DE1249837B - Verfahren zur Gewinnung von reinem Wasserstoff aus einem Gasgemisch, das Wasserstoff, Stickstoff sowie geringe Mengen Ammoniak und Wasser enthält - Google Patents

Verfahren zur Gewinnung von reinem Wasserstoff aus einem Gasgemisch, das Wasserstoff, Stickstoff sowie geringe Mengen Ammoniak und Wasser enthält

Info

Publication number
DE1249837B
DE1249837B DENDAT1249837D DE1249837DA DE1249837B DE 1249837 B DE1249837 B DE 1249837B DE NDAT1249837 D DENDAT1249837 D DE NDAT1249837D DE 1249837D A DE1249837D A DE 1249837DA DE 1249837 B DE1249837 B DE 1249837B
Authority
DE
Germany
Prior art keywords
hydrogen
pressure
gas mixture
nitrogen
layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DENDAT1249837D
Other languages
German (de)
English (en)
Inventor
Buffalo N. Y. Robert Walter Alexis Williamsville N.Y. William Francis (V. St. A.)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Union Carbide Corp
Original Assignee
Union Carbide Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Publication date
Publication of DE1249837B publication Critical patent/DE1249837B/de
Pending legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01S—RADIO DIRECTION-FINDING; RADIO NAVIGATION; DETERMINING DISTANCE OR VELOCITY BY USE OF RADIO WAVES; LOCATING OR PRESENCE-DETECTING BY USE OF THE REFLECTION OR RERADIATION OF RADIO WAVES; ANALOGOUS ARRANGEMENTS USING OTHER WAVES
    • G01S3/00—Direction-finders for determining the direction from which infrasonic, sonic, ultrasonic or electromagnetic waves, or particle emission, not having a directional significance, are being received
    • G01S3/80—Direction-finders for determining the direction from which infrasonic, sonic, ultrasonic or electromagnetic waves, or particle emission, not having a directional significance, are being received using ultrasonic, sonic or infrasonic waves
    • G01S3/802—Systems for determining direction or deviation from predetermined direction
    • G01S3/803—Systems for determining direction or deviation from predetermined direction using amplitude comparison of signals derived from receiving transducers or transducer systems having differently-oriented directivity characteristics
    • G01S3/8034—Systems for determining direction or deviation from predetermined direction using amplitude comparison of signals derived from receiving transducers or transducer systems having differently-oriented directivity characteristics wherein the signals are derived simultaneously
    • G01S3/8038—Systems for determining direction or deviation from predetermined direction using amplitude comparison of signals derived from receiving transducers or transducer systems having differently-oriented directivity characteristics wherein the signals are derived simultaneously derived from different combinations of signals from separate transducers comparing sum with difference
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification
    • C01B3/56—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/106—Silica or silicates
    • B01D2253/108—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/30—Physical properties of adsorbents
    • B01D2253/302—Dimensions
    • B01D2253/308—Pore size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/102—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/40—Nitrogen compounds
    • B01D2257/406—Ammonia
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/80—Water
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40064—Five
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/402—Further details for adsorption processes and devices using two beds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C01B2203/043—Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0495—Composition of the impurity the impurity being water

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Radar, Positioning & Navigation (AREA)
  • Remote Sensing (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Catalysts (AREA)
DENDAT1249837D 1960-05-26 Verfahren zur Gewinnung von reinem Wasserstoff aus einem Gasgemisch, das Wasserstoff, Stickstoff sowie geringe Mengen Ammoniak und Wasser enthält Pending DE1249837B (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US31888A US3111387A (en) 1960-05-26 1960-05-26 Hydrogen recovery

Publications (1)

Publication Number Publication Date
DE1249837B true DE1249837B (de) 1967-09-14

Family

ID=21861933

Family Applications (1)

Application Number Title Priority Date Filing Date
DENDAT1249837D Pending DE1249837B (de) 1960-05-26 Verfahren zur Gewinnung von reinem Wasserstoff aus einem Gasgemisch, das Wasserstoff, Stickstoff sowie geringe Mengen Ammoniak und Wasser enthält

