DE102016013753A1 - Verfahren und Vorrichtung zur Synthesegaszerlegung mittels Sauergaswäsche und kryogenem Trennprozess - Google Patents
Verfahren und Vorrichtung zur Synthesegaszerlegung mittels Sauergaswäsche und kryogenem Trennprozess Download PDFInfo
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- DE102016013753A1 DE102016013753A1 DE102016013753.3A DE102016013753A DE102016013753A1 DE 102016013753 A1 DE102016013753 A1 DE 102016013753A1 DE 102016013753 A DE102016013753 A DE 102016013753A DE 102016013753 A1 DE102016013753 A1 DE 102016013753A1
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- gas
- cryogenic
- pressure level
- carbon monoxide
- nitrogen
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- 238000000926 separation method Methods 0.000 title claims abstract description 64
- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 44
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 44
- 238000000034 method Methods 0.000 title claims abstract description 33
- 238000005201 scrubbing Methods 0.000 title claims abstract description 24
- 239000002253 acid Substances 0.000 title claims abstract description 18
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 140
- 239000007789 gas Substances 0.000 claims abstract description 127
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 68
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims abstract description 46
- 229910002091 carbon monoxide Inorganic materials 0.000 claims abstract description 46
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000003507 refrigerant Substances 0.000 claims abstract description 28
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 23
- 239000001257 hydrogen Substances 0.000 claims abstract description 23
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 19
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 8
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 8
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910052717 sulfur Inorganic materials 0.000 claims abstract description 6
- 239000011593 sulfur Substances 0.000 claims abstract description 6
- 239000007791 liquid phase Substances 0.000 claims description 19
- 238000009833 condensation Methods 0.000 claims description 17
- 230000005494 condensation Effects 0.000 claims description 17
- 238000010438 heat treatment Methods 0.000 claims description 16
- 238000001816 cooling Methods 0.000 claims description 15
- 239000012071 phase Substances 0.000 claims description 8
- 238000010992 reflux Methods 0.000 claims description 8
- 238000005057 refrigeration Methods 0.000 claims description 6
- 230000006835 compression Effects 0.000 claims description 4
- 238000007906 compression Methods 0.000 claims description 4
- 150000002431 hydrogen Chemical class 0.000 claims description 4
- 239000012808 vapor phase Substances 0.000 claims description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- 239000003599 detergent Substances 0.000 description 9
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- 239000007788 liquid Substances 0.000 description 5
- 230000008929 regeneration Effects 0.000 description 5
- 238000011069 regeneration method Methods 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 239000003245 coal Substances 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000004172 nitrogen cycle Methods 0.000 description 2
- 239000004071 soot Substances 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 208000001034 Frostbite Diseases 0.000 description 1
- QJGQUHMNIGDVPM-BJUDXGSMSA-N Nitrogen-13 Chemical compound [13N] QJGQUHMNIGDVPM-BJUDXGSMSA-N 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- AFYPFACVUDMOHA-UHFFFAOYSA-N chlorotrifluoromethane Chemical compound FC(F)(F)Cl AFYPFACVUDMOHA-UHFFFAOYSA-N 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000002737 fuel gas Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 239000010742 number 1 fuel oil Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
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- Y02C20/00—Capture or disposal of greenhouse gases
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
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DE102016013753.3A DE102016013753A1 (de) | 2016-11-18 | 2016-11-18 | Verfahren und Vorrichtung zur Synthesegaszerlegung mittels Sauergaswäsche und kryogenem Trennprozess |
PCT/EP2017/025324 WO2018091146A1 (de) | 2016-11-18 | 2017-11-08 | Verfahren und vorrichtung zur synthesegaszerlegung mittels sauergaswäsche und kryogenem trennprozess |
CN201780071227.7A CN109963810B (zh) | 2016-11-18 | 2017-11-08 | 使用酸性气体洗涤和低温分离工艺进行合成气分馏的方法和装置 |
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Cited By (2)
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FR3097951A1 (fr) * | 2019-06-26 | 2021-01-01 | L'Air Liquide Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Procede et appareil de separation cryogenique d’un gaz de synthese pour la production de ch4 |
EP3851179A1 (en) * | 2020-01-14 | 2021-07-21 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Method and apparatus for separating a synthesis gas by cryogenic distillation |
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FR2718725B1 (fr) * | 1994-04-13 | 1996-05-24 | Air Liquide | Procédé et installation de séparation d'un mélange gazeux. |
FR2775276B1 (fr) * | 1998-02-20 | 2002-05-24 | Air Liquide | Procede et installation de production de monoxyde de carbone et d'hydrogene |
US6416568B1 (en) * | 1999-05-14 | 2002-07-09 | Texaco, Inc. | Hydrogen recycle and acid gas removal using a membrane |
DE102005021530A1 (de) * | 2005-05-10 | 2006-11-23 | Linde Ag | Verfahren und Vorrichtung zur Gewinnung von Produkten aus Synthesegas |
DE102005025651A1 (de) * | 2005-06-03 | 2006-12-07 | Linde Ag | Verfahren und Vorrichtung zur Gewinnung von Produkten aus Synthesegas |
EP2311544A1 (en) * | 2009-10-05 | 2011-04-20 | L'Air Liquide Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Process and apparatus for the treatment of a synthesis gas |
WO2012097497A1 (en) * | 2011-01-17 | 2012-07-26 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Process and apparatus for production of ammonia synthesis gas and pure methane by cryogenic separation |
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Cited By (3)
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FR3097951A1 (fr) * | 2019-06-26 | 2021-01-01 | L'Air Liquide Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Procede et appareil de separation cryogenique d’un gaz de synthese pour la production de ch4 |
EP3851179A1 (en) * | 2020-01-14 | 2021-07-21 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Method and apparatus for separating a synthesis gas by cryogenic distillation |
US11999622B2 (en) | 2020-01-14 | 2024-06-04 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Method and apparatus for separating a synthesis gas by cryogenic distillation |
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CN109963810B (zh) | 2023-01-24 |
WO2018091146A1 (de) | 2018-05-24 |
CN109963810A (zh) | 2019-07-02 |
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