DE10210C - Process for the production of lacquers by treating nitrocellulose with solvents - Google Patents
Process for the production of lacquers by treating nitrocellulose with solventsInfo
- Publication number
- DE10210C DE10210C DENDAT10210D DE10210DA DE10210C DE 10210 C DE10210 C DE 10210C DE NDAT10210 D DENDAT10210 D DE NDAT10210D DE 10210D A DE10210D A DE 10210DA DE 10210 C DE10210 C DE 10210C
- Authority
- DE
- Germany
- Prior art keywords
- nitro
- camphor
- cellulose
- solvents
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000020 Nitrocellulose Substances 0.000 title claims description 22
- 229920001220 nitrocellulos Polymers 0.000 title claims description 22
- 239000002904 solvent Substances 0.000 title claims description 20
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- 238000000034 method Methods 0.000 title claims description 4
- 239000004922 lacquer Substances 0.000 title description 2
- 229940079938 Nitrocellulose Drugs 0.000 claims description 21
- FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2S,3R,4S,5R,6R)-2-[(2R,3R,4S,5R,6S)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2R,3R,4S,5R,6S)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical class O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 claims description 20
- DSSYKIVIOFKYAU-UHFFFAOYSA-N Camphor Chemical compound C1CC2(C)C(=O)CC1C2(C)C DSSYKIVIOFKYAU-UHFFFAOYSA-N 0.000 claims description 16
- 229960000846 Camphor Drugs 0.000 claims description 16
- 241000723346 Cinnamomum camphora Species 0.000 claims description 16
- 229930007890 camphor Natural products 0.000 claims description 16
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 229920001800 Shellac Polymers 0.000 claims description 5
- 229940113147 shellac Drugs 0.000 claims description 5
- 235000013874 shellac Nutrition 0.000 claims description 5
- 239000004208 shellac Substances 0.000 claims description 5
- LSNNMFCWUKXFEE-UHFFFAOYSA-N sulfonic acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 5
- -1 chlorine-carbon Chemical compound 0.000 claims description 4
- 238000002844 melting Methods 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 239000002966 varnish Substances 0.000 claims description 4
- 241000779819 Syncarpia glomulifera Species 0.000 claims description 3
- 229940036248 Turpentine Drugs 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 239000001739 pinus spp. Substances 0.000 claims description 3
- 229920002160 Celluloid Polymers 0.000 claims description 2
- 238000004040 coloring Methods 0.000 claims 1
- 238000004090 dissolution Methods 0.000 claims 1
- 238000010422 painting Methods 0.000 claims 1
- 239000000975 dye Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229920000591 gum Polymers 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 210000001520 Comb Anatomy 0.000 description 1
- 229920002522 Wood fibre Polymers 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 239000006193 liquid solution Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 230000001681 protective Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 230000001131 transforming Effects 0.000 description 1
- 239000002025 wood fiber Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/16—Esters of inorganic acids
- C09D101/18—Cellulose nitrate
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
- H01M50/30—Arrangements for facilitating escape of gases
- H01M50/317—Re-sealable arrangements
- H01M50/325—Re-sealable arrangements comprising deformable valve members, e.g. elastic or flexible valve members
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Description
1879.1879.
KlasseGreat
HENRY PARKES in BIRMINGHAM (England). Verfahren zur Herstellung von Lacken durch Behandeln von NitrocellulHENRY PARKES in BIRMINGHAM (England). Process for the production of lacquers by treating nitrocellul
Patentirt im Deutschen Reiche vom 29. October 1879 ab.Patented in the German Empire on October 29, 1879.
Der nach dem verbesserten Verfahren herzustellende Körper kann zur Fabrikation verschiedenartiger Gegenstände dienen, wie zu Kämmen, Bürstendeckeln, Cliches, Stereotypplatten, Messerschalen, Klaviertasten; ferner zur Bildung künstlicher Zähne und dergleichen mehr.The body to be produced according to the improved method can be used for production of various types Objects serve as combs, brush covers, cliches, stereotype plates, Knife shells, piano keys; also for the formation of artificial teeth and the like.
