 15-30 Sek. auf eine Temperatur von 21 bis unter 320C abgekühlt wird.A method according to claim 1, characterized labeled in se leans, as / 3 for a jSrzielung Viscositüt 200-500 Ceritipoise at 25 0 C, the resulting suspension over a period of 5-100 seconds, preferably 15-30 sec. To a temperature of 21 to is cooled below 32 0 C. PurPure The Procter & Gamble CompanyThe Procter & Gamble Company Cincinnati, Ohio, 7»St.k. Cincinnati, Ohio, 7th St. k. HechtsanwaltPike attorney 9098'. 4 /16589098 '. 4/1658
DE1966P0040527 1964-04-28 1966-10-08 Process for the production of a textile melt Pending DE1619139A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US36328864A 1964-04-28 1964-04-28
US49491065A 1965-10-11 1965-10-11

Publications (1)

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DE1619139A1 true DE1619139A1 (en) 1969-10-30

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Application Number Title Priority Date Filing Date
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GB (1) GB1116149A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4433597C2 (en) * 1993-09-28 1996-10-02 Clariant Finance Bvi Ltd Process for increasing the wet lubricity of textile material and wet lubricant therefor

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GB1116149A (en) 1968-06-06

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