Country Status (5)

Country Link
US (1) US3111387A (show.php)
BE (1) BE604026A (show.php)
DE (1) DE1249837B (show.php)
GB (1) GB977969A (show.php)
NL (1) NL265205A (show.php)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3221476A (en) * 1961-12-07 1965-12-07 Chemical Design Inc Adsorption-desorption method
NL136381C (show.php) * 1962-02-26
NL297067A (show.php) * 1962-09-04 1900-01-01
US3306706A (en) * 1962-10-17 1967-02-28 Hydrocarbon Research Inc Process for producing hydrogen and hydrogen carrier therefor
US3254956A (en) * 1963-03-14 1966-06-07 Bishop & Co Platinum Works J Production of ultra pure hydrogen
US3479149A (en) * 1963-09-10 1969-11-18 Mobil Oil Corp Process for reducing carbon dioxide with hydrogen to carbon monoxide
DE3143993A1 (de) * 1981-11-05 1983-05-11 Bayer Ag, 5090 Leverkusen Molekularsieb-zeolith fuer die gewinnung von wasserstoff mit der druckwechsel-adsorptions-technik
DE3333386A1 (de) * 1983-09-15 1985-04-11 Siemens AG, 1000 Berlin und 8000 München Verfahren und einrichtung zum beschriften von teilen, insbesondere von elektronischen bauelementen
GB8414491D0 (en) * 1984-06-07 1984-07-11 Humphreys & Glasgow Ltd Ammonia plant re-vamp process
US4957514A (en) * 1989-02-07 1990-09-18 Air Products And Chemicals, Inc. Hydrogen purification
FR2718979B1 (fr) * 1994-04-20 1996-06-07 Air Liquide Procédé de redémarrage d'un récipient de purification d'hydrogène par adsorption, et son application au traitement de certains gaz contenant de l'hydrogène.
US7404846B2 (en) * 2005-04-26 2008-07-29 Air Products And Chemicals, Inc. Adsorbents for rapid cycle pressure swing adsorption processes
DK200801093A (en) * 2008-08-13 2010-02-14 Topsoe Haldor As Process and system for removing impurities from a gas stream
JP6473221B2 (ja) * 2014-07-03 2019-02-20 ヌヴェラ・フュエル・セルズ，エルエルシー 圧縮された湿潤水素を乾燥させるための吸収ベッドを再生するためのシステムおよび方法
US11655147B2 (en) * 2020-10-20 2023-05-23 Hyundai Motor Company System and method for generating hydrogen through ammonia adsorption
CN117529359A (zh) 2021-06-18 2024-02-06 气体产品与化学公司 氨裂化用于绿色氢
KR102667696B1 (ko) * 2021-12-31 2024-05-22 한국에너지기술연구원 암모니아 분해가스로부터 수소 정제용 압력변동흡착장치 및 이를 이용한 수소 정제 방법
KR102921114B1 (ko) * 2022-07-06 2026-02-02 주식회사 포스코 이산화탄소 프리 암모니아 분해 설비

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2578193A (en) * 1949-03-01 1951-12-11 Jr Walton H Marshall Ammonia dissociator
US2601221A (en) * 1949-03-29 1952-06-17 Baker & Co Inc Dissociation of ammonia
US2882244A (en) * 1953-12-24 1959-04-14 Union Carbide Corp Molecular sieve adsorbents
US2882243A (en) * 1953-12-24 1959-04-14 Union Carbide Corp Molecular sieve adsorbents
US2901519A (en) * 1957-04-29 1959-08-25 Exxon Research Engineering Co Molecular sieve separation process
US2944627A (en) * 1958-02-12 1960-07-12 Exxon Research Engineering Co Method and apparatus for fractionating gaseous mixtures by adsorption
US3025145A (en) * 1958-07-28 1962-03-13 Gen Electric Retort for an ammonia dissociator and the like
NL127140C (show.php) * 1959-11-30

Also Published As

Publication number Publication date
NL265205A (show.php)
GB977969A (en) 1964-12-16
BE604026A (fr) 1961-09-18
US3111387A (en) 1963-11-19

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