Zur Ausführung ,meiner Erfindung bediene ich mich der Nitro - Cellulose, gleichviel, ob dieselbe aus Papier, Baumwolle, Leinen, gewebten, gefilzten, zerfallenen Substanzen oder Holzfasern u. s. w. hergestellt worden, und gleichviel, ob sie nach ihrer Umwandlung gebleicht oder gefärbt worden ist oder nicht.To carry out my invention, I use nitro-cellulose, regardless of whether the same made of paper, cotton, linen, woven, felted, disintegrated substances or Wood fibers etc. have been produced, and it does not matter whether they are bleached after their transformation or has been colored or not.
Ich erweiche oder löse die Nitro - Cellulose in einer Auflösung von vierfach Chlorkohlenstoff und Kampher allein oder mit anderen Auflösungsmitteln, wie Gummi, Harze, OeIe, Farbstoffe u. s. w. versetzt.I soften or dissolve the nitro - cellulose in a fourfold chlorocarbon solution and camphor alone or with other dissolving agents such as gum, resins, oils, Dyes and so on added.
• Ein anderes Lösungsmittel, dessen ich mich bediene, besteht aus zweifach Schwefel-Kohlenstoff und Kampher; die Lösung der Nitrocellulose geschieht hierbei vorzugsweise unter An- ■ Wendung von Hitze und Druck.• Another solvent I use is double sulfur carbon and camphor; the solution of the nitrocellulose is preferably done with an ■ Turn of heat and pressure.
Ein gutes Lösungsmittel für Nitro - Cellulose ist Kampher, wenn er bis zu seinem Schmelzpunkt erhitzt wird; bei dieser Temperatur löst sich die Nitro-Cellulose ebenso schnell, wie sie dem geschmolzenen Kampher zugefügt wird, bis er eine steife Masse bildet; die Verbindung geht noch schneller vor sich, wenn das Gefäfs, in welchem die Lösung vorgenommen werden soll, unter Druck gesetzt wird. Der Masse können andere Stoffe beigefügt werden, und die mehr oder weniger feste, .plastische Masse läfst sich formen oder kann zu, verschiedenen Formen ausgewalzt werden, wie zu dünnen Platten, Röhren, Cylindern u. s. w.A good solvent for nitro cellulose is camphor if it is up to its melting point is heated; at this temperature the nitro-cellulose dissolves as quickly as it does added to the melted camphor until it forms a stiff mass; the connection goes on even faster when the vessel in which the solution is made is supposed to be put under pressure. Other substances can be added to the mass, and the more or less solid, plastic mass can be shaped or can be different Shapes are rolled out, such as thin plates, tubes, cylinders and so on.
Ist es erwünscht, die hohe Schmelzhitze des Kamphers zu erniedrigen, so können demselben Körper, wie OeIe, Paraffin, Terpentin, Alkohol, Benzol, Aether u. s. w. zugesetzt werden, wodurch dünnere Auflösungen erzielt werden.If it is desired to lower the high melting temperature of camphor, the same can be used Body such as oil, paraffin, turpentine, alcohol, benzene, ether, etc. are added, whereby thinner resolutions can be achieved.
Ein anderes Lösungsmittel der Nitro-Cellulose wird hergestellt, indem man schweflige Säure durch granulirten Kampher hindurchleitet, bis derselbe von dem schwefligsauren Gas aufgelöst worden. Die so erhaltene schwefligsaure Lösung ist ein starkes Auflösungsmittel für Nitro-Cellulose und seine Verbindungen. Auch stelle ich Lösungsmittel dar, indem ich Kampher in schwefliger Säure auflöse.Another solvent of nitro-cellulose is made by adding sulphurous acid passes through granulated camphor until it is dissolved by the sulphurous acid gas been. The sulfuric acid solution thus obtained is a strong dissolving agent for nitro-cellulose and its connections. I also make solvents by putting camphor in Dissolve sulphurous acid.
Ein anderes Lösungsmittel der Nitro-Cellulose wird erhalten durch Auflösen von Kampher in Benzol von solcher Qualität, dafs kein unangenehmer Geruch verbleibt, wenn die Celluloidverbindungen fertig sind; diese Lösung arbeitet sehr schnell unter Mitwirkung von Wärme und Druck. QeIe, Gummi, Harze und Farbstoffe können nach Belieben beigemischt werden.Another solvent of nitro-cellulose is obtained by dissolving camphor in Benzene of such a quality that no unpleasant odor remains when the celluloid compounds are done; this solution works very quickly with the participation of heat and Pressure. QeIe, gum, resins and dyes can be added as desired.
Terpentin und Kampher lösen bei Erwärmung und Druck die Nitro-Cellulose schnell auf.Turpentine and camphor dissolve the nitro-cellulose quickly when heated and under pressure.
Ich habe gefunden, dafs Nitro-Cellulose sich schnell erweicht, wenn sie mit Alkohol, Aether, Weingeist oder anderen Lösungsmitteln der Schiefsbaumwolle besprengt oder in dieselben eingetaucht wird und nun der Hitze und dem Druck in Formen u. s. w. ausgesetzt wird.I have found that nitro-cellulose softens quickly when mixed with alcohol, ether, Spirit of alcohol or other solvents sprinkled with the skew cotton or in the same is immersed and is now exposed to heat and pressure in molds and so on.
Bisweilen ist es besser, die Nitro-Cellulose vor der Auflösung zu färben, wobei man zarte und glänzende Farben erhält, die schöner sind, als die nach den bisher gebräuchlichen Methoden erhaltenen.Sometimes it is better to dye the nitro-cellulose before dissolving it, being more delicate and gets shiny colors that are more beautiful than those obtained by the methods that have hitherto been used received.
Wenn die Compositionen der Nitro-Cellulose als Lacke gebraucht werden sollen, so ist natürlich viel mehr flüssiges Lösungsmittel nöthig, als wenn feste Körper gebildet werden sollen. Die Lösungen können allein verwendet werden oder man kann sie mit anderen Stoffen vermischen, wie mit Gummi, Harzen, Pigmentfarben, Metallbroncen u. s. w., um alle möglichen Variationen zu erhalten, und damit schutz- oder wasserdichte Anstriche für Flächen zu gewinnen oder die Masse zum Verkapseln von Flaschen zu verwenden. Auch Schellack vermische ich mit den flüssigen Lösungen der Nitro-Cellulose. Dies wird mir insofern möglich, da die Lösungsmittel, welche ich zum Auflösen der Nitro-Cellulose verwende, auch Lösungsmittel für Schellack sind. Alle obengenannten Lösungsmittel können hierzu gebraucht werden, ebenso läfst sich zweifach Schwefel-Kohlenstoff mit Benzol und Weingeist gebrauchen.If the compositions of nitro-cellulose are to be used as varnishes, it is natural much more liquid solvent is required than when solids are to be formed. The solutions can be used alone or they can be mixed with other substances, like with rubber, resins, pigment paints, metal bronzes and so on, to all kinds of things To obtain variations, and thus to gain protective or waterproof coatings for surfaces or to use the mass to encapsulate bottles. Mix shellac as well I use the liquid solutions of nitro-cellulose. This becomes possible for me insofar as because the solvents that I use to dissolve the nitro-cellulose are also solvents for shellac are. All the solvents mentioned above can be used for this purpose, and sulfur-carbon can also be used twice to use with benzene and alcohol.
In einzelnen Fällen können Lösungen von Schellack in einem der obengenannten Lösungsmittel mit Ricinusöl und mit metallischen Broncen oder Pigmenten gebraucht werden, um Flächen zu lackiren oder anzustreichen.In individual cases, solutions of shellac in one of the solvents mentioned above can be used with castor oil and with metallic bronzes or pigments are used to varnish or paint surfaces.
Claims (10)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE10210C true DE10210C (en) |
Family
ID=287525
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT10210D Active DE10210C (en) | Process for the production of lacquers by treating nitrocellulose with solvents |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE10210C (en) |
-
0
- DE DENDAT10210D patent/DE10210C/en active Active
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